WO2000004115A3 - Detergent tablet - Google Patents

Detergent tablet Download PDF

Info

Publication number
WO2000004115A3
WO2000004115A3 PCT/US1999/015149 US9915149W WO0004115A3 WO 2000004115 A3 WO2000004115 A3 WO 2000004115A3 US 9915149 W US9915149 W US 9915149W WO 0004115 A3 WO0004115 A3 WO 0004115A3
Authority
WO
WIPO (PCT)
Prior art keywords
phase
tablet
mould
detergent
detergent tablet
Prior art date
Application number
PCT/US1999/015149
Other languages
French (fr)
Other versions
WO2000004115A2 (en
Inventor
Patrizio Ricci
Brenda Frances Bennie
Christopher James Binder
Original Assignee
Procter & Gamble
Patrizio Ricci
Brenda Frances Bennie
Christopher James Binder
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=26314052&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=WO2000004115(A3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Priority claimed from GBGB9815525.2A external-priority patent/GB9815525D0/en
Priority to CA002337427A priority Critical patent/CA2337427C/en
Priority to SK59-2001A priority patent/SK592001A3/en
Priority to EP99933685A priority patent/EP1133542A1/en
Priority to AU49686/99A priority patent/AU4968699A/en
Application filed by Procter & Gamble, Patrizio Ricci, Brenda Frances Bennie, Christopher James Binder filed Critical Procter & Gamble
Priority to JP2000560214A priority patent/JP2002520474A/en
Priority to BR9912836-5A priority patent/BR9912836A/en
Priority to PL99348764A priority patent/PL190559B1/en
Priority to US09/743,879 priority patent/US6551982B1/en
Publication of WO2000004115A2 publication Critical patent/WO2000004115A2/en
Publication of WO2000004115A3 publication Critical patent/WO2000004115A3/en
Priority to HK02106338.6A priority patent/HK1046425A1/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0047—Detergents in the form of bars or tablets
    • C11D17/0065—Solid detergents containing builders
    • C11D17/0073—Tablets
    • C11D17/0086—Laundry tablets
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/62—Quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0047—Detergents in the form of bars or tablets
    • C11D17/0065—Solid detergents containing builders
    • C11D17/0073—Tablets
    • C11D17/0078—Multilayered tablets
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0047—Detergents in the form of bars or tablets
    • C11D17/0065—Solid detergents containing builders
    • C11D17/0073—Tablets
    • C11D17/0091—Dishwashing tablets
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246—Silicates, e.g. diatomaceous earth
    • C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
    • C11D3/126—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite in solid compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246—Silicates, e.g. diatomaceous earth
    • C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
    • C11D3/1273—Crystalline layered silicates of type NaMeSixO2x+1YH2O
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/22—Carbohydrates or derivatives thereof
    • C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3707—Polyethers, e.g. polyalkyleneoxides
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3769—(Co)polymerised monomers containing nitrogen, e.g. carbonamides, nitriles or amines
    • C11D3/3776—Heterocyclic compounds, e.g. lactam
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3792—Amine oxide containing polymers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38609—Protease or amylase in solid compositions only
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38645—Preparations containing enzymes, e.g. protease or amylase containing cellulase
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/40—Dyes ; Pigments
    • C11D3/42—Brightening agents ; Blueing agents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols

Abstract

A multi-phase detergent tablet for use in a washing machine, the tablet comprising: a) a first phase in the form of a shaped body having at least one mould therein; and b) a second phase in the form of a compressed body adhesively contained within said mould, wherein the tablet composition comprises one or more detergent actives which is predominantly concentrated in the second phase, and wherein the second phase additionally comprises a binder. The multi-phase tablets provide improved dissolution and cleaning characteristics together with excellent tablet integrity and strength.
PCT/US1999/015149 1998-07-17 1999-07-09 Detergent tablet WO2000004115A2 (en)

Priority Applications (9)

Application Number Priority Date Filing Date Title
US09/743,879 US6551982B1 (en) 1998-07-17 1999-07-09 Detergent tablet
PL99348764A PL190559B1 (en) 1998-07-17 1999-07-09 Detergent tablet
SK59-2001A SK592001A3 (en) 1998-07-17 1999-07-09 Detergent tablet
EP99933685A EP1133542A1 (en) 1998-07-17 1999-07-09 Detergent tablet
AU49686/99A AU4968699A (en) 1998-07-17 1999-07-09 Detergent tablet
CA002337427A CA2337427C (en) 1998-07-17 1999-07-09 Detergent tablet
JP2000560214A JP2002520474A (en) 1998-07-17 1999-07-09 Cleaning tablets
BR9912836-5A BR9912836A (en) 1998-07-17 1999-07-09 Detergent tablet
HK02106338.6A HK1046425A1 (en) 1998-07-17 2002-08-27 Detergent tablet

