WO2003068381A1 - Procede pour la production de nanogouttes monodispersees et dispositif pour l'execution de ce procede - Google Patents
Procede pour la production de nanogouttes monodispersees et dispositif pour l'execution de ce procede Download PDFInfo
- Publication number
- WO2003068381A1 WO2003068381A1 PCT/EP2003/001418 EP0301418W WO03068381A1 WO 2003068381 A1 WO2003068381 A1 WO 2003068381A1 EP 0301418 W EP0301418 W EP 0301418W WO 03068381 A1 WO03068381 A1 WO 03068381A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- fluid
- module
- microfluidic reactor
- focusing module
- fluids
- Prior art date
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/02—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/41—Emulsifying
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/41—Emulsifying
- B01F23/414—Emulsifying characterised by the internal structure of the emulsion
- B01F23/4143—Microemulsions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/30—Injector mixers
- B01F25/31—Injector mixers in conduits or tubes through which the main component flows
- B01F25/313—Injector mixers in conduits or tubes through which the main component flows wherein additional components are introduced in the centre of the conduit
- B01F25/3131—Injector mixers in conduits or tubes through which the main component flows wherein additional components are introduced in the centre of the conduit with additional mixing means other than injector mixers, e.g. screens, baffles or rotating elements
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/30—Injector mixers
- B01F25/31—Injector mixers in conduits or tubes through which the main component flows
- B01F25/313—Injector mixers in conduits or tubes through which the main component flows wherein additional components are introduced in the centre of the conduit
- B01F25/3132—Injector mixers in conduits or tubes through which the main component flows wherein additional components are introduced in the centre of the conduit by using two or more injector devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
- B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
- B01F25/43—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
- B01F25/433—Mixing tubes wherein the shape of the tube influences the mixing, e.g. mixing tubes with varying cross-section or provided with inwardly extending profiles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
- B01F25/45—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/05—Mixers using radiation, e.g. magnetic fields or microwaves to mix the material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/05—Mixers using radiation, e.g. magnetic fields or microwaves to mix the material
- B01F33/052—Mixers using radiation, e.g. magnetic fields or microwaves to mix the material the energy being electric fields for electrostatically charging of the ingredients or compositions for mixing them
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/05—Mixers using radiation, e.g. magnetic fields or microwaves to mix the material
- B01F33/053—Mixers using radiation, e.g. magnetic fields or microwaves to mix the material the energy being magnetic or electromagnetic energy, radiation working on the ingredients or compositions for or during mixing them
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/05—Mixers using radiation, e.g. magnetic fields or microwaves to mix the material
- B01F33/054—Mixers using radiation, e.g. magnetic fields or microwaves to mix the material the energy being in the form of a laser to modify the characteristics or conditions of the products, e.g. for heating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/30—Micromixers
- B01F33/301—Micromixers using specific means for arranging the streams to be mixed, e.g. channel geometries or dispositions
- B01F33/3011—Micromixers using specific means for arranging the streams to be mixed, e.g. channel geometries or dispositions using a sheathing stream of a fluid surrounding a central stream of a different fluid, e.g. for reducing the cross-section of the central stream or to produce droplets from the central stream
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/30—Micromixers
- B01F33/301—Micromixers using specific means for arranging the streams to be mixed, e.g. channel geometries or dispositions
- B01F33/3012—Interdigital streams, e.g. lamellae
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F35/94—Heating or cooling systems using radiation, e.g. microwaves or electromagnetic radiation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/04—Making microcapsules or microballoons by physical processes, e.g. drying, spraying
Abstract
L'invention concerne un procédé et un dispositif servant à produire des nanogouttes monodispersées. L'invention vise à obtenir une répartition de taille mieux contrôlable et une forme plus régulière des nanogouttes qu'avec les procédés et les dispositifs déjà connus. Le procédé selon l'invention pour la production de nanogouttes monodispersées est caractérisé en ce qu'on introduit dans un fluide A s'écoulant en continu un deuxième fluide B non miscible, en ce que le fluide B est entouré par le fluide A et en ce que la section d'écoulement (16, 25) du fluide B rétrécit dans le sens d'écoulement (2) de sorte que le fluide B se désagrège en gouttes individuelles (26) en raison de son instabilité hydrodynamique. L'invention concerne également un réacteur microfluidique pour l'exécution de ce procédé, dans lequel on introduit dans un premier flux continu d'un fluide A un deuxième flux d'un fluide B, le fluide B étant entouré par le fluide A et les fluides A et B n'étant pas miscibles. Le réacteur selon l'invention est caractérisé par un module de focalisation (1) comprenant une trémie d'entrée (3) rétrécissant dans le sens d'écoulement (2) et à l'extrémité (4) à petite ouverture de laquelle est raccordé un conduit de formation de gouttes (5).
