US2486921A - Detergent composition - Google Patents
Detergent composition Download PDFInfo
- Publication number
- US2486921A US2486921A US558961A US55896144A US2486921A US 2486921 A US2486921 A US 2486921A US 558961 A US558961 A US 558961A US 55896144 A US55896144 A US 55896144A US 2486921 A US2486921 A US 2486921A
- Authority
- US
- United States
- Prior art keywords
- detergent
- cleansing
- water
- alkali metal
- sodium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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- 239000003599 detergent Substances 0.000 title description 57
- 239000000203 mixture Substances 0.000 title description 53
- -1 alkali metal tripolyphosphate Chemical class 0.000 description 38
- 239000000271 synthetic detergent Substances 0.000 description 24
- 229910052783 alkali metal Inorganic materials 0.000 description 23
- 235000019832 sodium triphosphate Nutrition 0.000 description 23
- 239000008233 hard water Substances 0.000 description 20
- 239000004744 fabric Substances 0.000 description 11
- 150000003839 salts Chemical class 0.000 description 11
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 11
- 235000019864 coconut oil Nutrition 0.000 description 10
- 239000003240 coconut oil Substances 0.000 description 10
- 239000000194 fatty acid Substances 0.000 description 9
- 238000005406 washing Methods 0.000 description 9
- 125000004432 carbon atom Chemical group C* 0.000 description 8
- 235000014113 dietary fatty acids Nutrition 0.000 description 8
- 229930195729 fatty acid Natural products 0.000 description 8
- 239000002244 precipitate Substances 0.000 description 8
- 150000001298 alcohols Chemical class 0.000 description 7
- 150000004665 fatty acids Chemical class 0.000 description 7
- 239000004615 ingredient Substances 0.000 description 7
- 229910052708 sodium Inorganic materials 0.000 description 7
- 239000011734 sodium Substances 0.000 description 7
- 238000004900 laundering Methods 0.000 description 6
- 239000000344 soap Substances 0.000 description 6
- 159000000000 sodium salts Chemical class 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 150000008051 alkyl sulfates Chemical class 0.000 description 5
- 230000006866 deterioration Effects 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 150000001340 alkali metals Chemical class 0.000 description 4
- 239000007864 aqueous solution Substances 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical class [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 230000000622 irritating effect Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- 235000019198 oils Nutrition 0.000 description 3
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 3
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 description 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 2
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 2
- SUZRRICLUFMAQD-UHFFFAOYSA-N N-Methyltaurine Chemical compound CNCCS(O)(=O)=O SUZRRICLUFMAQD-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 230000002860 competitive effect Effects 0.000 description 2
- 230000002708 enhancing effect Effects 0.000 description 2
- 229910017053 inorganic salt Inorganic materials 0.000 description 2
- SUMDYPCJJOFFON-UHFFFAOYSA-N isethionic acid Chemical compound OCCS(O)(=O)=O SUMDYPCJJOFFON-UHFFFAOYSA-N 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- CMCBDXRRFKYBDG-UHFFFAOYSA-N 1-dodecoxydodecane Chemical compound CCCCCCCCCCCCOCCCCCCCCCCCC CMCBDXRRFKYBDG-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- YPFUJZAAZJXMIP-UHFFFAOYSA-N 3-sulfopropanediol Chemical compound OCC(O)CS(O)(=O)=O YPFUJZAAZJXMIP-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 229920000388 Polyphosphate Polymers 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 150000008107 benzenesulfonic acids Chemical class 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- XPPKVPWEQAFLFU-UHFFFAOYSA-J diphosphate(4-) Chemical compound [O-]P([O-])(=O)OP([O-])([O-])=O XPPKVPWEQAFLFU-UHFFFAOYSA-J 0.000 description 1
- 235000011180 diphosphates Nutrition 0.000 description 1
- MOTZDAYCYVMXPC-UHFFFAOYSA-N dodecyl hydrogen sulfate Chemical compound CCCCCCCCCCCCOS(O)(=O)=O MOTZDAYCYVMXPC-UHFFFAOYSA-N 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- 229940045996 isethionic acid Drugs 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 239000003350 kerosene Substances 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- 239000000395 magnesium oxide Substances 0.000 description 1
- 159000000003 magnesium salts Chemical class 0.000 description 1
- 125000005341 metaphosphate group Chemical group 0.000 description 1
- 235000019488 nut oil Nutrition 0.000 description 1
- 239000010466 nut oil Substances 0.000 description 1
- FATBGEAMYMYZAF-KTKRTIGZSA-N oleamide Chemical compound CCCCCCCC\C=C/CCCCCCCC(N)=O FATBGEAMYMYZAF-KTKRTIGZSA-N 0.000 description 1
- 239000003346 palm kernel oil Substances 0.000 description 1
- 235000019865 palm kernel oil Nutrition 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 235000021317 phosphate Nutrition 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
- 239000001205 polyphosphate Substances 0.000 description 1