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
GBGB9815525.2A GB9815525D0 (en) 1998-07-17 1998-07-17 Detergent tablet
GB9815525.2 1998-07-17
GB9911268.2 1999-05-17
GB9911268A GB2339793B (en) 1998-07-17 1999-05-17 Detergent tablet

Publications (2)

Publication Number Publication Date
WO2000004115A2 WO2000004115A2 (en) 2000-01-27
WO2000004115A3 true WO2000004115A3 (en) 2001-08-23

Family

ID=26314052

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US1999/015149 WO2000004115A2 (en) 1998-07-17 1999-07-09 Detergent tablet

Country Status (21)

Country Link
EP (2) EP0979865B1 (en)
JP (1) JP2002520474A (en)
CN (1) CN1337997A (en)
AT (3) ATE342956T1 (en)
AU (1) AU4968699A (en)
BR (1) BR9912836A (en)
CA (1) CA2337427C (en)
DE (3) DE69933709T2 (en)
DK (1) DK0979865T3 (en)
ES (3) ES2175903T3 (en)
FI (1) FI4409U1 (en)
FR (1) FR2782091B1 (en)
IE (1) IES990573A2 (en)
IT (2) ITMI991512A1 (en)
NL (1) NL1012586C1 (en)
PL (1) PL190559B1 (en)
PT (1) PT979865E (en)
RU (1) RU2203934C2 (en)
SK (1) SK592001A3 (en)
TR (1) TR200100091T2 (en)
WO (1) WO2000004115A2 (en)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE29911484U1 (en) * 1998-07-17 2000-02-24 Procter & Gamble Detergent tablet
ES2168835T3 (en) * 1998-07-17 2002-06-16 Procter & Gamble METHOD TO PREPARE DETERGENT TABLETS.
EP0976819B1 (en) * 1998-07-17 2002-01-30 The Procter & Gamble Company Detergent tablet
DE19922578C2 (en) * 1999-05-17 2003-12-24 Benckiser Nv Process for the production of a multilayer tablet, in particular detergent tablet, and product which can be produced thereafter
DE10108153A1 (en) * 2000-09-28 2002-10-24 Henkel Kgaa Tray tablets and process for their manufacture
GB0029095D0 (en) * 2000-11-29 2001-01-10 Reckitt Benckiser Nv Improvements in or relating to packaging
GB0111863D0 (en) † 2001-05-15 2001-07-04 Unilever Plc Granular composition
GB0616439D0 (en) * 2006-08-18 2006-09-27 Reckitt Benckiser Nv Detergent composition
AU2007321362B2 (en) * 2006-11-16 2010-09-02 Unilever Global Ip Limited Self adhesive hard surface cleaning block
GB201003892D0 (en) * 2010-03-09 2010-04-21 Reckitt Benckiser Nv Detergent composition
JP2014534308A (en) * 2011-10-19 2014-12-18 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ Method of using the formulation for the preparation of its formulation, its manufacture and dishwashing detergent
US20190201345A1 (en) 2016-06-28 2019-07-04 Japan Antivirus Res. Inst., Ltd. Excipient and tablet
WO2020236873A1 (en) 2019-05-20 2020-11-26 Ecolab Usa Inc. Surfactant package for high foaming detergents with low level of medium to long chain linear alcohols
KR102333166B1 (en) * 2021-09-10 2021-12-02 주식회사 지원정 Method for manufacturing Washing tablet

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0466484A2 (en) * 1990-07-13 1992-01-15 Unilever Plc Detergent compositions
EP0481547A1 (en) * 1990-10-17 1992-04-22 Unilever N.V. Machine dishwashing detergent tablets
EP0481793A1 (en) * 1990-10-19 1992-04-22 Unilever Plc Detergent composition in tablet form
EP0716144A2 (en) * 1994-11-14 1996-06-12 Unilever Plc Detergent tablet having a water-soluble coating

