WO2003002246A1 - Dispositif et procede optimisant la circulation d'une suspension dans une installation comprenant un reacteur triphasique - Google Patents

Dispositif et procede optimisant la circulation d'une suspension dans une installation comprenant un reacteur triphasique Download PDF

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Publication number
WO2003002246A1
WO2003002246A1 PCT/FR2002/001919 FR0201919W WO03002246A1 WO 2003002246 A1 WO2003002246 A1 WO 2003002246A1 FR 0201919 W FR0201919 W FR 0201919W WO 03002246 A1 WO03002246 A1 WO 03002246A1
Authority
WO
WIPO (PCT)
Prior art keywords
slurry
circuit
plant
circulation
suspension
Prior art date
Application number
PCT/FR2002/001919
Other languages
English (en)
Other versions
WO2003002246A9 (fr
Inventor
Jean-Marc Schweitzer
Eric Lenglet
Franck Gaviot-Blanc
Original Assignee
Institut Francais Du Petrole
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Institut Francais Du Petrole filed Critical Institut Francais Du Petrole
Priority to US10/481,818 priority Critical patent/US7125524B2/en
Publication of WO2003002246A1 publication Critical patent/WO2003002246A1/fr
Publication of WO2003002246A9 publication Critical patent/WO2003002246A9/fr
Priority to US11/483,778 priority patent/US7560495B2/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2/00—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon
    • C10G2/30—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen
    • C10G2/32—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts
    • C10G2/34—Apparatus, reactors
    • C10G2/342—Apparatus, reactors with moving solid catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
    • B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
    • B01J8/224—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid the particles being subject to a circulatory movement
    • B01J8/228—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid the particles being subject to a circulatory movement externally, i.e. the particles leaving the vessel and subsequently re-entering it
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00256—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles in a heat exchanger for the heat exchange medium separate from the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00265—Part of all of the reactants being heated or cooled outside the reactor while recycling
    • B01J2208/00292—Part of all of the reactants being heated or cooled outside the reactor while recycling involving reactant solids
    • B01J2208/003—Part of all of the reactants being heated or cooled outside the reactor while recycling involving reactant solids involving reactant slurries
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00539—Pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00548—Flow
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00245—Avoiding undesirable reactions or side-effects
    • B01J2219/00247—Fouling of the reactor or the process equipment

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Combustion & Propulsion (AREA)
  • General Chemical & Material Sciences (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Installation de conversion chimique d'une charge, comprenant un réacteur (2) contenant un slurry constitué au moins d'une suspension d'au moins un solide dans un liquide, une alimentation de gaz, un circuit, externe au réacteur, de circulation continue d'un courant de slurry, ledit slurry étant soutiré en au moins un point (A) et réintroduit au moins en partie in au moins un autre point (B), une section de séparation d'au moins un fluide du slurry traversant ledit circuit externe, ladite installation comprenant en outre: - des moyens permettant l'arrêt de la circulation dudit slurry dans ledit circuit; - des moyens d'introduction sous pression d'au moins un fluide de vidange du slurry contenu dans le circuit; - des moyens permettant la circulation du slurry dans ledit circuit externe dans des conditions telles que le nombre de Reynolds soit supérieur à 2500.
PCT/FR2002/001919 2001-06-25 2002-06-05 Dispositif et procede optimisant la circulation d'une suspension dans une installation comprenant un reacteur triphasique WO2003002246A1 (fr)

Priority Applications (2)

Application Number Priority Date Filing Date Title
US10/481,818 US7125524B2 (en) 2001-06-25 2002-06-05 Device and method for optimising the circulation of a suspension in a plant comprising a three-phase reactor
US11/483,778 US7560495B2 (en) 2001-06-25 2006-07-11 Apparatus and process for optimising the circulation of a suspension in a facility comprising a three-phase reactor

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR0108442A FR2826295B1 (fr) 2001-06-25 2001-06-25 Dispositif et procede optimisant la circulation d'une suspension dans une installation comprenant un reacteur triphasique
FR01/08442 2001-06-25

Related Child Applications (2)

Application Number Title Priority Date Filing Date
US10481818 A-371-Of-International 2002-06-05
US11/483,778 Division US7560495B2 (en) 2001-06-25 2006-07-11 Apparatus and process for optimising the circulation of a suspension in a facility comprising a three-phase reactor

Publications (2)

Publication Number Publication Date
WO2003002246A1 true WO2003002246A1 (fr) 2003-01-09
WO2003002246A9 WO2003002246A9 (fr) 2005-11-03

Family

ID=8864806

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/FR2002/001919 WO2003002246A1 (fr) 2001-06-25 2002-06-05 Dispositif et procede optimisant la circulation d'une suspension dans une installation comprenant un reacteur triphasique

Country Status (3)