- 235000011176 polyphosphates Nutrition 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000009877 rendering Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 229940080236 sodium cetyl sulfate Drugs 0.000 description 1
- GGHPAKFFUZUEKL-UHFFFAOYSA-M sodium;hexadecyl sulfate Chemical compound [Na+].CCCCCCCCCCCCCCCCOS([O-])(=O)=O GGHPAKFFUZUEKL-UHFFFAOYSA-M 0.000 description 1
- NWZBFJYXRGSRGD-UHFFFAOYSA-M sodium;octadecyl sulfate Chemical compound [Na+].CCCCCCCCCCCCCCCCCCOS([O-])(=O)=O NWZBFJYXRGSRGD-UHFFFAOYSA-M 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- AGGIJOLULBJGTQ-UHFFFAOYSA-N sulfoacetic acid Chemical compound OC(=O)CS(O)(=O)=O AGGIJOLULBJGTQ-UHFFFAOYSA-N 0.000 description 1
- DIORMHZUUKOISG-UHFFFAOYSA-N sulfoformic acid Chemical class OC(=O)S(O)(=O)=O DIORMHZUUKOISG-UHFFFAOYSA-N 0.000 description 1
- 125000001273 sulfonato group Chemical group [O-]S(*)(=O)=O 0.000 description 1
- 150000003460 sulfonic acids Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/06—Phosphates, including polyphosphates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
Definitions
- This invention relates to cleansing agents and more particularly concerns compositions having markedly improved characteristics rendering them suitable as all-purpose, hard water detergent agents for use both in the househSld where mildness is desirable and in the laundry where heavy-duty performance is required.
- An object of the present invention is to provide a general purpose household detergent composition having superior performance in hard water.
- Another object is to provide a synthetic detergent composition that will suds and clean in hard water as well as, or better than, heavy-duty or other detergent compositions of the prior art at a comparable cost.
- a further object is to provide a heavy-duty economical detergent composition that will not precipitate as an insoluble curd in hard water either in washing or in rinsing, and will be especially suitable for use in automatic washing machines.
- a still further object is to provide a detergent composition which combines the properties of heavy-duty performance, resistance to the formation of curd in hard water, with the property of unusual mildness toward the skin.
- compositions of my invention comprise essentially a synthetic detergent resistant to the hardness imparting constituents of hard water and from two to five times its weight of an alkali metal tripolyphosphate.
- compositions containing as the synthetic detergent ingredient water-soluble salts of higher aliphatic sulfuric acids containing from eight to eighteen carbon atoms in the alkyl radical and of monoglyceride sulfuric acids of fatty acids having ten to eighteen carbon atoms, which salts have pronounced detergent power in aqueous solution.
- compositions of the prior art do not form undesirable flocculent precipitates when the same are added to hard water.
- Precipitates such as those resulting from such prior art compositions collect on the fabrics being washed and render the same dingy or discolored in appearance and are as undesirable as soap curd precipitates formed on addition of soap to hard water.
- any detergent composition that forms in the rinsing operation this characteristic precipitate with salts of the hard water is highly unsuited for use in certain new automatic type washing machines, in which the clothes are not only laundered but also rinsed and partially dried automatically, because of the tendency of the precipitate to filter out on the clothes as the rinse water is drawn off.
- the alkali metal tripolyphosphate-detergent compositions of the present invention do not form such a precipitate either on addition to hard water or during the subsequent rinsing of clothes in hard water and therefore they offer an excellent solution to an important problem relative to the use of automatic washers in hard water territories.
- compositions of the prior art do not have desired stability during use and tend to break down and lose their sudsing and detergent elliciency. Because of this characteristic, synthetic detergent compositions containing metaphosphates, for example, are unsatisfactory for home laundry use where several batches of clothes are successively washed in the'same solution.
- Example 1.50 parts of a commercial synthetic detergent containing as the active ingredient about 40% sodium alkyl sulfate derived from the higher alcohols obtained by the reduction of coconut oil are mixed with 50 parts of sodium tripolyphosphate.
- the amount by weight of sodium tripolyphosphate is about 2 /2 times the amount by weight of the alkyl sulfate.
- the composition is an excellent' all-purpose detergent agent characterized by balanced sudsing and detergent power and heavyduty cleansing performance with mildness toward colored fabrics and the skin.
- Example 2 An eflicient heavy-duty cleansing composition which is mild toward colored fabrics and the skin in aqueous cleansing solutions may be prepared in thesame manner as in Example 1 except that a commercial synthetic detergent containing about 35% of the sodium salt of the sulfuric acid ester of coconut oil monoglyceride is employed.
