US3842888A - Apparatus for introducing ingredients into a spray drying tower - Google Patents

Apparatus for introducing ingredients into a spray drying tower Download PDF

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Publication number
US3842888A
US3842888A US00328750A US32875073A US3842888A US 3842888 A US3842888 A US 3842888A US 00328750 A US00328750 A US 00328750A US 32875073 A US32875073 A US 32875073A US 3842888 A US3842888 A US 3842888A
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holes
spray tower
liquid material
drying
solids
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US00328750A
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E Gibbons
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Colgate Palmolive Co
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Colgate Palmolive Co
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Priority to US00328750A priority Critical patent/US3842888A/en
Priority to US441302A priority patent/US3882034A/en
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/04Water-soluble compounds
    • C11D3/046Salts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/16Evaporating by spraying
    • B01D1/18Evaporating by spraying to obtain dry solids
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00Special methods for preparing compositions containing mixtures of detergents ; Methods for using cleaning compositions
    • C11D11/02Preparation in the form of powder by spray drying

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Detergent Compositions (AREA)

Abstract

An apparatus for introducing ingredients into a spray tower for producing adjustable density products having uncrutchable solids comprising a drying body having sides provided with a plurality of holes, spray nozzles connected to a pipe extending through the sides of the drying body for spraying hydrated liquid material into the drying body, and a substantially circular conduit having arms that attach and circumscribe the outside of the drying body with at least one inlet where hot drying gas enters to be effused through the holes in the drying body to flow either countercurrent or concurrently to the hydrated liquid material and dry it to form dry particulate matter. A cylindrical tube extends through the top of the drying body and provides for the introduction of uncrutchable solids. A top connects to the drying body and includes at least one aperture within the drying gas exits. The dry particulate material having uncrutchable solids is recovered through an outlet in the bottom of the body.