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3962107A (en) * 1974-06-24 1976-06-08 Johnson & Johnson Enzyme-containing denture cleanser tablet
JPS5476836A (en) * 1977-12-02 1979-06-19 Kukidento Kuruto Kurisupu Kg Tablet for cleaning false tooth and production thereof
US4460490A (en) * 1980-12-18 1984-07-17 Jeyes Group Limited Lavatory cleansing blocks
EP0151203B1 (en) * 1984-02-08 1989-08-16 Richardson GmbH Anti-plaque denture cleansing tablet
DE3541146A1 (en) * 1985-11-21 1987-05-27 Henkel Kgaa MULTILAYERED DETERGENT TABLETS FOR MACHINE DISHWASHER
JP2898375B2 (en) * 1990-08-20 1999-05-31 ポーラ化成工業株式会社 Composite solid and method for producing the same
DE59606257D1 (en) * 1995-07-13 2001-02-01 Benckiser Nv DISHWASHER DETERGENT IN THE FORM OF A TABLET
US5837663A (en) * 1996-12-23 1998-11-17 Lever Brothers Company, Division Of Conopco, Inc. Machine dishwashing tablets containing a peracid
GB2327949A (en) * 1997-08-02 1999-02-10 Procter & Gamble Detergent tablet
ATE244296T1 (en) * 1997-11-10 2003-07-15 Procter & Gamble METHOD FOR PRODUCING A DETERGENT TABLET
ES2198769T3 (en) * 1997-11-10 2004-02-01 THE PROCTER & GAMBLE COMPANY MULTIPLE LAYER DETERGENT PAD THAT HAS BOTH PORTIONS COMPRESSED AND NOT COMPRESSED.
ATE234913T1 (en) * 1997-11-10 2003-04-15 Procter & Gamble METHOD FOR PRODUCING A DETERGENT TABLET
DE69828816T2 (en) * 1997-11-26 2005-12-22 The Procter & Gamble Company, Cincinnati DETERGENT TABLET
DE69833335T2 (en) * 1997-11-26 2006-09-28 The Procter & Gamble Company, Cincinnati detergent tablet
ATE276350T1 (en) * 1997-11-26 2004-10-15 Procter & Gamble METHOD FOR PRODUCING A DETERGENT TABLET
BR9815064A (en) * 1997-11-26 2001-11-20 Procter & Gamble Detergent tablet
DE29911484U1 (en) * 1998-07-17 2000-02-24 Procter & Gamble Detergent tablet
EP0976819B1 (en) * 1998-07-17 2002-01-30 The Procter & Gamble Company Detergent tablet
ES2168835T3 (en) * 1998-07-17 2002-06-16 Procter & Gamble METHOD TO PREPARE DETERGENT TABLETS.
CA2337401C (en) * 1998-07-17 2005-10-11 The Procter & Gamble Company A multi-phase detergent tablet
BR9912838A (en) * 1998-07-17 2001-05-02 Procter & Gamble Detergent tablet

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0466484A2 (en) * 1990-07-13 1992-01-15 Unilever Plc Detergent compositions
EP0481547A1 (en) * 1990-10-17 1992-04-22 Unilever N.V. Machine dishwashing detergent tablets
EP0481793A1 (en) * 1990-10-19 1992-04-22 Unilever Plc Detergent composition in tablet form
EP0716144A2 (en) * 1994-11-14 1996-06-12 Unilever Plc Detergent tablet having a water-soluble coating

Also Published As

Publication number Publication date
DE69908605D1 (en) 2003-07-10
CA2337427C (en) 2004-04-27
WO2000004115A2 (en) 2000-01-27
ATE342956T1 (en) 2006-11-15
EP0979865A1 (en) 2000-02-16
JP2002520474A (en) 2002-07-09
ES2275032T3 (en) 2007-06-01
NL1012586C1 (en) 2000-01-25
ITMI991569A0 (en) 1999-07-15
FIU990323U0 (en) 1999-07-16
IES990573A2 (en) 2000-03-08
CA2337427A1 (en) 2000-01-27
FR2782091A1 (en) 2000-02-11
PL348764A1 (en) 2002-06-03
DE69933709D1 (en) 2006-11-30
ES2199904T3 (en) 2004-03-01
CN1337997A (en) 2002-02-27
NL1012586A1 (en) 2000-01-19
FI4409U1 (en) 2000-05-18
DE69901211T2 (en) 2002-11-14
DE69901211D1 (en) 2002-05-16
FR2782091B1 (en) 2004-11-26
DE69933709T2 (en) 2007-08-23
EP0979865B1 (en) 2002-04-10
PT979865E (en) 2002-09-30
EP1133542A1 (en) 2001-09-19
ATE215985T1 (en) 2002-04-15
AU4968699A (en) 2000-02-07
TR200100091T2 (en) 2002-03-21
RU2203934C2 (en) 2003-05-10
SK592001A3 (en) 2001-07-10
DK0979865T3 (en) 2002-08-19
PL190559B1 (en) 2005-12-30
ES2175903T3 (en) 2002-11-16
DE69908605T2 (en) 2004-04-29
ITMI991569A1 (en) 2001-01-15
ITMI991512A1 (en) 2000-01-18
ATE242312T1 (en) 2003-06-15
ITMI991512A0 (en) 1999-07-09
BR9912836A (en) 2001-05-02

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