WO2001039290A3 - Method and apparatus for producing lithium based cathodes - Google Patents

Method and apparatus for producing lithium based cathodes Download PDF

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Publication number
WO2001039290A3
WO2001039290A3 PCT/US2000/031889 US0031889W WO0139290A3 WO 2001039290 A3 WO2001039290 A3 WO 2001039290A3 US 0031889 W US0031889 W US 0031889W WO 0139290 A3 WO0139290 A3 WO 0139290A3
Authority
WO
WIPO (PCT)
Prior art keywords
solution
producing lithium
lithium based
based cathodes
acac
Prior art date
Application number
PCT/US2000/031889
Other languages
French (fr)
Other versions
WO2001039290A2 (en
Inventor
Lonnie G Johnson
Ahmet Erbil
Original Assignee
Johnson Res & Dev Company Inc
Lonnie G Johnson
Ahmet Erbil
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US09/447,250 external-priority patent/US6582481B1/en
Priority claimed from US09/511,275 external-priority patent/US6511516B1/en
Application filed by Johnson Res & Dev Company Inc, Lonnie G Johnson, Ahmet Erbil filed Critical Johnson Res & Dev Company Inc
Priority to AU19237/01A priority Critical patent/AU1923701A/en
Priority to JP2001540859A priority patent/JP2003515888A/en
Priority to IL14979500A priority patent/IL149795A0/en
Priority to EP00982172A priority patent/EP1252664A2/en
Publication of WO2001039290A2 publication Critical patent/WO2001039290A2/en
Publication of WO2001039290A3 publication Critical patent/WO2001039290A3/en

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    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/139—Processes of manufacture
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G49/00—Compounds of iron
    • C01G49/0018—Mixed oxides or hydroxides
    • C01G49/0027—Mixed oxides or hydroxides containing one alkali metal
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00—Compounds of cobalt
    • C01G51/40—Cobaltates
    • C01G51/42—Cobaltates containing alkali metals, e.g. LiCoO2
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/40—Nickelates
    • C01G53/42—Nickelates containing alkali metals, e.g. LiNiO2
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/04—Processes of manufacture in general
    • H01M4/0402—Methods of deposition of the material
    • H01M4/0421—Methods of deposition of the material involving vapour deposition
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/04—Processes of manufacture in general
    • H01M4/0402—Methods of deposition of the material
    • H01M4/0421—Methods of deposition of the material involving vapour deposition
    • H01M4/0423—Physical vapour deposition
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/131—Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/485—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/08—Intercalated structures, i.e. with atoms or molecules intercalated in their structure
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/77—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by unit-cell parameters, atom positions or structure diagrams
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Abstract

A method of producing a layer of lithiated material is provided wherein a mixture of Li(acac) and Co (acac)3 is dissolved in solution (50). The solution is deposited upon a substrate (56) by atomizing t he solution (52), passing the atomized solution into a heated gas stream (51) so as to vaporize the solution, and directing the vaporized solution (55) onto a substrate (56).
PCT/US2000/031889 1999-11-23 2000-11-20 Method and apparatus for producing lithium based cathodes WO2001039290A2 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
AU19237/01A AU1923701A (en) 1999-11-23 2000-11-20 Method and apparatus for producing lithium based cathodes
JP2001540859A JP2003515888A (en) 1999-11-23 2000-11-20 Method and apparatus for producing a lithium-based cathode
IL14979500A IL149795A0 (en) 1999-11-23 2000-11-20 Method and apparatus for producing lithium based cathodes
EP00982172A EP1252664A2 (en) 1999-11-23 2000-11-20 Method and apparatus for producing lithium based cathodes

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US09/447,250 US6582481B1 (en) 1999-11-23 1999-11-23 Method of producing lithium base cathodes
US09/447,250 1999-11-23
US09/511,275 2000-02-23
US09/511,275 US6511516B1 (en) 2000-02-23 2000-02-23 Method and apparatus for producing lithium based cathodes

Publications (2)

Publication Number Publication Date
WO2001039290A2 WO2001039290A2 (en) 2001-05-31
WO2001039290A3 true WO2001039290A3 (en) 2001-11-22

Family

ID=27034917

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2000/031889 WO2001039290A2 (en) 1999-11-23 2000-11-20 Method and apparatus for producing lithium based cathodes

Country Status (7)

Country Link
EP (1) EP1252664A2 (en)
JP (1) JP2003515888A (en)
KR (1) KR20030014346A (en)
CN (1) CN1195681C (en)
AU (1) AU1923701A (en)
IL (1) IL149795A0 (en)
WO (1) WO2001039290A2 (en)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8354294B2 (en) * 2006-01-24 2013-01-15 De Rochemont L Pierre Liquid chemical deposition apparatus and process and products therefrom
JP2008300190A (en) * 2007-05-31 2008-12-11 Fuji Heavy Ind Ltd Manufacturing method of electrode
CN100511777C (en) * 2007-07-13 2009-07-08 张家港市国泰华荣化工新材料有限公司 A making method of cathode material for lithium ion battery
JP2010083700A (en) * 2008-09-30 2010-04-15 Dainippon Printing Co Ltd Layered body having cobalt oxide film
BR112012003369A2 (en) * 2009-08-14 2016-02-16 Univ Michigan direct thermal spray synthesis of lithium-ion battery components.
CN113913787A (en) * 2021-10-15 2022-01-11 浙江生波智能装备有限公司 Novel film preparation process and vacuum coating equipment

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH05106045A (en) * 1991-10-17 1993-04-27 Tosoh Akzo Corp Metallic acetyl acetonato-complex for forming oxide thin film
US5589300A (en) * 1993-09-27 1996-12-31 Arthur D. Little, Inc. Small particle electrodes by aerosol process
US5770018A (en) * 1996-04-10 1998-06-23 Valence Technology, Inc. Method for preparing lithium manganese oxide compounds
US5976489A (en) * 1996-04-10 1999-11-02 Valence Technology, Inc. Method for preparing lithium manganese oxide compounds

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH05106045A (en) * 1991-10-17 1993-04-27 Tosoh Akzo Corp Metallic acetyl acetonato-complex for forming oxide thin film
US5589300A (en) * 1993-09-27 1996-12-31 Arthur D. Little, Inc. Small particle electrodes by aerosol process
US5770018A (en) * 1996-04-10 1998-06-23 Valence Technology, Inc. Method for preparing lithium manganese oxide compounds
US5976489A (en) * 1996-04-10 1999-11-02 Valence Technology, Inc. Method for preparing lithium manganese oxide compounds

Also Published As

Publication number Publication date
EP1252664A2 (en) 2002-10-30
AU1923701A (en) 2001-06-04
CN1195681C (en) 2005-04-06
IL149795A0 (en) 2002-11-10
KR20030014346A (en) 2003-02-17
CN1414924A (en) 2003-04-30
JP2003515888A (en) 2003-05-07
WO2001039290A2 (en) 2001-05-31

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