WO2002069726A2 - Milchprodukt und verfahren zu seiner herstellung - Google Patents
Milchprodukt und verfahren zu seiner herstellung Download PDFInfo
- Publication number
- WO2002069726A2 WO2002069726A2 PCT/AT2002/000066 AT0200066W WO02069726A2 WO 2002069726 A2 WO2002069726 A2 WO 2002069726A2 AT 0200066 W AT0200066 W AT 0200066W WO 02069726 A2 WO02069726 A2 WO 02069726A2
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- gelling agent
- milk product
- milk
- product according
- cream
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 15
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- 235000013365 dairy product Nutrition 0.000 title abstract 2
- 239000003349 gelling agent Substances 0.000 claims abstract description 39
- 239000006071 cream Substances 0.000 claims abstract description 18
- FHVDTGUDJYJELY-UHFFFAOYSA-N 6-{[2-carboxy-4,5-dihydroxy-6-(phosphanyloxy)oxan-3-yl]oxy}-4,5-dihydroxy-3-phosphanyloxane-2-carboxylic acid Chemical compound O1C(C(O)=O)C(P)C(O)C(O)C1OC1C(C(O)=O)OC(OP)C(O)C1O FHVDTGUDJYJELY-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229940072056 alginate Drugs 0.000 claims abstract description 9
- 235000010443 alginic acid Nutrition 0.000 claims abstract description 9
- 229920000615 alginic acid Polymers 0.000 claims abstract description 9
- 239000001913 cellulose Substances 0.000 claims abstract description 9
- 229920002678 cellulose Polymers 0.000 claims abstract description 9
- 229920002752 Konjac Polymers 0.000 claims abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 230000002441 reversible effect Effects 0.000 claims abstract description 6
- 239000000416 hydrocolloid Substances 0.000 claims abstract description 3
- 235000013336 milk Nutrition 0.000 claims description 40
- 239000008267 milk Substances 0.000 claims description 40
- 210000004080 milk Anatomy 0.000 claims description 40
- 239000000203 mixture Substances 0.000 claims description 24
- 235000020183 skimmed milk Nutrition 0.000 claims description 22
- 239000000679 carrageenan Substances 0.000 claims description 13
- 229920001525 carrageenan Polymers 0.000 claims description 12
- 229940113118 carrageenan Drugs 0.000 claims description 12
- 235000010418 carrageenan Nutrition 0.000 claims description 11
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 10
- 239000004615 ingredient Substances 0.000 claims description 9
- 235000010980 cellulose Nutrition 0.000 claims description 8
- 239000000084 colloidal system Substances 0.000 claims description 7
- 241001312219 Amorphophallus konjac Species 0.000 claims description 6
- 235000001206 Amorphophallus rivieri Nutrition 0.000 claims description 6
- 235000013312 flour Nutrition 0.000 claims description 6
- 239000000252 konjac Substances 0.000 claims description 6
- 235000010485 konjac Nutrition 0.000 claims description 6
- 238000004806 packaging method and process Methods 0.000 claims description 5
- 239000001814 pectin Substances 0.000 claims description 5
- 235000010987 pectin Nutrition 0.000 claims description 5
- 235000013311 vegetables Nutrition 0.000 claims description 5
- 238000000265 homogenisation Methods 0.000 claims description 4
- 229920001277 pectin Polymers 0.000 claims description 4
- 229910052708 sodium Inorganic materials 0.000 claims description 4
- 239000011734 sodium Substances 0.000 claims description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- ZNOZWUKQPJXOIG-XSBHQQIPSA-L [(2r,3s,4r,5r,6s)-6-[[(1r,3s,4r,5r,8s)-3,4-dihydroxy-2,6-dioxabicyclo[3.2.1]octan-8-yl]oxy]-4-[[(1r,3r,4r,5r,8s)-8-[(2s,3r,4r,5r,6r)-3,4-dihydroxy-6-(hydroxymethyl)-5-sulfonatooxyoxan-2-yl]oxy-4-hydroxy-2,6-dioxabicyclo[3.2.1]octan-3-yl]oxy]-5-hydroxy-2-( Chemical compound O[C@@H]1[C@@H](O)[C@@H](OS([O-])(=O)=O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H]2OC[C@H]1O[C@H](O[C@H]1[C@H]([C@@H](CO)O[C@@H](O[C@@H]3[C@@H]4OC[C@H]3O[C@H](O)[C@@H]4O)[C@@H]1O)OS([O-])(=O)=O)[C@@H]2O ZNOZWUKQPJXOIG-XSBHQQIPSA-L 0.000 claims description 2
- 230000002378 acidificating effect Effects 0.000 claims description 2
- 235000020121 low-fat milk Nutrition 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- -1 preferably carragen Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 description 27
- 239000000499 gel Substances 0.000 description 6
- 229920000159 gelatin Polymers 0.000 description 4
- 235000019322 gelatine Nutrition 0.000 description 4
- 108010010803 Gelatin Proteins 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 230000002349 favourable effect Effects 0.000 description 3
- 239000008273 gelatin Substances 0.000 description 3
- 235000011852 gelatine desserts Nutrition 0.000 description 3
- 239000011265 semifinished product Substances 0.000 description 3
- 241000283690 Bos taurus Species 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000001768 carboxy methyl cellulose Substances 0.000 description 2
- 235000010948 carboxy methyl cellulose Nutrition 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 238000005189 flocculation Methods 0.000 description 2