- Example 3 To 30 parts of the alkyl sulfate detergent employed in Example 1 are added 12 parts of a mixture consisting essentially of about 20% sodium cetyl sulfate and sodium stearyl sulfate (the sodium alkyl sulfate derived from Stenolf) and 72 parts by weight sodium tripolyphosphate.
- the alkyl sulfate and the tripolyphosphate are inthe ratio of 1;3.
- the composition thus prepared is outstandingly effective in cleansing and sudsing and has a balanced sudsing and detergent action which is unequaled, as far as I am aware, by any synthetic detergent composition of comparable cost.
- Example 4.50 parts of a commercial synthetic detergent paste containing about 28% sodium alkyl sulfate derived from'the higher alcohols obtained by the reduction of coconut oil, about 68% water and the balance unsulfated material and inorganic salt are mixed with 45 parts sodium tripolyphosphate.
- the composition has balanced sudsing and detergent power and is especially suited as an all-purpose cleansing agent for use in the household.
- my invention comprises essentially a, synthetic detergent resistant to lime, magnesia, etc. compounds contained in hard water and from two to five times its weight of an alkali metal tripolyphosphate, the term alkali metal being used herein and in the claims to include ammonium as well as the true alkali metals such as sodium and potassium for exampie.
- the various synthetic sulfate and sulfonate detergents well known in the art are particularly useful in the practice of my invention, and of outstanding interest in this connection are the water-soluble salts of high molecular aliphatic sulfuric acid esters such as the alkali metal salts of sulfuric acid esters of normal primary aliphatic alcohols having twelve to eighteen carbon atoms, particularly those whose principal active ingredient is a water-soluble salt of lauryl sulfuric acid or oleyl sulfuric acid.
- Specific examples are the sodium alkyl sulfate obtained from the mixed higher alcohols produced by the reduction of coconut oil, palm kernel oil or other oils of the coconut oil group (a group of tropical nut oils characterized by their high content of combined fatty acids having ten to fourteen carbon atoms) or the sodium alkyl sulfate derived from the higher alcohols of sperm oil.
- water-soluble salt of other aliphatic sulfuric acids having pronounced detergent power set forth.
- water-soluble salts of sulfuric acid esters of higher fatty acid monoglycerides e. g., sodium salt of the coconut oil fatty, acid monoester of 1,2-dihydroxy propane- 3-sulfuric acid ester
- sulfated higher fatty acid alkyiolamides e. g. sodium salt of sulfated coconut oil fatty acid ethanolamide
- Synthetic detergents having a true sulfonate group and possessing a substantial power to wash and cleanse in aqueous solution such as watersoluble salts of higher mono-fatty acid esters of 1,2-dihydroxy propane-3-sulfonic acid (sodium salt Of the coconut oil fatty acid monoester of this sulfonic acid is a specific example) will find use in the practice of the invention.
- watersoluble salts of higher fatty acid monoesters of lower molecular weight hydroxy alkyl sulfonic acids e. g. oleic acid ester of the sodium salt of isethionic acid
- the higher fatty acid amides of lower molecular amino alkyl sulfonic acids e. g.
- ammonium salt of oleic acid amide of N-methyl taurine may be employed.
- heavy-duty detergents may be prepared from synthetic detergents such as the water-soluble salts of the higher alcohol esters of sulfocarboxylic acids (e. g. sodium salt of the lauryl alcohol ester of sulfoacetic acid), higher alkylated benzene sulfonic acids (e. g. potassium salt of the sulfonic acid derived from the condensation product of benzene and a chlorinated kerosene fraction containing predominantly twelve carbon atoms per molecule) and ethers of high molecular alcohols and lower hydroxy sulfonic acids (e. g.
- the invention is not limited to any particular method of mixing the alkali metal tripolyphosphate with the synthetic detergents and it may be incorporated in the detergent in any of the forms in which detergents are manufactured, such as paste, flake, powdered, and spray dried forms.
- the polyphosphate may be mechanically mixed in, crutched into the detergent in the form of a slurry, or it may be added to a solution of the detergent. Although such ready-for-use mixtures may be manufactured and may be prefer- 6 able for many purposes. it is likewise within the scope of my invention to add the alkali metal tripoiyphosphates to the water prior to the adding of the detergent or vice versa, or to add both the tripolyphosphate and the detergent simultaneously but separately to the water.
- the cleansing agent of the composition of the present invention comprises essentially a mixture of a detergent of the class herein described with a tripolyphosphate
- the incorporation in the mixture of additional ingredients commonly used with cleansing agents, such as soap, perfume, inorganic salt, etc. is contemplated as part of the instant invention.
