WO2002012175A3 - Verfahren zur herstellung von hydrolysestabilen ammoniumnitrilen - Google Patents

Verfahren zur herstellung von hydrolysestabilen ammoniumnitrilen Download PDF

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Publication number
WO2002012175A3
WO2002012175A3 PCT/EP2001/008883 EP0108883W WO0212175A3 WO 2002012175 A3 WO2002012175 A3 WO 2002012175A3 EP 0108883 W EP0108883 W EP 0108883W WO 0212175 A3 WO0212175 A3 WO 0212175A3
Authority
WO
WIPO (PCT)
Prior art keywords
alkyl
hydrogen
phenyl
alkoxy
alkenyl
Prior art date
Application number
PCT/EP2001/008883
Other languages
English (en)
French (fr)
Other versions
WO2002012175A2 (de
Inventor
Manfred Schreiber
Georg Borchers
Oliver Mogck
Frank Weinelt
Original Assignee
Clariant Gmbh
Manfred Schreiber
Georg Borchers
Oliver Mogck
Frank Weinelt
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Clariant Gmbh, Manfred Schreiber, Georg Borchers, Oliver Mogck, Frank Weinelt filed Critical Clariant Gmbh
Priority to JP2002518153A priority Critical patent/JP2004505946A/ja
Priority to BR0112869-8A priority patent/BR0112869A/pt
Priority to US10/343,495 priority patent/US7005534B2/en
Priority to DE50109972T priority patent/DE50109972D1/de
Priority to EP01971836A priority patent/EP1309542B1/de
Publication of WO2002012175A2 publication Critical patent/WO2002012175A2/de
Publication of WO2002012175A3 publication Critical patent/WO2002012175A3/de

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/39—Organic or inorganic per-compounds
    • C11D3/3902—Organic or inorganic per-compounds combined with specific additives
    • C11D3/3905—Bleach activators or bleach catalysts
    • C11D3/3907—Organic compounds
    • C11D3/3917—Nitrogen-containing compounds
    • C11D3/3925—Nitriles; Isocyanates or quarternary ammonium nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/32—Separation; Purification; Stabilisation; Use of additives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Detergent Compositions (AREA)

Abstract

Gegenstand der Erfindung ist ein Verfahren zur Herstellung von hydrolysestabilen Ammoniumnitrilen durch Umsetzung einer Verbindung der Formel (1), worin R?1, R2, R3¿ gleich oder verschieden sind, und für lineare oder verzweigte C¿1?-C24-Alkylgruppen, C2-C24-Alkenylgruppen, substituiert oder unsubstituiertes Benzyl oder für C1-C4-Alkoxy-C1-C4-Alkylgruppen stehen, oder worin R?1 und R2¿ zusammen mit dem Stickstoffatom, an das sie gebunden sind, einen Ring mit 4 bis 6 C-Atomen bilden, der mit C¿1?-C5-Alkyl, C1-C5-Alkoxy, C1-C5-Alkanoyl, Phenyl, Amino, Ammonium, Cyano, Cyanamino, Chlor oder Brom substituiert sein kann und zusätzlich zum Stickstoffatom anstelle von Kohlenstoffatomen ein oder zwei Sauerstoff- oder Stickstoffatome, eine Gruppe N-R?6¿ oder eine Gruppe R3-N-R6 enthalten kann, worin R6 Wasserstoff, C¿1?-C5-Alkyl, C2-C5-Alkenyl, C2-C5-Alkinyl, Phenyl, C7-C9-Aralkyl, C5-C7-Cycloalkyl, C1-C6-Alkanoyl, Cyanomethyl oder Cyan ist, R?4 und R5¿ Wasserstoff, C¿1?-C4-Alkyl, C1-C4-Alkenyl, C1-C4-Alkoxy-C1-C4-alkyl, Phenyl oder C1-C3-Alkylphenyl, vorzugsweise Wasserstoff, Methyl oder Phenyl sind, wobei insbesondere R?4¿ Wasserstoff bedeutet, wenn R5 keinen Wasserstoff bedeutet, und X für ein Anion steht, mit einem Alkali- oder Ammoniumsalz eines Alkansulfonats, Paraffinsulfonats, Arylsulfonats, Alkoholsulfats oder Fettsäurealkylcarboxylats in Gegenwart von Wasser bei erhöhter Temperatur.
PCT/EP2001/008883 2000-08-04 2001-08-01 Verfahren zur herstellung von hydrolysestabilen ammoniumnitrilen WO2002012175A2 (de)

Priority Applications (5)