- 230000016615 flocculation Effects 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 238000005204 segregation Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 229920002134 Carboxymethyl cellulose Polymers 0.000 description 1
- 241000755093 Gaidropsarus vulgaris Species 0.000 description 1
- 239000001828 Gelatine Substances 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 235000015278 beef Nutrition 0.000 description 1
- 239000008112 carboxymethyl-cellulose Substances 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 239000000661 sodium alginate Substances 0.000 description 1
- 235000010413 sodium alginate Nutrition 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L sulfate group Chemical group S(=O)(=O)([O-])[O-] QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
- 238000010257 thawing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C13/00—Cream; Cream preparations; Making thereof
- A23C13/12—Cream preparations
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/152—Milk preparations; Milk powder or milk powder preparations containing additives
- A23C9/154—Milk preparations; Milk powder or milk powder preparations containing additives containing thickening substances, eggs or cereal preparations; Milk gels
- A23C9/1544—Non-acidified gels, e.g. custards, creams, desserts, puddings, shakes or foams, containing eggs or thickening or gelling agents other than sugar; Milk products containing natural or microbial polysaccharides, e.g. cellulose or cellulose derivatives; Milk products containing nutrient fibres
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Definitions
- the invention relates to a milk product which consists essentially, preferably exclusively, of cream, skimmed milk or water, and gelling agents.
- the invention further relates to several methods for producing the milk product according to the invention.
- An object of the invention is to provide a novel milk product which has the same properties as the milk products produced according to the prior art, but avoids the use of gelatin produced from bovine split.
- the gelling agent only comprises vegetable raw materials, preferably vegetable hydrocolloids.
- the advantage of this novel milk product is therefore primarily that it is possible to dispense entirely with the use of gelatin, which is produced from animal products, but this novel milk product has the same properties as the conventional milk products made with gelatin , ie is structure reversible.
- structure-reversible means that the finished milk product has a gel structure which, when it has been destroyed by shear forces, such as, for example, when stirring with a whisk or in a mixer, is formed again. This is important insofar as it is only through this property that the novel milk product can be used as a semi-finished product.
- the novel milk product remains structurally reversible even when the pH is below 5 (ph ⁇ 5), for example by adding acidic components, ie it is acid-stable.
- the novel milk product has, because of these two properties, namely the structural reversibility and the acid stability, a further property which is important for use as a semi-finished product, namely that it is or remains temperature stable.
- the previously known products had no freeze and thaw stability due to their non-reversible gel structure and due to the fact that they clot when acid or shear forces are added, which is why the use of such milk products as a semi-finished product was not possible.
- the gelling agent is a mixture of carrageenan, cellulose and pectin. Due to the negatively charged sulfate groups, the carrageenan can react with the proteins of the skim milk. In order to avoid the coagulation of the carrageenan below a pH of 4.8, cellulose, preferably physically or chemically treated lota and / or kappa cellulose, is used as a protective colloid. Thus, a gel structure can build up, which is freeze / thaw stable and which behaves the same after thawing as before freezing. To improve the new formation of the gel structure after destruction by shear forces when cold, pectin or konjac flour is used. Sodium casinate can also be added to the gelling agent as a buffer.
- the gelling agent additionally comprises alginate. It is only through the use of alginate that it is possible for the oil to form a connection with the milk product when it is stirred in, i.e. that the oil does not separate from the milk product again.
- this novel milk product is to be specified. It has proven to be particularly favorable for the mixing of the gelling agent with the skim milk and thus for the formation of a gel structure if the powdered gelling agent is stirred into skim milk or water in a mixing tank, the skim milk or the water having a temperature between 3 and 10 ° C, preferably between 5 and 7 ° C, this mixture is then allowed to swell and then mixed with the remaining ingredients.
