US4970A - Improvement in bleaching rosin - Google Patents
Improvement in bleaching rosin Download PDFInfo
- Publication number
- US4970A US4970A US4970DA US4970A US 4970 A US4970 A US 4970A US 4970D A US4970D A US 4970DA US 4970 A US4970 A US 4970A
- Authority
- US
- United States
- Prior art keywords
- rosin
- bleaching
- improvement
- lye
- boiling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 title description 48
- 238000004061 bleaching Methods 0.000 title description 8
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Inorganic materials [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 32
- 235000011121 sodium hydroxide Nutrition 0.000 description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- 239000003513 alkali Substances 0.000 description 6
- 238000009835 boiling Methods 0.000 description 6
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 6
- 238000000034 method Methods 0.000 description 4
- 235000015320 potassium carbonate Nutrition 0.000 description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L sodium carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 2
- 235000015450 Tilia cordata Nutrition 0.000 description 2
- 235000011941 Tilia x europaea Nutrition 0.000 description 2
- 235000009499 Vanilla fragrans Nutrition 0.000 description 2
- 240000006722 Vanilla planifolia Species 0.000 description 2
- 235000012036 Vanilla tahitensis Nutrition 0.000 description 2
- -1 artificial heat Substances 0.000 description 2
- 239000003518 caustics Substances 0.000 description 2
- 239000004571 lime Substances 0.000 description 2
- 229940072033 potash Drugs 0.000 description 2
- KWYUFKZDYYNOTN-UHFFFAOYSA-M potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 2
- 235000017550 sodium carbonate Nutrition 0.000 description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 238000010626 work up procedure Methods 0.000 description 2
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09F—NATURAL RESINS; FRENCH POLISH; DRYING-OILS; DRIERS (SICCATIVES); TURPENTINE
- C09F1/00—Obtaining purification, or chemical modification of natural resins, e.g. oleo-resins
Definitions
- my invention consists in the art ofmaking rosin white by submitting the I same to a boiling-heat and applying. to the same a quantity of alkali and water.
- the strength of the lye by the alkaliineter may be from five toten degrees.
- This quantity of lye is heated along with a barrel of rosin until the lye boils through the rosin. I then pour into the vessel containing the boiling rosin and alkali about fifteen gallons of boiling water, continuing to apply heat and using the precaution of frequently stirring to prevent burning, andalso to thoroughly incorporate the rosin with the alkaline lye.
Description
' rrn STATES PATENT OFFICE.
JOSEPH W. HARMON, OF WILLIAMSBURG, NEW YORK, ASSIGNOR TO .HUMPHREY B. DUNHAM, OF NEWARK, NEW JERSEY.
IMPROVEMENT IN BLEACHING RQSIN,v
Specification forming part of Letters Patent No. 4.970, dated February 20, 1847.
To all whom it may concern.-
Be it known that I, JOSEPH W. HARMON, of 'Williamsburg, Kings county, and State of New York, have invented a new and useful Art of Bleaching Rosin White; and I do hereby declare that the following is a full and exact description.
The nature of my invention consists in the art ofmaking rosin white by submitting the I same to a boiling-heat and applying. to the same a quantity of alkali and water.
To enable others skilled in the arts to make and use my invention, I will proceed to describe the process.
I take about twelve gallons of lye prepared from pearlash, sodaash, or vanilla, being previously decarbonated or made caustic by the action of lime or a lye prepared by dissolving potash. The strength of the lye by the alkaliineter may be from five toten degrees.
This quantity of lye is heated along with a barrel of rosin until the lye boils through the rosin. I then pour into the vessel containing the boiling rosin and alkali about fifteen gallons of boiling water, continuing to apply heat and using the precaution of frequently stirring to prevent burning, andalso to thoroughly incorporate the rosin with the alkaline lye.
The boiling-- maybe continued for-about five minutes, the'heat is then removed, the rosin being continually mixed or worked up with the lye as long as it is suificiently soft for that purpose. I then draw off the liquidland add about fifteen gallons boiling water, with which I again work up .the rosin, the water washing out the coloring-matter which had been previously acted on by the lye. This is to be repeated, provided the rosin has failed ot'lbeing.
sufiiciently cleansed.
What I claim as-new and as my invention,
and desire to secure by Letters Patent, is-
The mode of bleaching rosin white by means of alkali, artificial heat, and water combined and connected in. process, substantially as herein described, so as to extract the coloringmatter from the rosin;
J. W. HABMON. [L..S.] Witnesses:
A. W. OQSPoONER, O. A. SPAFORD.
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US4970A true US4970A (en) | 1847-02-20 |
Family
ID=2065271
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US4970D Expired - Lifetime US4970A (en) | Improvement in bleaching rosin |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US4970A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5543110A (en) * | 1993-03-16 | 1996-08-06 | Westvaco Corporation | Tall oil deodorization process |
| US20080097062A1 (en) * | 2005-02-09 | 2008-04-24 | Albemarle Corporation | Method of Producing Disproportionated Rosin |
-
0
- US US4970D patent/US4970A/en not_active Expired - Lifetime
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5543110A (en) * | 1993-03-16 | 1996-08-06 | Westvaco Corporation | Tall oil deodorization process |
| US20080097062A1 (en) * | 2005-02-09 | 2008-04-24 | Albemarle Corporation | Method of Producing Disproportionated Rosin |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US99823A (en) | Improved indigo soap | |
| US4970A (en) | Improvement in bleaching rosin | |
| US1892548A (en) | Compound and process for treating vegetable and animal fibers and fabrics | |
| US793600A (en) | Process of manufacturing size. | |
| US242298A (en) | Compound for removing paint | |
| GB191357A (en) | Process for obtaining and cleaning cellulose from wood and similar substances containing cellulose | |
| US91407A (en) | Improved process of cleaning cotton and woollen-wastes from oils | |
| US102981A (en) | smitij | |
| USRE10040E (en) | Liquid drier for oils | |
| US1792088A (en) | Process for the manufacture of soluble starch | |
| US720922A (en) | Lubricant for wool and process of making same. | |
| US7049A (en) | Improvement in wash mixtures | |
| US42001A (en) | Improved washing-fluid | |
| US3144A (en) | Improvement in tanners flesh-blacking | |
| US138109A (en) | Improvement in wood-finishing compounds or oils | |
| US113918A (en) | Improvement in products from madder | |
| US2083280A (en) | High quality products from cellulose | |
| USRE3864E (en) | Improvement in compounds for treating- hides and skins | |
| US355935A (en) | Thomas holliday | |
| US115202A (en) | Improvement in bleaching rubber, guttarpercha | |
| US177607A (en) | Improvement in processes of making soap | |
| US149756A (en) | Improvement in soaps for washing and bleaching | |
| US100953A (en) | Improvement in the manufacture of rosinroil | |
| US4161A (en) | Improvement in compositions for removing grease from cloth | |
| US175829A (en) | Improvement in dyes |