US3412044A - Diamine soap as dispersant in magnetic tape formulations - Google Patents
Diamine soap as dispersant in magnetic tape formulations Download PDFInfo
- Publication number
- US3412044A US3412044A US461170A US46117065A US3412044A US 3412044 A US3412044 A US 3412044A US 461170 A US461170 A US 461170A US 46117065 A US46117065 A US 46117065A US 3412044 A US3412044 A US 3412044A
- Authority
- US
- United States
- Prior art keywords
- soap
- diamine
- dispersant
- magnetic tape
- magnetic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- G—PHYSICS
- G11—INFORMATION STORAGE
- G11B—INFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
- G11B5/00—Recording by magnetisation or demagnetisation of a record carrier; Reproducing by magnetic means; Record carriers therefor
- G11B5/62—Record carriers characterised by the selection of the material
- G11B5/68—Record carriers characterised by the selection of the material comprising one or more layers of magnetisable material homogeneously mixed with a bonding agent
- G11B5/70—Record carriers characterised by the selection of the material comprising one or more layers of magnetisable material homogeneously mixed with a bonding agent on a base layer
- G11B5/7013—Record carriers characterised by the selection of the material comprising one or more layers of magnetisable material homogeneously mixed with a bonding agent on a base layer characterised by the dispersing agent
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L75/00—Compositions of polyureas or polyurethanes; Compositions of derivatives of such polymers
- C08L75/04—Polyurethanes
- C08L75/06—Polyurethanes from polyesters
-
- G—PHYSICS
- G11—INFORMATION STORAGE
- G11B—INFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
- G11B5/00—Recording by magnetisation or demagnetisation of a record carrier; Reproducing by magnetic means; Record carriers therefor
- G11B5/62—Record carriers characterised by the selection of the material
Definitions
- This invention relates to magnetic recording tapes and, more particularly, relates to magnetic recording tapes wherein a novel fatty acid soap of a long chain diamine is used as a dispersing agent informing a dispersion of the magnetic iron oxide utilized in making the recording tape.
- the dispersant mixture contains at least 50% of the diamine soap in order to secure effective results.
- the novel dispersant was employed in conjunction with a polyurethane resin system.
- the particular polyurethane employed is sold under the trade name of Estane 5701 by B. F. Goodrich.
- This particular polyurethane was made by reacting p-p'- diphenylmethane diisocyanate, adipic acid and butanediol- 1,4 in such proportions that all of the isocyanate groups have reacted to give a substantially unreactive polymer having the following characteristics:
- This polyurethane resin can be used either alone or in combination with other resins such as a vinyl chloridevinyl acetate copolymer.
- the particular copolymer selected is one sold under the trade name VAGH by Union Carbide and Chemical Corporation.
- This particular vinyl chloride-vinyl acetate copolymer contains approximately: 91% vinyl chloride; 3% vinyl acetate; 6% vinyl alcohol.
- This copolymer has an intrinsic viscosity in cyclohexanone at 20 C. of 0.57 c.p.s. and a specific gravity of 1.39.
- a novel fatty acid soap of a long chain diamine is employed to replace all or part of the licithin which is normally used in pre paring dispersions of magnetic iron oxides.
- One particularly suitable fatty acid soap is sold under the trade name Troykyd 98C, and this is a soap made by reacting stoichiometric amounts of a saturated fatty acid having from 12 to 18 carbon atoms and a diamine having from 12 to 18 carbon atoms in each chain.
- Troykyd 98C has a molecular weight of about 490. As the following examples show, this can be effectively combined with lecithin for use as a dispersant or it can be used along as a dispersant.
- Components 1 to 5 are dispersed in a pebble-mill using appropriate amounts of methylethyl ketone, methylisobutyl ketone and toluol for 48 hours. At the end of this grinding period a solution of the binder in similar solvents is added and grinding is continued for 24 hours. This mixture is then coated on a plastic base and dried.
- Example 3 The dispersion and coating of this example is the same as Example 1.
- the improvement consisting essentially of employing as a dispersing agent a diamine soap having a molecular weight of about 490; said soap being made from a fatty acid having 12 to 18 carbon atoms and a diamine having from 12. to 18 carbon atoms in each chain.
- the dispersant comprises a mixture of the long chain fatty acid-diamine soap and lecithin, wherein the amine soap constitutes at least one half of the dispersant.
Priority Applications (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US461170A US3412044A (en) | 1965-06-03 | 1965-06-03 | Diamine soap as dispersant in magnetic tape formulations |
DEA52561A DE1285004B (de) | 1965-06-03 | 1966-05-18 | Verfahren zur Herstellung eines magnetisierbaren Aufzeichnungstraegers |
GB24004/66A GB1079609A (en) | 1965-06-03 | 1966-05-27 | Improvements in or relating to magnetic iron oxide dispersions suitable for magnetic recording media |
BE681701D BE681701A (xx) | 1965-06-03 | 1966-05-27 | |
FR63665A FR1481679A (fr) | 1965-06-03 | 1966-06-01 | Agent dispersant perfectionné pour la préparation d'une dispersion d'un oxyde de fer magnétique dans un solvant organique |
NL6607670A NL6607670A (xx) | 1965-06-03 | 1966-06-02 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US461170A US3412044A (en) | 1965-06-03 | 1965-06-03 | Diamine soap as dispersant in magnetic tape formulations |
Publications (1)
Publication Number | Publication Date |
---|---|
US3412044A true US3412044A (en) | 1968-11-19 |
Family
ID=23831478
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US461170A Expired - Lifetime US3412044A (en) | 1965-06-03 | 1965-06-03 | Diamine soap as dispersant in magnetic tape formulations |
Country Status (5)
Country | Link |
---|---|
US (1) | US3412044A (xx) |
BE (1) | BE681701A (xx) |
DE (1) | DE1285004B (xx) |
GB (1) | GB1079609A (xx) |
NL (1) | NL6607670A (xx) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1431854A (en) * | 1972-04-07 | 1976-04-14 | Sony Corp | Magnetic recording media and methods of making them |
DE3128013C1 (de) * | 1981-07-15 | 1982-11-11 | Siemens Ag | Ansteuerschaltung fuer wenigstens eine lichtemittierende Diode |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3149996A (en) * | 1960-11-16 | 1964-09-22 | Basf Ag | Magnetic record member |
US3262812A (en) * | 1964-03-26 | 1966-07-26 | Gen Electric | Magnetic recording tape with magnetic layer of oxide coated iron-cobalt alloy particles in a binder |
-
1965
- 1965-06-03 US US461170A patent/US3412044A/en not_active Expired - Lifetime
-
1966
- 1966-05-18 DE DEA52561A patent/DE1285004B/de active Pending
- 1966-05-27 BE BE681701D patent/BE681701A/xx unknown
- 1966-05-27 GB GB24004/66A patent/GB1079609A/en not_active Expired
- 1966-06-02 NL NL6607670A patent/NL6607670A/xx unknown
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3149996A (en) * | 1960-11-16 | 1964-09-22 | Basf Ag | Magnetic record member |
US3262812A (en) * | 1964-03-26 | 1966-07-26 | Gen Electric | Magnetic recording tape with magnetic layer of oxide coated iron-cobalt alloy particles in a binder |
Also Published As
Publication number | Publication date |
---|---|
GB1079609A (en) | 1967-08-16 |
NL6607670A (xx) | 1966-12-05 |
BE681701A (xx) | 1966-10-31 |
DE1285004B (de) | 1968-12-12 |
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