- the vegetable raw materials that form the gelling agent are particularly good when the fat content of the skimmed milk is below 0.3%, preferably below 0.1%.
- the novel milk product has a preferred fat content of about 15%, it is provided according to a further embodiment that the fat portion of the cream used is about 36%.
- the pH of the mixture of all ingredients is between 6.5-7.5, preferably 6.7, means that the end product is tasteless.
- the filling temperature of the mixture containing at least cream and skimmed milk-containing gelling agent is between 30 ° C and 60 ° C, whereby it has been found that segregation or flocculation of the gelling agent can be avoided if the milk product after the Filling quickly to a temperature below 25 ° C, preferably below 15 ° C, is cooled.
- Another process for the production of this novel milk product is characterized in that all the ingredients are introduced into a colloid mill, preferably a tooth colloid mill, mixed there and this mixture is then left to swell.
- This method also uses skimmed milk with a fat content preferably below 0.1%, and cream with a fat content of about 36%.
- the pH of the mixture of all ingredients is between 6.5 - 7.5, preferably 6.7%.
- the homogenization takes place at a temperature of about 100 ° C. and a pressure between 4 and 7 bar, preferably between 5 and 6 bar.
- a temperature of about 100 ° C. and a pressure between 4 and 7 bar, preferably between 5 and 6 bar.
- FIG. 1 shows a schematic representation of a process sequence according to the invention
- FIG. 2 shows the approximate temperature profile during the individual process steps according to FIG. 1.
- skimmed milk 1 is introduced into a toothed colloid mill 4, for example of the Fryma Koruma Delemix type, via a funnel 5 and gelling agent 2 via a funnel 5 '.
- Gelling agent 2 is a mixture of Iota carrageenan (E 407), carboxymethyl cellulose (E 466), pectin type C-1828 (E 440) and NA alginate (E 401).
- the gelling agent is made exclusively from carrageenan, cellulose, konjac flour and alginate, the carrageenan being a mixture of lota-carrageenan and kappa-carrageenan.
- the gelling agent is composed of 22% Iota and Kappa Carragenan, 26% Cellulose, 26% Konjac Flour and 26% Na Alginate.
- Na-casinate can be added to the gelling agent as a buffer, the proportion of Na-casinate in the gelling agent being approximately 10.5%.
- step II the skimmed milk 1 is mixed with the gelling agent 2 at about 5 to 7 ° C. and left to swell for about 5 to 10 minutes with gentle stirring.
- step III is added to this mixture via an intake 6 cream 3 with a temperature of about 5 ° C.
- this mixture which has a temperature between 5 and 7 ° C. and a fat content of about 15%, is at 100 ° C. in step IV for about three minutes heated and then homogenized in step V at about 100 ° C and a pressure of about 5 to 6 bar in the sterile area.
- This mixture is then filled into the packaging 7 in step VI and stored in pallets 8.
- these pallets 8 are rapidly cooled in the cold store 9 to a temperature below 25 ° C., preferably 15 ° C., and stored there at 5 to 6 ° C. for about 7 to 10 days.
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Dispersion Chemistry (AREA)
- Dairy Products (AREA)
- Jellies, Jams, And Syrups (AREA)
Abstract
Description
Claims
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2002568920A JP2004518445A (ja) | 2001-03-05 | 2002-03-05 | 乳製品とその製造方法 |
EP02700007A EP1408764A2 (de) | 2001-03-05 | 2002-03-05 | Milchprodukt und verfahren zu seiner herstellung |
US10/655,885 US20040047965A1 (en) | 2001-03-05 | 2003-09-05 | Milk product and process for its prouduction |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ATA340/2001 | 2001-03-05 | ||
AT0034001A ATA3402001A (de) | 2001-03-05 | 2001-03-05 | Milchprodukt und verfahren zu seiner herstellung |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US10/655,885 Continuation US20040047965A1 (en) | 2001-03-05 | 2003-09-05 | Milk product and process for its prouduction |
Publications (2)
Publication Number | Publication Date |
---|---|
WO2002069726A2 true WO2002069726A2 (de) | 2002-09-12 |