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10206083A DE10206083B4 (de) | 2002-02-13 | 2002-02-13 | Verfahren zum Erzeugen monodisperser Nanotropfen sowie mikrofluidischer Reaktor zum Durchführen des Verfahrens |
DE10206083.5 | 2002-02-13 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2003068381A1 true WO2003068381A1 (fr) | 2003-08-21 |
Family
ID=27618679
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/EP2003/001418 WO2003068381A1 (fr) | 2002-02-13 | 2003-02-13 | Procede pour la production de nanogouttes monodispersees et dispositif pour l'execution de ce procede |
Country Status (2)
Country | Link |
---|---|
DE (1) | DE10206083B4 (fr) |
WO (1) | WO2003068381A1 (fr) |
Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1415708A3 (fr) * | 2002-11-01 | 2004-12-29 | Hitachi, Ltd. | Reacteur chimique et dispositif |
WO2006051153A2 (fr) * | 2004-11-09 | 2006-05-18 | Nanolab Systems Oy | Procedes et dispositifs pour simplifier la production de nanoparticules, et leurs applications |
US7307104B2 (en) | 2003-05-16 | 2007-12-11 | Velocys, Inc. | Process for forming an emulsion using microchannel process technology |
US7485671B2 (en) | 2003-05-16 | 2009-02-03 | Velocys, Inc. | Process for forming an emulsion using microchannel process technology |
US7556776B2 (en) | 2005-09-08 | 2009-07-07 | President And Fellows Of Harvard College | Microfluidic manipulation of fluids and reactions |
EP1913994A3 (fr) * | 2006-10-20 | 2009-12-02 | Hitachi Plant Technologies, Ltd. | Appareil d'émulsion et appareil de fabrication de grains fins |
US7816411B2 (en) | 2004-10-01 | 2010-10-19 | Velocys, Inc. | Multiphase mixing process using microchannel process technology |
US7943671B2 (en) | 2005-08-08 | 2011-05-17 | Max-Planck-Gesellschaft Zur Foerderung Der Wissenschaften E.V. | Formation of an emulsion in a fluid microsystem |
US9573099B2 (en) | 2011-05-23 | 2017-02-21 | President And Fellows Of Harvard College | Control of emulsions, including multiple emulsions |
US9664619B2 (en) | 2008-04-28 | 2017-05-30 | President And Fellows Of Harvard College | Microfluidic device for storage and well-defined arrangement of droplets |
US10195571B2 (en) | 2011-07-06 | 2019-02-05 | President And Fellows Of Harvard College | Multiple emulsions and techniques for the formation of multiple emulsions |
US10316873B2 (en) | 2005-03-04 | 2019-06-11 | President And Fellows Of Harvard College | Method and apparatus for forming multiple emulsions |
WO2020074721A1 (fr) | 2018-10-11 | 2020-04-16 | Emulco Laboratories C.V.B.A. | Procédé pour produire des émulsions et émulsion de polyisobutène aqueuse |
US10874997B2 (en) | 2009-09-02 | 2020-12-29 | President And Fellows Of Harvard College | Multiple emulsions created using jetting and other techniques |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP3930495B2 (ja) | 2004-06-16 | 2007-06-13 | 三菱重工業株式会社 | ニッケル超微粒子分散液体ナトリウムの製造方法、装置、液体ナトリウムの漏洩検出方法 |
JP4661942B2 (ja) * | 2008-05-13 | 2011-03-30 | ソニー株式会社 | マイクロチップとその流路構造 |
EP2827979A1 (fr) | 2012-03-22 | 2015-01-28 | Universiteit Twente | Appareil et procédé de production en masse d'un agent de microbulles monodispersées |
DE102012010959B4 (de) * | 2012-05-30 | 2019-03-28 | Technische Universität Dresden | Vorrichtung zur Bereitstellungkonstanter Strömungsverhältnisse vonunterschiedlichen Fluidphasen in Mikrokanalelementen |
DE102017105194A1 (de) | 2017-03-10 | 2018-09-13 | Little Things Factory Gmbh | Fokussiereinrichtung, Tropfengenerator und Verfahren zum Erzeugen einer Vielzahl von Tröpfchen |
Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
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FR1296788A (fr) * | 1961-04-28 | 1962-06-22 | Teerverwertung Gmbh | Procédé pour transformer en grenailles sphériques des matières fusibles, solides à la température ambiante |
US3329745A (en) * | 1965-10-05 | 1967-07-04 | Grange Lee D La | Process for making gelled spherical particles of oxides |
CH563807A5 (en) * | 1973-02-14 | 1975-07-15 | Battelle Memorial Institute | Fine granules and microcapsules mfrd. from liquid droplets - partic. of high viscosity requiring forced sepn. of droplets |
US3933679A (en) * | 1972-01-14 | 1976-01-20 | Gulf Oil Corporation | Uniform microspheroidal particle generating method |
US3962383A (en) * | 1972-10-03 | 1976-06-08 | Yoshiro Hagiwara | Method and apparatus for manufacturing seamless material-filled capsules |
US4251195A (en) * | 1975-12-26 | 1981-02-17 | Morishita Jinta Company, Limited | Apparatus for making miniature capsules |
US4422985A (en) * | 1982-09-24 | 1983-12-27 | Morishita Jintan Co., Ltd. | Method and apparatus for encapsulation of a liquid or meltable solid material |
WO1996011053A1 (fr) * | 1994-10-07 | 1996-04-18 | Warner-Lambert Company | Procede de fabrication de capsules sans soudure |
WO2000062913A1 (fr) * | 1999-04-16 | 2000-10-26 | INSTITUT FüR MIKROTECHNIK MAINZ GMBH | Procede et micromelangeur pour la realisation d'une dispersion |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4120613A1 (de) * | 1991-06-20 | 1992-03-05 | Suesse Harald | Selbstregulierender hochdrucktrennstrahlbeschleuniger |
US5344676A (en) * | 1992-10-23 | 1994-09-06 | The Board Of Trustees Of The University Of Illinois | Method and apparatus for producing nanodrops and nanoparticles and thin film deposits therefrom |
GB9318241D0 (en) * | 1993-09-02 | 1993-10-20 | Univ Mcgill | Distribution of fine bubbles or droplets in a fluid |
DE19510651A1 (de) * | 1994-06-03 | 1995-12-07 | Bayer Ag | Wäßrige 2-Komponenten-Polyurethanlack-Emulsionen und Verfahren zu deren Herstellung |
US6187214B1 (en) * | 1996-05-13 | 2001-02-13 | Universidad De Seville | Method and device for production of components for microfabrication |
DE10007816A1 (de) * | 2000-02-21 | 2001-09-06 | Bayer Ag | Verfahren zur Herstellung von Nanosuspensionen |
-
2002
- 2002-02-13 DE DE10206083A patent/DE10206083B4/de not_active Expired - Lifetime
-
2003
- 2003-02-13 WO PCT/EP2003/001418 patent/WO2003068381A1/fr not_active Application Discontinuation
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR1296788A (fr) * | 1961-04-28 | 1962-06-22 | Teerverwertung Gmbh | Procédé pour transformer en grenailles sphériques des matières fusibles, solides à la température ambiante |
US3329745A (en) * | 1965-10-05 | 1967-07-04 | Grange Lee D La | Process for making gelled spherical particles of oxides |
US3933679A (en) * | 1972-01-14 | 1976-01-20 | Gulf Oil Corporation | Uniform microspheroidal particle generating method |
US3962383A (en) * | 1972-10-03 | 1976-06-08 | Yoshiro Hagiwara | Method and apparatus for manufacturing seamless material-filled capsules |
CH563807A5 (en) * | 1973-02-14 | 1975-07-15 | Battelle Memorial Institute | Fine granules and microcapsules mfrd. from liquid droplets - partic. of high viscosity requiring forced sepn. of droplets |
US4251195A (en) * | 1975-12-26 | 1981-02-17 | Morishita Jinta Company, Limited | Apparatus for making miniature capsules |
