WO2006089773A3 - Verfahren und vorrichtung zur konzentrationsermittlung von organisch gebundenen halogenen - Google Patents

Verfahren und vorrichtung zur konzentrationsermittlung von organisch gebundenen halogenen Download PDF

Info

Publication number
WO2006089773A3
WO2006089773A3 PCT/EP2006/001717 EP2006001717W WO2006089773A3 WO 2006089773 A3 WO2006089773 A3 WO 2006089773A3 EP 2006001717 W EP2006001717 W EP 2006001717W WO 2006089773 A3 WO2006089773 A3 WO 2006089773A3
Authority
WO
WIPO (PCT)
Prior art keywords
test sample
concentration
sample
bound halogens
organically bound
Prior art date
Application number
PCT/EP2006/001717
Other languages
English (en)
French (fr)
Other versions
WO2006089773A2 (de
Inventor
Christian Buck
Original Assignee
Merck Patent Gmbh
Christian Buck
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE200520006570 external-priority patent/DE202005006570U1/de
Priority claimed from DE202005010595U external-priority patent/DE202005010595U1/de
Application filed by Merck Patent Gmbh, Christian Buck filed Critical Merck Patent Gmbh
Priority to EP06707256A priority Critical patent/EP1851530A2/de
Priority to US11/817,047 priority patent/US20080153173A1/en
Priority to AU2006218103A priority patent/AU2006218103A1/en
Priority to JP2007557391A priority patent/JP2008532023A/ja
Publication of WO2006089773A2 publication Critical patent/WO2006089773A2/de
Publication of WO2006089773A3 publication Critical patent/WO2006089773A3/de

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/18—Water
    • G01N33/1826—Water organic contamination in water
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/19—Halogen containing
    • Y10T436/193333—In aqueous solution

Abstract

Bei einem Verfahren zur Ermittlung der Konzentration von in Abwasser befindlichen organisch gebundenen Halogenen wird eine vorgegebene Menge an Abwasser entnommen und in eine Messprobe überführt. Anschließend wird an der Messprobe eine spektrale Messung durchgeführt und das Ergebnis der spektralen Messung mit Referenzmessungen verglichen, um die Konzentration der organisch gebundenen Halogene zu bestimmen. Die organisch gebundenen Halogene werden durch Extraktion oder Adsorption in der Messprobe angereichert. Anorganisch gebundene Halogene werden aus der Messprobe entfernt. Der Vergleich der spektralen Messung mit Referenzmessungen wird mit chemometrischen Methoden durchgeführt. Eine automatische Messvorrichtung 9 weist eine Vorrichtung 10 zur Entnahme einer Probenmenge aus einem Fließsystem, eine Vorrichtung 11 zum Überführen der Probenmenge in eine Messprobe, eine Vorrichtung 12 zur Durchführung von spektralen Messungen an der Messprobe und eine Auswertevorrichtung 13 zur Auswertung des Ergebnisses der spektralen Messungen mit Referenzmessungen auf . Die Messvorrichtung weist auch eine Vorrichtung zur automatischen Bereitstellung einer Probenmenge sowie eine Vorrichtung 11 zur automatischen Überführung der Messprobe in die Vorrichtung 12 zur Durchführung der spektralen Messung auf. Die Messvorrichtung kann auch zur Durchführung einer Bestimmung der Konzentration anderer spektroskopisch aktiver Substanzen, insbesondere der Konzentrationen von AOX-Beitragern, BTEX-Beitragern, Alkoholen, Peroxiden, Metallen, Aldehyden, Ketonen, Polymeren, Aromaten, funktionalisierten Aromaten oder Polyaromaten verwendet werden.
PCT/EP2006/001717 2005-02-25 2006-02-24 Verfahren und vorrichtung zur konzentrationsermittlung von organisch gebundenen halogenen WO2006089773A2 (de)

Priority Applications (4)

Application Number Priority Date Filing Date Title
EP06707256A EP1851530A2 (de) 2005-02-25 2006-02-24 Verfahren und vorrichtung zur konzentrationsermittlung von organisch gebundenen halogenen
US11/817,047 US20080153173A1 (en) 2005-02-25 2006-02-24 Method and Device for Determining the Concentration of Organically Bound Halogens
AU2006218103A AU2006218103A1 (en) 2005-02-25 2006-02-24 Method and device for determining the concentration of organically bound halogens
JP2007557391A JP2008532023A (ja) 2005-02-25 2006-02-24 有機結合ハロゲン濃度の決定方法および装置