Description

United States Patent [191 Oct. 22, 1974 Gibbons 1 1 APPARATUS FOR INTRODUCING INGREDIENTS INTO A SPRAY DRYING TOWER [75] Inventor: Edward .1. Gibbons, Fanwood, NJ.
[73] Assignee: Colgate-Palmolive Company, New
York, NY.
[22] Filed: Feb. 1, 1973 [21] Appl. No.: 328,750
Related U.S. Application Data [63] Continuation-impart of Ser. No. 885,079, Dec. 15,
1969, abandoned.
[52] U.S. Cl. 159/4 CC [51] Int. Cl 801d 1/16 [58] Field of Search 159/4 CC, 4 B, 4 R, 48 R, 159/4 C, DIG. 3', 34/10, 57 A; 99/203 [56] References Cited UNITED STATES PATENTS 1,157,935 10/1915 Gray 99/199 1,634,640 7/1927 Zizinia 159/4 R 2,004,840 6/1935 Suchtelen 159/4 S 2,900,256 8/1959 Scott 99/56 3,143,428 8/1964 Reimers et a1. 159/4 CC X 3,354,933 11/1967 Wengeler 159/48 R 3,547,179 12/1970 Hussmann 159/4 CC 3,626,672 12/1971 Burbidge 159/4 CC 3,629,951 12/1971 Davis 159/4 CC X DUST 8i EXHAUST GASES PRODUCT BELT; l
FOREIGN PATENTS OR APPLICATIONS 118,692 7/1944 Australia 159/4 C 982,521 2/1965 Great Britain 1.59/48 R Primary Examiner-.1ack Sofer Attorney, Agent, or Firm-Herbert S. Sylvester, Esq.; Murray M. Grill, Esq.; Kenneth A. Koch, Esq.
[ 5 7 ABSTRACT An apparatus for introducing ingredients into a spray tower for producing adjustable density products having uncrutchable solids comprising a drying body having sides provided with a plurality of holes, spray nozzles connected to a pipe extending through the sides of the drying body for spraying hydrated liquid material into the drying hotly, and a substantially circular conduit having arms that attach and circumscribe the outside of the drying body with at least one inlet where hot drying gas enters to be effused through the holes in the drying body to flow either countercurrently or concurrently to the hydrated liquid material and dry it to form dry particulate matter. A cylindrical tube extends through the top of the drying body and provides for the introduction of uncrutchable solids. A top connects to the drying body and includes at least one aperture within the drying gas exits. The dry particulate material having uncrutchable solids is recovered through an outlet in the bottom f th 39 8 Claims, 2 Drawing Figures SOLIDS FEEDER TUBE FOR INTRODUCING UNCRUTCHABLE SOLIDS AT ANY PRE-SET LEVEL I DRIED PARTICULATE MATERIAL PAIENIEUnmzmsu D UST 8\ EXHAUST GASES /j l souos FEEDER T A S WD CU ww 0 O E 5 E NBU I RHE 00 R FWP ER wmm 7 TUA l, 1 4 Y /r\ m u m 0 U N Q PRODUCT BELT 7/ DRIED Fl PARTICULATE MATERIAL APPARATUS FOR INTRODUCING INGREDIENTS INTO A SPRAY DRYING TOWER RELATED APPLICATIONS This application is a continuation-in-part of copending application Ser. No. 885,079 filed Dec. 15, 1969, now abandoned.
BACKGROUND OF THE INVENTION 1. Field of the Invention This invention relates to an apparatus for producing adjustable density products. More specifically, this invention provides an apparatus for introducing ingredients into a spray drying tower that produces a low density product having uncrutchable solids.
2. Description of the Prior Art Conventional devices for dehydrating and producing low density particulate matter, for example, borax particles, utilize rapidly moving heated gas with the entrained particulate matter which is to be dehydrated. These devices are undersirable because they cause calcination and breakage of the product. They also require use of a tremendous amount of heat, are expensive and highly inefficient. The conventional devices are also not versatile because they require special modification to the basic apparatus for modification of the basic process. Various devices, e.g., Kilns, roasting pans, and fluidized beds, have been suggested for effecting dehydrating, puffing and decrepitation of particulate matter, e.g.., borax particles, without the fore going deficiencies. But these devices have also been unsuccessful in attempting to dehydrate solid particulate matter crystals, and for drying liquid solutions into dry particulate matter. What is needed and what has been invented is a novel spray tower having means for introducing ingredients thereinto to produce adjustable density products having uncrutchable solids without the foregoing deficiencies.
ity of holes, means for spraying hydrated liquid material into said drying body, and means for effusing hot drying gas through the holes to countercurrently flow against the hydrated liquid material to dry the liquid material to form dry particulate material. Also provided are means for introducing the uncrutchable solids into the drying body so as to produce the dry particulate material having the uncrutchable solids, and a top connected to the drying body having at least one aperture wherein the drying gas exits. A bottom is attached to the drying body and has at least one outlet wherefrom the dry particulate material having uncrutchable solids is recovered.
It is therefore an object at the invention to provide a spray tower forproducingadjustable density products that doesnt utilize rapidly moving heated gas with the entrained particulate matter which is to be dehydrated.
It is another object-oi the invention to provide a spray tower for producing adjustable density'products having uncrutchable. solids that doesnt cause calcinationand 2 breakage of the product; and is inexpensive, highly efficient, and requires a relatively small amount of heat.
It is yet another object of the invention to provide a versatile means for introducing ingredients into a spray tower requiring no special modification when the height of introduction of uncrut'chable solids is varied.
These, together with various ancillary objects and features which will become apparent as the following description proceeds are obtained by this novel spray tower, a preferred embodiment is shown in the accompanying drawing, by way of example only, wherein:
BRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 is a schematic vertical sectional view of the apparatus used in the invention; and
FIG. 2 is a horizontal sectional view taken along the plane of line 2-2 in FIG. 1.