US4422985A (en) * | 1982-09-24 | 1983-12-27 | Morishita Jintan Co., Ltd. | Method and apparatus for encapsulation of a liquid or meltable solid material |
WO1996011053A1 (fr) * | 1994-10-07 | 1996-04-18 | Warner-Lambert Company | Procede de fabrication de capsules sans soudure |
WO2000062913A1 (fr) * | 1999-04-16 | 2000-10-26 | INSTITUT FüR MIKROTECHNIK MAINZ GMBH | Procede et micromelangeur pour la realisation d'une dispersion |
Cited By (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7374726B2 (en) | 2002-11-01 | 2008-05-20 | Hitachi, Ltd. | Chemical reactor |
EP1415708A3 (fr) * | 2002-11-01 | 2004-12-29 | Hitachi, Ltd. | Reacteur chimique et dispositif |
US7485671B2 (en) | 2003-05-16 | 2009-02-03 | Velocys, Inc. | Process for forming an emulsion using microchannel process technology |
US7307104B2 (en) | 2003-05-16 | 2007-12-11 | Velocys, Inc. | Process for forming an emulsion using microchannel process technology |
US7816411B2 (en) | 2004-10-01 | 2010-10-19 | Velocys, Inc. | Multiphase mixing process using microchannel process technology |
WO2006051153A3 (fr) * | 2004-11-09 | 2006-06-29 | Nanolab Systems Oy | Procedes et dispositifs pour simplifier la production de nanoparticules, et leurs applications |
WO2006051153A2 (fr) * | 2004-11-09 | 2006-05-18 | Nanolab Systems Oy | Procedes et dispositifs pour simplifier la production de nanoparticules, et leurs applications |
US10316873B2 (en) | 2005-03-04 | 2019-06-11 | President And Fellows Of Harvard College | Method and apparatus for forming multiple emulsions |
US7943671B2 (en) | 2005-08-08 | 2011-05-17 | Max-Planck-Gesellschaft Zur Foerderung Der Wissenschaften E.V. | Formation of an emulsion in a fluid microsystem |
US7556776B2 (en) | 2005-09-08 | 2009-07-07 | President And Fellows Of Harvard College | Microfluidic manipulation of fluids and reactions |
EP1913994A3 (fr) * | 2006-10-20 | 2009-12-02 | Hitachi Plant Technologies, Ltd. | Appareil d'émulsion et appareil de fabrication de grains fins |
US9664619B2 (en) | 2008-04-28 | 2017-05-30 | President And Fellows Of Harvard College | Microfluidic device for storage and well-defined arrangement of droplets |
US10828641B2 (en) | 2008-04-28 | 2020-11-10 | President And Fellows Of Harvard College | Microfluidic device for storage and well-defined arrangement of droplets |
US11498072B2 (en) | 2008-04-28 | 2022-11-15 | President And Fellows Of Harvard College | Microfluidic device for storage and well-defined arrangement of droplets |
US10874997B2 (en) | 2009-09-02 | 2020-12-29 | President And Fellows Of Harvard College | Multiple emulsions created using jetting and other techniques |
US9573099B2 (en) | 2011-05-23 | 2017-02-21 | President And Fellows Of Harvard College | Control of emulsions, including multiple emulsions |
US10195571B2 (en) | 2011-07-06 | 2019-02-05 | President And Fellows Of Harvard College | Multiple emulsions and techniques for the formation of multiple emulsions |
WO2020074721A1 (fr) | 2018-10-11 | 2020-04-16 | Emulco Laboratories C.V.B.A. | Procédé pour produire des émulsions et émulsion de polyisobutène aqueuse |
EP3646941A2 (fr) | 2018-10-11 | 2020-05-06 | Emulco Laboratories C.V.B.A. | Procédé de production d'émulsions et émulsion aqueuse de polyisobutène |
Also Published As
Publication number | Publication date |
---|---|
DE10206083A1 (de) | 2003-08-21 |
DE10206083B4 (de) | 2009-11-26 |
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