Applications Claiming Priority (8)

Application Number Priority Date Filing Date Title
DE202005003171 2005-02-25
DE202005003171.2 2005-02-28
DE202005006570.6 2005-04-23
DE200520006570 DE202005006570U1 (de) 2005-04-23 2005-04-23 Vorrichtung zur schnellen Onlinemessung von AOX und BTEX mittels Extraktion, Spektroskopie und Chemometrie
DE202005010595.3 2005-07-04
DE202005010595U DE202005010595U1 (de) 2005-02-25 2005-07-04 Vorrichtung zur schnellen Onlinemessung von AOX sowie von Quecksilber und Chalkogenen
DE202005010988.6 2005-07-11
DE202005010988 2005-07-12

Publications (2)

Publication Number Publication Date
WO2006089773A2 WO2006089773A2 (de) 2006-08-31
WO2006089773A3 true WO2006089773A3 (de) 2007-04-26

Family

ID=36228793

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2006/001717 WO2006089773A2 (de) 2005-02-25 2006-02-24 Verfahren und vorrichtung zur konzentrationsermittlung von organisch gebundenen halogenen

Country Status (5)

Country Link
US (1) US20080153173A1 (de)
EP (1) EP1851530A2 (de)
JP (1) JP2008532023A (de)
AU (1) AU2006218103A1 (de)
WO (1) WO2006089773A2 (de)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5764799B2 (ja) * 2011-03-29 2015-08-19 国立研究開発法人産業技術総合研究所 フッ素化不飽和炭化水素の検出方法及び検出センサー
JP5764798B2 (ja) * 2011-03-29 2015-08-19 国立研究開発法人産業技術総合研究所 フッ素化炭化水素の検出方法及び検出センサー
JP5830796B2 (ja) * 2011-03-29 2015-12-09 国立研究開発法人産業技術総合研究所 フッ素化炭化水素化合物の検出方法及び検出センサー
CN111982952A (zh) * 2020-09-03 2020-11-24 北京赛诺新炜科技有限公司 一种有机卤化物检测装置及使用方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5222032A (en) * 1990-10-26 1993-06-22 E. I. Du Pont De Nemours And Company System and method for monitoring the concentration of volatile material dissolved in a liquid
EP0614079A2 (de) * 1993-03-03 1994-09-07 W.R. Grace & Co.-Conn. Verfahren zur direkten Überwachung von Konzentrationen von Bioziden in wässrigen Systemen
US5445008A (en) * 1994-03-24 1995-08-29 Martin Marietta Energy Systems, Inc. Microbar sensor
US5547877A (en) * 1994-10-25 1996-08-20 Ensys Environmental Products, Inc. Methods for the rapid detection of toxic halogenated hydrocarbons and kits useful in performing the same
DE10138428A1 (de) * 2001-08-06 2003-03-06 Ech Elektrochemie Halle Gmbh Verfahren zur summarischen Bestimmung von Organohalogen- und Organoschwefelverbindungen

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5028543A (en) * 1988-03-18 1991-07-02 Dexsil Corporation Method for measuring the content of halogenated organic compounds in soil samples
US5364797A (en) * 1993-05-20 1994-11-15 Mobil Oil Corp. Sensor device containing mesoporous crystalline material
US5358875A (en) * 1993-06-25 1994-10-25 Fic - Fiberchem, Inc. Method and composition for halohydrocarbon detection
US5691205A (en) * 1994-06-23 1997-11-25 Canon Kabushiki Kaisha Fluorometric analysis of chloride ion and chemical sensor therefor