DETAILED DESCRIPTION OF THE INVENTION Referring now in detail to the drawing, wherein like reference numerals designate similar parts throughout the views, and in particular to FIG. 1, drying body 10 is of cylindrical shape with circular holes 12 having centers which are essentially equidistant from the axis of drying body 10. Pipe 20 extends through the sides of drying body 10 and spray nozzles 22 and 24 are connected to it for spraying hydrated liquid material 28, or the like, into drying zone 30. In a preferred embodiment of the invention, pipe 20 is situated in the upper portion of drying body 10. A substantially channel shaped conduit 32 has inlet 34 where hot drying gases 36 enter. Conduit 32 is of dimensions greater than the diameters of holes 12, and attached to and circumscribe the outside of drying body 10, enclosing holes 12 where gases 36 effuse to countercurrently flow against hydrated liquid material 28 to form dry particulate material 38.
A top 40 is essentially a truncated cone and is integrally connected to the drying body 10 and includes mouth 42 where drying gases 36 exit in the form of dust and exhaust gases 44. Mouth 42 is circular with a center essentially positioned on the axis of drying body 10.
A cylindrical tube 46 extends through the top 40, and a worm feeder 48, driven by motor 50 introduces uncrutchable solids in the direction of arrows 52 to be mixed with the dry particulate material 38. The tube 46 is adjustable at any pre-set height level within drying body 10. A bottom 54 is provided with an outlet 56; The bottom 54 is of conical shape and outlet 56 is substantially circular with a center situated essentially on the axis of drying body 10, and dry particulate material 38 with uncrutchable solids 52 leave bottom 54 through outlet 56 to be initially deposited on the produce belt 58 which is driven by driving pulleys 60and 62', in the direction of arrow 60 and finally deposited through funnel member 62.
In a preferred embodiment for operation of the invention, a particulate material (e.g. detergent composition or other hydrated liquids or solids material that is in need of dehydrating) is prepared as an aqueous suspension or paste in a suitable mixer (not shown). It is then pumped by a pump (not shown) through pipe 20 to spray nozzles 22 and 24 from which it is sprayed into the interior of spray tower body 20. In falling through the tower body 10, spray 28 is dried to solid particles 38 by hot air 36 entering the tower at inlet 34 and exiting through outlet 42 in the form of dust and exhaust gases 44. The hot air is usually produced by burning either fuel oil or gas in a burner (not shown). Also, these dust fines 44 being removed save on the need for dust collecting equipment on the spray tower l0.
Uncrutchable solid materisl 52, such as solid hydrated borax, which can be dehydrated and expanded is fed to feeder 48 (driven by motor 50) from hopper 49 through pipe 46 into drying zone 30. Pipe 46 maybe adjusted so that the introduction may be done at such a place and in such a manner that advantage can be taken of the physical effect that the temperature/time relationship in the tower may produce. Thus, the time of dwell of the borax hydrate particles in a heated area 30 can be controlled by controlling the height at which they are fed into the spray tower by tube 46. Solid borax and detergent composition are recovered through outlet 56.
While the present invention has been described herein with reference to particular embodiments thereof, a latitude of modification, various changes and substitutions are intended in the foregoing disclosure, and in some instances some features of the invention will be employed without a corresponding use of other features without departing from the scope of the invention as set forth.
I claim:
1. A spray tower for producing adjustable density products comprising a drying body having sides provided with a plurality of holes, nozzle means for spraying hydrated liquid material into said body, means for effusing hot drying gas through said holes to countercurrently flow against said hydrated liquid material to dry said liquid material into dry particulate form, said body having a top provided with a mouth wherein said drying gas exits, a bottom provided with an outlet wherefrom said dry particulate material is removed, a cylindrical tube extending through said top and having a discharge opening that is adjustable to any pre-set height level within said body between said holes and said nozzle means and a feeding means for feeding dry solids into said cylindrical tube.
2. The spray tower of claim 1 wherein said feeding means includes a worm feeder for supplying said solids to said tube and a motor operatively connected to said worm feeder for driving said feeder.
3. The spray tower of claim 1, wherein said body is cylindrically shaped and said holes are circular with centers essentially equidistant from the axis of said body.
4. The spray tower of claim 3, wherein said means for effusing hot drying gas through said holes is a substantially channel shaped cofferdam having at least one inlet, said cofferdam surrounding and enclosing said holes, whereby said hot drying gas enters said inlet to be effused through said holes.
5. The spray tower of claim 1, wherein said means for spraying hydrated liquid material comprises at least one spray nozzle, a pipe extending through the sides of said body and connected to said spray nozzle for conducting said liquid material to said spray nozzle, and said pipe being situated in the upper portion of said body.
6. The spray tower of claim 5, wherein said top, is essentially an upright truncated cone, and said aperture is circular with a center essentially positioned on said axis of said body.
7. The spray tower of claim 1, wherein said bottom is an inverted frusto-cone.
8. The spray tower of claim 7, wherein said outlet of said bottom is substantially circular with a center situated essentially on an axis of said body.