Country Link
US (2) US7125524B2 (fr)
FR (1) FR2826295B1 (fr)
WO (1) WO2003002246A1 (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107537407A (zh) * 2017-09-28 2018-01-05 河南神马尼龙化工有限责任公司 己二腈加氢反应系统及该系统处理反应器重度堵塞的方法

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU2008304801B2 (en) * 2007-09-27 2011-03-24 Cosmo Oil Co., Ltd. Bubbling tower hydrocarbon reactor and method of detecting slurry surface level
CA2700126C (fr) * 2007-09-27 2014-02-18 Japan Oil, Gas And Metals National Corporation Systeme de reaction de synthese
CA2718077C (fr) 2008-03-14 2014-04-15 Cosmo Oil Co., Ltd. Systeme reactionnel de synthese pour des composes hydreocarbones et procede d'extraction des particules catalytiques pulverisees
US8119014B2 (en) * 2008-12-23 2012-02-21 Exxonmobil Research And Engineering Company Systems and methods to remove liquid product and fines from a slurry reactor
JP5501706B2 (ja) 2009-09-16 2014-05-28 独立行政法人石油天然ガス・金属鉱物資源機構 炭化水素の製造方法及び合成反応システム
US9023195B2 (en) 2009-11-06 2015-05-05 Japan Oil, Gas And Metals National Corporation Process for hydrotreating naphtha fraction and process for producing hydrocarbon oil
JP5675146B2 (ja) * 2010-03-30 2015-02-25 独立行政法人石油天然ガス・金属鉱物資源機構 炭化水素の製造方法
JP5730495B2 (ja) 2010-03-30 2015-06-10 独立行政法人石油天然ガス・金属鉱物資源機構 フィッシャー・トロプシュ合成反応用活性化触媒の製造方法、触媒スラリーの製造方法、並びに触媒スラリーのフィッシャー・トロプッシュ合成反応器への供給方法
JP5757704B2 (ja) 2010-08-19 2015-07-29 独立行政法人石油天然ガス・金属鉱物資源機構 炭化水素油の製造方法及び炭化水素油の製造システム
JP5764307B2 (ja) 2010-08-19 2015-08-19 独立行政法人石油天然ガス・金属鉱物資源機構 炭化水素油の製造方法及び炭化水素油の製造システム
JP5808559B2 (ja) 2011-03-31 2015-11-10 独立行政法人石油天然ガス・金属鉱物資源機構 炭化水素油の製造方法、フィッシャー・トロプシュ合成反応装置及び炭化水素油の製造システム
FR3044565B1 (fr) * 2015-12-08 2017-12-01 Ifp Energies Now Chargement d'un catalyseur dans une colonne a bulles pour la synthese fischer-tropsch
CN108854859B (zh) * 2018-07-27 2023-08-18 中化蓝天霍尼韦尔新材料有限公司 一种悬浮液气液相反应装置及运行方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1038608A (fr) * 1950-03-10 1953-09-30 Bataafsche Petroleum Dispositif de réglage de la circulation des solides fluidifiés
US3546296A (en) * 1966-03-10 1970-12-08 Melle Bezons Continuous process for reducing aromatic nitro compounds to aromatic amines
EP0952132A1 (fr) * 1998-04-23 1999-10-27 AGIP PETROLI S.p.A. Procédé pour la synthèse d'hydrocarbures à partir de gaz de synthèse

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5900159A (en) * 1996-02-29 1999-05-04 Shell Oil Company Method for separating liquid from a slurry
US5770629A (en) * 1997-05-16 1998-06-23 Exxon Research & Engineering Company Slurry hydrocarbon synthesis with external product filtration

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1038608A (fr) * 1950-03-10 1953-09-30 Bataafsche Petroleum Dispositif de réglage de la circulation des solides fluidifiés
US3546296A (en) * 1966-03-10 1970-12-08 Melle Bezons Continuous process for reducing aromatic nitro compounds to aromatic amines
EP0952132A1 (fr) * 1998-04-23 1999-10-27 AGIP PETROLI S.p.A. Procédé pour la synthèse d'hydrocarbures à partir de gaz de synthèse

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107537407A (zh) * 2017-09-28 2018-01-05 河南神马尼龙化工有限责任公司 己二腈加氢反应系统及该系统处理反应器重度堵塞的方法
CN107537407B (zh) * 2017-09-28 2020-09-22 河南神马尼龙化工有限责任公司 己二腈加氢反应系统及该系统处理反应器重度堵塞的方法

Also Published As

Publication number Publication date
FR2826295A1 (fr) 2002-12-27
US7560495B2 (en) 2009-07-14
WO2003002246A9 (fr) 2005-11-03
FR2826295B1 (fr) 2003-09-26
US20070014703A1 (en) 2007-01-18
US7125524B2 (en) 2006-10-24
US20040258579A1 (en) 2004-12-23

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