WO2002069726A3 WO2002069726A3 (de) | 2003-11-06 |
Family
ID=3672107
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/AT2002/000066 WO2002069726A2 (de) | 2001-03-05 | 2002-03-05 | Milchprodukt und verfahren zu seiner herstellung |
Country Status (3)
Country | Link |
---|---|
JP (1) | JP2004518445A (de) |
AT (1) | ATA3402001A (de) |
WO (1) | WO2002069726A2 (de) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2004105512A1 (en) * | 2003-05-27 | 2004-12-09 | Unilever N.V. | Method for preparing a gelled food product |
EP2338352A1 (de) * | 2009-12-22 | 2011-06-29 | Corporacion Alimentaria Penasanta, S.A. | Butter und Verfahren zu deren Herstellung |
Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2211678A (en) * | 1939-06-05 | 1940-08-13 | William R Voss | Fresh ingredient base for food products |
DE2600028A1 (de) * | 1976-01-02 | 1977-07-14 | Molkerei Zentrale Westfalen | Verfahren zur herstellung eines halbfettes auf milchfettbasis und halbfett auf milchfettbasis |
US4631196A (en) * | 1985-04-15 | 1986-12-23 | Zeller Clifford L | Low calorie dairy product |
US4874627A (en) * | 1988-06-14 | 1989-10-17 | Nouevelle Ice Cream Corporation | Non-fat dairy compositions |
EP0616774A1 (de) * | 1993-03-24 | 1994-09-28 | Soremartec S.A. | Verfahren zur Herstellung eines flüssigen Nahrungsmittelproduktes |
WO1997025874A1 (de) * | 1996-01-18 | 1997-07-24 | Zott Gmbh & Co. | Pastöse nahrungsprodukte auf milchbasis |
US5789004A (en) * | 1995-12-15 | 1998-08-04 | Fmc Corporation | Coprocessed microcrystalline cellulose stabilizer compositions, foods containing the same and stabilization method |
EP0930017A1 (de) * | 1996-08-27 | 1999-07-21 | San-Ei Gen F.F.I., Inc. | Neue verwendung von natuerlichem gellangummi |
WO2000036930A1 (en) * | 1998-12-18 | 2000-06-29 | Cp Kelco U.S., Inc. | Gelatin replacement composition |
-
2001
- 2001-03-05 AT AT0034001A patent/ATA3402001A/de not_active Application Discontinuation
-
2002
- 2002-03-05 JP JP2002568920A patent/JP2004518445A/ja active Pending
- 2002-03-05 WO PCT/AT2002/000066 patent/WO2002069726A2/de not_active Application Discontinuation
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2211678A (en) * | 1939-06-05 | 1940-08-13 | William R Voss | Fresh ingredient base for food products |
DE2600028A1 (de) * | 1976-01-02 | 1977-07-14 | Molkerei Zentrale Westfalen | Verfahren zur herstellung eines halbfettes auf milchfettbasis und halbfett auf milchfettbasis |
US4631196A (en) * | 1985-04-15 | 1986-12-23 | Zeller Clifford L | Low calorie dairy product |
US4874627A (en) * | 1988-06-14 | 1989-10-17 | Nouevelle Ice Cream Corporation | Non-fat dairy compositions |
EP0616774A1 (de) * | 1993-03-24 | 1994-09-28 | Soremartec S.A. | Verfahren zur Herstellung eines flüssigen Nahrungsmittelproduktes |
US5789004A (en) * | 1995-12-15 | 1998-08-04 | Fmc Corporation | Coprocessed microcrystalline cellulose stabilizer compositions, foods containing the same and stabilization method |
WO1997025874A1 (de) * | 1996-01-18 | 1997-07-24 | Zott Gmbh & Co. | Pastöse nahrungsprodukte auf milchbasis |
EP0930017A1 (de) * | 1996-08-27 | 1999-07-21 | San-Ei Gen F.F.I., Inc. | Neue verwendung von natuerlichem gellangummi |
WO2000036930A1 (en) * | 1998-12-18 | 2000-06-29 | Cp Kelco U.S., Inc. | Gelatin replacement composition |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2004105512A1 (en) * | 2003-05-27 | 2004-12-09 | Unilever N.V. | Method for preparing a gelled food product |
WO2004105509A1 (en) * | 2003-05-27 | 2004-12-09 | Unilever N.V. | A semi-finished food product |
EP1502510A1 (de) * | 2003-05-27 | 2005-02-02 | Unilever N.V. | Methode zur Herstellung eines gelierten Lebensmittelproduktes |
CN100349527C (zh) * | 2003-05-27 | 2007-11-21 | 荷兰联合利华有限公司 | 制备胶态食品的方法 |
EP2338352A1 (de) * | 2009-12-22 | 2011-06-29 | Corporacion Alimentaria Penasanta, S.A. | Butter und Verfahren zu deren Herstellung |
Also Published As
Publication number | Publication date |
---|---|
WO2002069726A3 (de) | 2003-11-06 |
JP2004518445A (ja) | 2004-06-24 |
ATA3402001A (de) | 2006-01-15 |
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