Claims (8)

1. A spray tower for producing adjustable density products comprising a drying body having sides provided with a plurality of holes, nozzle means for spraying hydrated liquid material into said body, means for effusing hot drying gas through said holes to countercurrently flow against said hydrated liquid material to dry said liquid material into dry particulate form, said body having a top provided with a mouth wherein said drying gas exits, a bottom provided with an outlet wherefrom said dry particulate material is removed, a cylindrical tube extending through said top and having a discharge opening that is adjustable to any preset height level within said body between said holes and said nozzle means and a feeding means for feeding dry solids into said cylindrical tube.
2. The spray tower of claim 1 wherein said feeding means includes a worm feeder for supplying said solids to said tube and a motor operatively connected to said worm feeder for driving said feeder.
3. The spray tower of claim 1, wherein said body is cylindrically shaped and said holes are circular with centers essentially equidistant from the axis of said body.
4. The spray tower of claim 3, wherein said means for effusing hot drying gas through said holes is a substantially channel shaped cofferdam having at least one inlet, said cofferdam surrounding and enclosing said holes, whereby said hot drying gas enters said inlet to be effused through said holes.
5. The spray tower of claim 1, wherein said means for spraying hydrated liquid material comprises at least one spray nozzle, a pipe extending through the sides of said body and connected to said spray nozzle for conducting said liquid material to said spray nozzle, and said pipe being situated in the upper portion of said body.
6. The spray tower of claim 5, wherein said top, is essentially an upright truncated cone, and said aperture is circular with a center essentially positioned on said axis of said body.
7. The spray tower of claim 1, wherein said bottom is an inverted frusto-cone.
8. The spray tower of claim 7, wherein said outlet of said bottom is substantially circular with a center situated essentially on an axis of said body.
US00328750A 1969-12-15 1973-02-01 Apparatus for introducing ingredients into a spray drying tower Expired - Lifetime US3842888A (en)

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US00328750A US3842888A (en) 1969-12-15 1973-02-01 Apparatus for introducing ingredients into a spray drying tower
US441302A US3882034A (en) 1969-12-15 1974-02-11 Simultaneous formation of expanding borax particles and spray dried detergents

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US88507969A 1969-12-15 1969-12-15
US00328750A US3842888A (en) 1969-12-15 1973-02-01 Apparatus for introducing ingredients into a spray drying tower
US441302A US3882034A (en) 1969-12-15 1974-02-11 Simultaneous formation of expanding borax particles and spray dried detergents

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4005987A (en) * 1973-10-01 1977-02-01 Metallgesellschaft Aktiengesellschaft Process for drying moist materials, particularly crystalline solids containing water of hydration
EP0362665A1 (en) * 1988-10-04 1990-04-11 Henkel Kommanditgesellschaft auf Aktien Process for preparing a particulate detergent composition
US4946653A (en) * 1982-02-20 1990-08-07 Bayer Aktiengesellschaft Process for the simultaneous classification and regulated, continuous discharge of particulate material from fluidized bed reactors
US5489392A (en) * 1994-09-20 1996-02-06 The Procter & Gamble Company Process for making a high density detergent composition in a single mixer/densifier with selected recycle streams for improved agglomerate properties
WO1996004973A1 (en) * 1994-08-11 1996-02-22 Henkel Kommanditgesellschaft Auf Aktien Improved spray-drying process for aqueous valuable substance compositions from the group of the wetting, washing and/or cleaning agents
US5496487A (en) * 1994-08-26 1996-03-05 The Procter & Gamble Company Agglomeration process for making a detergent composition utilizing existing spray drying towers for conditioning detergent agglomerates
US5516448A (en) * 1994-09-20 1996-05-14 The Procter & Gamble Company Process for making a high density detergent composition which includes selected recycle streams for improved agglomerate
DE4442318B4 (en) * 1994-11-29 2008-01-24 Henkel Kgaa Device for distillative cleaning of feedstock
DE102006053375A1 (en) * 2006-11-10 2008-05-15 Boehringer Ingelheim Pharma Gmbh & Co. Kg Process for mixing powders

