USRE10040E - Liquid drier for oils - Google Patents
Liquid drier for oils Download PDFInfo
- Publication number
- USRE10040E USRE10040E US RE10040 E USRE10040 E US RE10040E
- Authority
- US
- United States
- Prior art keywords
- manganese
- oils
- soap
- oil
- liquid drier
- Prior art date
Links
- 239000003921 oil Substances 0.000 title description 24
- 239000007788 liquid Substances 0.000 title description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 28
- 235000019198 oils Nutrition 0.000 description 22
- PWHULOQIROXLJO-UHFFFAOYSA-N manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 18
- 229910052748 manganese Inorganic materials 0.000 description 18
- 239000011572 manganese Substances 0.000 description 18
- 239000000344 soap Substances 0.000 description 18
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 16
- VEXZGXHMUGYJMC-UHFFFAOYSA-M chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 10
- 239000012261 resinous substance Substances 0.000 description 10
- 235000011121 sodium hydroxide Nutrition 0.000 description 10
- 238000000034 method Methods 0.000 description 8
- 239000000243 solution Substances 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 6
- 150000003839 salts Chemical class 0.000 description 6
- 239000011780 sodium chloride Substances 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 235000004431 Linum usitatissimum Nutrition 0.000 description 4
- 240000006240 Linum usitatissimum Species 0.000 description 4
- 239000003513 alkali Substances 0.000 description 4
- 239000003518 caustics Substances 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 235000004426 flaxseed Nutrition 0.000 description 4
- 238000011010 flushing procedure Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000003973 paint Substances 0.000 description 4
- BVKZGUZCCUSVTD-UHFFFAOYSA-N Carbonic acid Chemical class OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 2
- 241000779819 Syncarpia glomulifera Species 0.000 description 2
- 229940036248 Turpentine Drugs 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- KZBUYRJDOAKODT-UHFFFAOYSA-N chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 159000000011 group IA salts Chemical class 0.000 description 2
- 235000021388 linseed oil Nutrition 0.000 description 2
- 239000000944 linseed oil Substances 0.000 description 2
- 150000002696 manganese Chemical class 0.000 description 2
- NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Inorganic materials O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 2
- 239000001739 pinus spp. Substances 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
Description
UNITED STATES ALFRED W. PRATT, OF FLUSHING, NEW YORK, ASSIGNOR.OF ONE-HALF TO HENRY S. LAMBERT, OF ORANGE. NEW JERSEY.
LIQUID DRIER'FOR OILS.
SPECIFICATION forming part of Reissued Letters Patent No. 10,040, dated February 21, 1882. Original No. 211,782, dated January 28, 1879. Application for reissue filed November 10, L880.
To all who: it may concern:
Be it known that I, ALFRED W. PRATT, of Flushing, in thecountyof Queens, in the State of New .York,have invented a new and useful Process for Manufacturing a Compound to be Used as a Drier for Oils, Paints, &c., which is fully set forth in the following specification.
My invention consists of a process for the production of a manganese-soap to be used as [O a. drier for oils, paints, 850., as follows: I take linseed or other suitable oil and add to it a solution of caustic soda, or other caustic alkali.
sullicicnt to saponify the oil. 7 This mixture 1 boil together in a kettle or other receptacle until the mass becomes viscid. I then take chloride of manganese, or other soluble salt of manganese, dissolve it in water, and add to the soapy mass as much of this solution of the chloride of manganese as the soapy mass will absorb to produce a manganese-soap by the reaction between the manganese salt and the soap produced by the action of the caustic alkali on the oil. I then cleansethis manganesesoap by washing it with water, the elfect of which is to remove the alkaline salt produced in the reaction ofthe soap and manganese. 1 then add resin or other resinous substances and simmer the'wholc mass in a suitable receptacle over a firc'until the entire mass be- 0 comes homogeneous.
I obtain the best results by taking ten pounds of caustic soda, dissolve it in water to produce a strong lye, to which I add seven and a half gallons of oil, (linseed preferred,) and boil that mixture together in a kettle to form a soap. I then add ten gallonsof aqueous solution of manganese, or soluble salt of manganese, and wash out the solution of soda salt which is libcrated by the double decomposition of the salt of man gancse on the soda-soap, and add thereto thirty-four poundspf rosin, or other suitable resinous substances,a-nd simmer the whole mass over a fire until it becomes entirely homogeneous.
rosin .or other resinous substances, but not so good as when used.
I prefer using the chloride of manganese such as produced as a residuum in the ordinary method of manufacturing chlorine gas by means 5c of black oxide of manganese. I do not. however, confine myself to these exact proportions, as various changes may be made without departing from the spirit of my invention.
I prefer,-and the best results are obtained by, using linseed-oilyfbut any other suitable oils may be used, and instead of rosin, other suitable resinous substances. To thin this manganese-soap I use linseed-oil, or turpentine and naphtha may be substituted for a part of 6c the oil for that purpose.
What I claim is- 1. The within-desci ihed process of producing a man ganese-soap by treating oil with caustic soda, or its equivalent, and then with a solution 6 of chloride of manganese, or its equivalent.
2. The within-described process of producing a man gancse-soap by treating oil with caustic soda, or its equivalent, and then with chloride of manganese, or its equivalent, and adding thereto rosin or other resinous substances.
J 01m BIGELOW, Jorm R.'BENNETT.
A drier will be produced by omitting the 5
Family
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