WO1986002952A3 - Method for producing anisotropic carbon fibres - Google Patents

Method for producing anisotropic carbon fibres Download PDF

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Publication number
WO1986002952A3
WO1986002952A3 PCT/EP1985/000619 EP8500619W WO8602952A3 WO 1986002952 A3 WO1986002952 A3 WO 1986002952A3 EP 8500619 W EP8500619 W EP 8500619W WO 8602952 A3 WO8602952 A3 WO 8602952A3
Authority
WO
WIPO (PCT)
Prior art keywords
pitch
weight
temperature comprised
mixture
fibres
Prior art date
Application number
PCT/EP1985/000619
Other languages
German (de)
French (fr)
Other versions
WO1986002952A2 (en
Inventor
Michael Hein
Ingo Romey
Original Assignee
Bergwerksverband Gmbh
Michael Hein
Ingo Romey
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bergwerksverband Gmbh, Michael Hein, Ingo Romey filed Critical Bergwerksverband Gmbh
Priority to AT86900087T priority Critical patent/ATE37909T1/en
Priority to DE8686900087T priority patent/DE3565559D1/en
Publication of WO1986002952A2 publication Critical patent/WO1986002952A2/en
Publication of WO1986002952A3 publication Critical patent/WO1986002952A3/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D13/00—Pencil-leads; Crayon compositions; Chalk compositions
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
    • D01F9/145—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from pitch or distillation residues
    • D01F9/15—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from pitch or distillation residues from coal pitch

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Textile Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Fibers (AREA)
  • Working-Up Tar And Pitch (AREA)

Abstract

The method for producing anisotropic carbon fibres from carbon-containing isotropic pitch comprises the following steps: a) an isotropic pitch of a size smaller than 0.1mm is released from unmeltable components at a temperature comprised between 150<o>C and 350<o>C, b) the pitch purified with a mononuclear organic solvent amount equal to 4-6 parts by weight of solvent for one part by weight of pitch filtrate is extracted at a temperature comprised between 70 and 90<o>C, c) the extraction residue is dried before its transformation into mesophase pitch, it is heat-treated during a period from 1 to 5 hours at a temperature comprised between 340<o>C and 410<o>C, and the mesophase pitch obtained is woven into fibres, d) the extraction residue is mixed before its heat treatment with 1-15% by weight of purified solvent extract by suction into a water jet. A mixture is obtained wherein the toluene soluble part is 20-40% by weight of the mixture.
PCT/EP1985/000619 1984-11-15 1985-11-13 Method for producing anisotropic carbon fibres WO1986002952A2 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
AT86900087T ATE37909T1 (en) 1984-11-15 1985-11-13 PROCESS FOR THE MANUFACTURE OF ANISOTROPIC CARBON FIBERS.
DE8686900087T DE3565559D1 (en) 1984-11-15 1985-11-13 Method for producing anisotropic carbon fibres

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DEP3441727.3 1984-11-15
DE19843441727 DE3441727A1 (en) 1984-11-15 1984-11-15 METHOD FOR PRODUCING ANISOTROPIC CARBON FIBERS

Publications (2)

Publication Number Publication Date
WO1986002952A2 WO1986002952A2 (en) 1986-05-22
WO1986002952A3 true WO1986002952A3 (en) 1986-07-03

Family

ID=6250354

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP1985/000619 WO1986002952A2 (en) 1984-11-15 1985-11-13 Method for producing anisotropic carbon fibres

Country Status (5)

Country Link
EP (1) EP0233185B1 (en)
JP (1) JPS62501302A (en)
AT (1) ATE37909T1 (en)
DE (2) DE3441727A1 (en)
WO (1) WO1986002952A2 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3702720A1 (en) * 1987-01-30 1988-08-11 Bergwerksverband Gmbh CARBONED PECH MATERIAL, METHOD FOR THE PRODUCTION THEREOF AND USE OF THE PECH MATERIAL
JPH0517782A (en) * 1991-07-09 1993-01-26 Tonen Corp Liquid crystal pitch for producing carbon yarn having high compression strength and production of carbon yarn having high compression strength

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2829288A1 (en) * 1977-07-08 1979-01-25 Exxon Research Engineering Co OPTICALLY ANISOTROPIC DEFORMABLE PECHE, METHOD OF PRODUCTION AND USE
GB2020310A (en) * 1978-05-05 1979-11-14 Exxon Research Engineering Co Carbonaceous pitches
EP0026647A1 (en) * 1979-09-28 1981-04-08 Union Carbide Corporation Mesophase pitch, processes for its production and fibers produced therefrom

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3595946A (en) * 1968-06-04 1971-07-27 Great Lakes Carbon Corp Process for the production of carbon filaments from coal tar pitch
DE2720169C2 (en) * 1977-05-05 1985-10-03 Bergwerksverband Gmbh, 4300 Essen Use of smoldering tar for the production of carbon or graphite fibers or threads
FR2392143A1 (en) * 1977-05-25 1978-12-22 British Petroleum Co PROCESS FOR MANUFACTURING CARBON OR GRAPHITE FIBERS FROM NATURAL ORGANIC MATERIAL FIBERS BY USE OF HYPERFREQUENCES
US4209500A (en) * 1977-10-03 1980-06-24 Union Carbide Corporation Low molecular weight mesophase pitch
US4277324A (en) * 1979-04-13 1981-07-07 Exxon Research & Engineering Co. Treatment of pitches in carbon artifact manufacture
JPS57154416A (en) * 1981-03-12 1982-09-24 Kureha Chem Ind Co Ltd Preparation of carbon fiber having random mosaic cross-sectional structure
JPS59163424A (en) * 1983-03-09 1984-09-14 Kashima Sekiyu Kk Spinning of petroleum mesophase

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2829288A1 (en) * 1977-07-08 1979-01-25 Exxon Research Engineering Co OPTICALLY ANISOTROPIC DEFORMABLE PECHE, METHOD OF PRODUCTION AND USE
GB2020310A (en) * 1978-05-05 1979-11-14 Exxon Research Engineering Co Carbonaceous pitches
EP0026647A1 (en) * 1979-09-28 1981-04-08 Union Carbide Corporation Mesophase pitch, processes for its production and fibers produced therefrom

Also Published As

Publication number Publication date
EP0233185B1 (en) 1988-10-12
ATE37909T1 (en) 1988-10-15
DE3565559D1 (en) 1988-11-17
DE3441727A1 (en) 1986-05-15
JPS6131153B2 (en) 1986-07-18
JPS62501302A (en) 1987-05-21
EP0233185A1 (en) 1987-08-26
WO1986002952A2 (en) 1986-05-22

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