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5222032A (en) * 1990-10-26 1993-06-22 E. I. Du Pont De Nemours And Company System and method for monitoring the concentration of volatile material dissolved in a liquid
EP0614079A2 (de) * 1993-03-03 1994-09-07 W.R. Grace & Co.-Conn. Verfahren zur direkten Überwachung von Konzentrationen von Bioziden in wässrigen Systemen
US5445008A (en) * 1994-03-24 1995-08-29 Martin Marietta Energy Systems, Inc. Microbar sensor
US5547877A (en) * 1994-10-25 1996-08-20 Ensys Environmental Products, Inc. Methods for the rapid detection of toxic halogenated hydrocarbons and kits useful in performing the same
DE10138428A1 (de) * 2001-08-06 2003-03-06 Ech Elektrochemie Halle Gmbh Verfahren zur summarischen Bestimmung von Organohalogen- und Organoschwefelverbindungen

Also Published As

Publication number Publication date
WO2006089773A2 (de) 2006-08-31
JP2008532023A (ja) 2008-08-14
US20080153173A1 (en) 2008-06-26
AU2006218103A1 (en) 2006-08-31
EP1851530A2 (de) 2007-11-07

Similar Documents

Publication Publication Date Title
WO2008020878A3 (en) Contaminant analyzer for fuel
WO2009047731A3 (en) Multi-channel device and method for measuring optical properties of a liquid
WO2007062196A3 (en) Portable meter to measure chlorophyll, nitrogen and water and methods
WO2006089027A3 (en) Lateral flow test kit and method for detecting an analyte
WO2004104552A3 (en) Apparatus and method for process monitoring
WO2006047182A3 (en) Method and apparatus for determining an analyte concentration in a sample having interferents
EP1845363A3 (de) Probenanalysegerät
EP1221341B8 (de) Verfahren und Vorrichtung zur Bestimmung des Volumens einer Flüssigkeitsprobe
Sutherland-Stacey et al. Continuous measurement of dissolved sulfide in sewer systems
DK1725676T3 (da) Kontaminationsmåling
WO2007141718A3 (en) Method and apparatus for providing samples of volatiles to analysis using a multi-port valve and cryo-modulation
WO2001057515A3 (en) Analytical devices based on diffusion boundary layer calibration and quantitative sorption
WO2006089773A3 (de) Verfahren und vorrichtung zur konzentrationsermittlung von organisch gebundenen halogenen
WO2008155820A1 (ja) 異常特定方法および分析装置
Bartolomé et al. Applying no-depletion equilibrium sampling and full-depletion bioaccessibility extraction to 35 historically polycyclic aromatic hydrocarbon contaminated soils
WO2009089130A3 (en) Apparatus and method for determining analyte content in a fluid
Chen et al. Solid phase extraction coupled with a liquid waveguide capillary cell for simultaneous redox speciation analysis of dissolved iron in estuarine and coastal waters
CN102175787A (zh) 采用排阻色谱分析水中溶解态有机物相对分子量的方法
WO2008084600A1 (ja) 波長特定方法および分析装置
DE60222016D1 (de) Spektroskopisches verfahren zur bestimmung der konzentration eines analyten in einer probe
Gutierrez et al. Assessment of field fluorometers
Bucci et al. Oils and grease determination by FT-IR and n-hexane as extraction solvent
CN206540820U (zh) 一种铬法uvcod一体机在线监测仪
Zhang et al. Assess the ability of detecting low concentration analyte with near-infrared spectroscopy based on dynamic enrichment
Ervin et al. Investigation of a robust flow-through Cu (I) optical sensor using 2, 9-dimethyl-4, 7-diphenyl-1, 10-phenanthroline immobilized into a Nafion film

Legal Events

Date Code Title Description
121 Ep: the epo has been informed by wipo that ep was designated in this application
WWE Wipo information: entry into national phase

Ref document number: 2006707256

Country of ref document: EP

WWE Wipo information: entry into national phase

Ref document number: 11817047

Country of ref document: US

Ref document number: 2007557391

Country of ref document: JP

NENP Non-entry into the national phase

Ref country code: DE

WWE Wipo information: entry into national phase

Ref document number: 2006218103

Country of ref document: AU

ENP Entry into the national phase

Ref document number: 2006218103

Country of ref document: AU

Date of ref document: 20060224

Kind code of ref document: A

WWP Wipo information: published in national office

Ref document number: 2006218103

Country of ref document: AU

WWP Wipo information: published in national office

Ref document number: 2006707256

Country of ref document: EP