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4412978A (en) * 1982-03-15 1983-11-01 Stokely-Van Camp, Inc. Method and apparatus for manufacturing improved puffed borax
US4636328A (en) * 1984-04-05 1987-01-13 Purex Corporation Multi functional laundry product and employment of same during fabric laundering
AT382142B (en) * 1984-12-17 1987-01-12 Ruthner Michael Johann Dipl In METHOD AND DEVICE FOR PRODUCING CERAMIC POWDERS BASED ON ONE AND / OR MULTI-COMPONENT METAL OXIDS, AND MIXTURES THEREOF
US4996001A (en) * 1989-01-23 1991-02-26 Capital City Products Company Puffed borax as an agglomerating aid
US5160710A (en) * 1991-11-08 1992-11-03 Ertle Raymond T Apparatus for continuous production of intumesced particles
US6037316A (en) * 1996-09-17 2000-03-14 The Clorox Company Water soluble abrasive composition containing borax pentahydrate
US5962393A (en) * 1996-11-14 1999-10-05 The Clorox Company Powdered abrasive cleanser comprising calcium carbonate and borax pentahydrate
US5899391A (en) * 1997-11-17 1999-05-04 Hudnut Industries Inc. Cyclonic processing system
US20110027158A1 (en) * 2006-10-20 2011-02-03 Eti Maden Isletmeleri Genel Mudurlugu Calcined Tincal Production Method by Calcination Autogenic Grinding and Separation (CASG) Method in a Single Step

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3454357A (en) * 1964-08-03 1969-07-08 American Potash & Chem Corp Process and apparatus for expanding inorganic salts
US3533942A (en) * 1968-04-29 1970-10-13 American Potash & Chem Corp Process for loading expanded water-solution hydrate salt particles
US3600319A (en) * 1968-06-25 1971-08-17 Procter & Gamble Process for application of enzymes to spray-dried detergent granules

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4005987A (en) * 1973-10-01 1977-02-01 Metallgesellschaft Aktiengesellschaft Process for drying moist materials, particularly crystalline solids containing water of hydration
US4946653A (en) * 1982-02-20 1990-08-07 Bayer Aktiengesellschaft Process for the simultaneous classification and regulated, continuous discharge of particulate material from fluidized bed reactors
EP0362665A1 (en) * 1988-10-04 1990-04-11 Henkel Kommanditgesellschaft auf Aktien Process for preparing a particulate detergent composition
WO1990004015A1 (en) * 1988-10-04 1990-04-19 Henkel Kommanditgesellschaft Auf Aktien Process for producing particulate detergents
WO1996004973A1 (en) * 1994-08-11 1996-02-22 Henkel Kommanditgesellschaft Auf Aktien Improved spray-drying process for aqueous valuable substance compositions from the group of the wetting, washing and/or cleaning agents
US5496487A (en) * 1994-08-26 1996-03-05 The Procter & Gamble Company Agglomeration process for making a detergent composition utilizing existing spray drying towers for conditioning detergent agglomerates
US5489392A (en) * 1994-09-20 1996-02-06 The Procter & Gamble Company Process for making a high density detergent composition in a single mixer/densifier with selected recycle streams for improved agglomerate properties
US5516448A (en) * 1994-09-20 1996-05-14 The Procter & Gamble Company Process for making a high density detergent composition which includes selected recycle streams for improved agglomerate
DE4442318B4 (en) * 1994-11-29 2008-01-24 Henkel Kgaa Device for distillative cleaning of feedstock
DE102006053375A1 (en) * 2006-11-10 2008-05-15 Boehringer Ingelheim Pharma Gmbh & Co. Kg Process for mixing powders
WO2008055951A1 (en) 2006-11-10 2008-05-15 Boehringer Ingelheim Pharma Gmbh & Co. Kg Method for mixing powders
US20100143331A1 (en) * 2006-11-10 2010-06-10 Boehringer Ingelheim Pharma Gmbh & Co. Kg Method for mixing powders

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