Application Number Priority Date Filing Date Title
JP2002518153A JP2004505946A (ja) 2000-08-04 2001-08-01 加水分解安定性アンモニウムニトリルを製造する方法
BR0112869-8A BR0112869A (pt) 2000-08-04 2001-08-01 Processo para preparação de nitrilas de amÈnio estáveis à hidrólise
US10/343,495 US7005534B2 (en) 2000-08-04 2001-08-01 Method for producing hydrolysis-stable ammonium nitriles
DE50109972T DE50109972D1 (de) 2000-08-04 2001-08-01 Verfahren zur herstellung von hydrolysestabilen ammoniumnitrilen
EP01971836A EP1309542B1 (de) 2000-08-04 2001-08-01 Verfahren zur herstellung von hydrolysestabilen ammoniumnitrilen

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10038086A DE10038086A1 (de) 2000-08-04 2000-08-04 Verfahren zur Herstellung von hydrolysestabilen Ammoniumnitrilen
DE10038086.7 2000-08-04

Publications (2)

Publication Number Publication Date
WO2002012175A2 WO2002012175A2 (de) 2002-02-14
WO2002012175A3 true WO2002012175A3 (de) 2002-04-11

Family

ID=7651325

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2001/008883 WO2002012175A2 (de) 2000-08-04 2001-08-01 Verfahren zur herstellung von hydrolysestabilen ammoniumnitrilen

Country Status (7)

Country Link
US (1) US7005534B2 (de)
EP (1) EP1309542B1 (de)
JP (1) JP2004505946A (de)
BR (1) BR0112869A (de)
DE (2) DE10038086A1 (de)
ES (1) ES2265441T3 (de)
WO (1) WO2002012175A2 (de)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10159386A1 (de) * 2001-12-04 2003-06-12 Henkel Kgaa Verfahren zur Herstellung von Bleichaktivatorgranulaten
DE10159388A1 (de) * 2001-12-04 2003-06-12 Henkel Kgaa Verfahren zur Herstellung von umhüllten Bleichaktivatorgranulaten
EP1509493A2 (de) 2002-05-31 2005-03-02 Henkel Kommanditgesellschaft auf Aktien Desodorierung von kationischen ammoniumacetonitrilderivaten
JP2006508170A (ja) 2002-12-18 2006-03-09 ザ プロクター アンド ギャンブル カンパニー 有機活性化剤
DE102004028494A1 (de) * 2004-06-11 2005-12-29 Clariant Gmbh Mischungen von Ammoniumnitril-Bleichaktivatoren und Aminosäuren
JP2007172716A (ja) * 2005-12-20 2007-07-05 Sony Corp 再生装置、再生方法および再生プログラム、記録媒体およびデータ構造、ならびに、オーサリング装置、オーサリング方法およびオーサリングプログラム
DE102006013664A1 (de) * 2006-03-24 2007-10-18 Clariant International Limited Verfahren zur Herstellung von Ammoniumnitrilen
DE102006013666A1 (de) * 2006-03-24 2007-09-27 Clariant International Limited Verbessertes Verfahren zur Herstellung von natriumchloridfreien Ammoniumnitrilen
US8124793B2 (en) * 2007-11-27 2012-02-28 Gail Marie Cronyn, legal representative Derivatives of ethylene methanedisulfonate as cancer chemotherapeutic agents

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0464880A1 (de) * 1990-05-30 1992-01-08 Unilever N.V. Bleichmittelzusammensetzung

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4915863A (en) 1987-08-14 1990-04-10 Kao Corporation Bleaching composition
GB9011618D0 (en) 1990-05-24 1990-07-11 Unilever Plc Bleaching composition
DE19605526A1 (de) 1996-02-15 1997-08-21 Hoechst Ag Ammoniumnitrile und deren Verwendung als Bleichaktivatoren
US6211130B1 (en) 1997-08-21 2001-04-03 Henkel Kommanditgesellschaft Auf Aktien Use of quaternary acetonitrile compounds as activators for detergents
DE10057045A1 (de) * 2000-11-17 2002-05-23 Clariant Gmbh Teilchenförmige Bleichaktivatoren auf der Basis von Acetonitrilen

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0464880A1 (de) * 1990-05-30 1992-01-08 Unilever N.V. Bleichmittelzusammensetzung

Also Published As

Publication number Publication date
BR0112869A (pt) 2003-04-22
US20040059148A1 (en) 2004-03-25
WO2002012175A2 (de) 2002-02-14
EP1309542B1 (de) 2006-05-31
JP2004505946A (ja) 2004-02-26
DE50109972D1 (de) 2006-07-06
EP1309542A2 (de) 2003-05-14
US7005534B2 (en) 2006-02-28
ES2265441T3 (es) 2007-02-16
DE10038086A1 (de) 2002-02-14

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