- a cleansing and laundering composition characterized by balanced sudsing and detergent power, heavy-duty cleansing performance, stability against deterioration durin storage and use, resistance toward the curd-forming ingredients of hard water during washing and rinsing, and mildness toward colored fabrics and the skin, consisting essentia1ly ⁇ of a mixture of a watersoluble, alkali metal salt of an organic sulfuric reaction product having in its molecular structure a higher molecular alkyl radical having 8 to 18 carbon atoms and a radical selected from the group consisting of sulfonic acid and sulfuric acid ester radicals, the said salt having pronounced detergent power in aqueous solution, and sodium tripolyphosphate, the amount by weight of sodium tripolyphosphate being from two to five times the amount by weight of the water-soluble, alkali metal salt.
- a cleansin and laundering composition characterized by balanced sudsing and detergent power, heavy-duty cleansing performance, stability against deterioration during storage and use, resistance toward the curd-forming ingredients of hard water during washing and rinsing, and mildness toward colored fabrics and the skin, consisting essentiall of a mixture of a watersoluble, alkali metal salt of a higher aliphatic sulfuric acid ester having 8 to 18 carbon atoms in the alkyl radical and having pronounced detergent power in aqueous solution, and sodium tripolyphosphate, the amount by weight of sodium tripolyphosphate being from two to five times the amount by weight of the water-soluble, alkali metal salt.
- a cleansing and laundering composition characterized by balanced sudsing and detergent power, heavy-duty cleansing performance, stability against deterioration during storage and use, resistance toward the curd-forming ingredients of hard water during washing and rinsing, and mildness toward colored fabrics and the skin, consisting essentially of a mixture of a water-soluble, alkali metal salt of the sulfuric acid esters of higher alcohols obtained by the reduction of an oil of the coconut oil group and sodium tripolyphosphate, the amount by weight of sodium tripolyphosphate being from two to five times the amount by weight of the water-soluble, alkali metal salt.
- a cleasing and laundering composition characterized by balanced sudsing and detergent power, heavy-duty cleansing performance, stability against deterioration during storage and use, resistance toward the curd-forming ingredients of hard water during washing and rinsing, and mildness toward colored fabrics and the skin, consisting essentially of a mixture of water-soluble, alkali metal alkyl sulfates containing predominantly 12 to 18 carbon atoms in the alkyl radicals and sodium tripolyphosphate, the amount by weight 01 .sodium tripolyphosphate being from two to five times the weight of the said mixture of the water-soluble, alkali metal alkyl sulfates.
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE498391D BE498391A (enrdf_load_html_response) | 1944-10-16 | ||
| US558961A US2486921A (en) | 1944-10-16 | 1944-10-16 | Detergent composition |
| GB19529/45A GB596560A (en) | 1944-10-16 | 1945-07-30 | All-purpose detergent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US558961A US2486921A (en) | 1944-10-16 | 1944-10-16 | Detergent composition |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US2486921A true US2486921A (en) | 1949-11-01 |
Family
ID=24231701
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US558961A Expired - Lifetime US2486921A (en) | 1944-10-16 | 1944-10-16 | Detergent composition |
Country Status (3)
| Country | Link |
|---|---|
| US (1) | US2486921A (enrdf_load_html_response) |
| BE (1) | BE498391A (enrdf_load_html_response) |
| GB (1) | GB596560A (enrdf_load_html_response) |
Cited By (295)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2610950A (en) * | 1947-07-23 | 1952-09-16 | California Research Corp | Detergent composition |
| US2631980A (en) * | 1949-07-22 | 1953-03-17 | California Research Corp | Noncaking alkyl aryl sulfonate detergent compositions |
| US2692237A (en) * | 1951-03-14 | 1954-10-19 | Colgate Palmolive Co | Detergent compositions |
| US2805989A (en) * | 1954-06-14 | 1957-09-10 | Louise P Greer | Process and composition for increasing rate of flow in sewage units |
| US2858300A (en) * | 1955-04-14 | 1958-10-28 | Corn Prod Refining Co | Sulfation of proteins |
| US2920045A (en) * | 1955-09-06 | 1960-01-05 | Colgate Palmolive Co | Heavy duty liquid detergent compositions |
| US2929788A (en) * | 1955-03-07 | 1960-03-22 | Gen Mills Inc | Detergent compositions composed of alkylaryl sulfonates and n-alkyl beta-aminopropionates |
| US2949425A (en) * | 1956-05-28 | 1960-08-16 | Colgate Palmolive Co | Mixed detergent composition |
| US2965576A (en) * | 1956-05-14 | 1960-12-20 | Procter & Gamble | Detergent compositions |
| US2990375A (en) * | 1957-07-22 | 1961-06-27 | Dow Chemical Co | Heavy duty liquid detergent compositions |
| US3034169A (en) * | 1956-12-10 | 1962-05-15 | Colgate Palmolive Co | Durable scouring pads and composition therefor |
| US3075922A (en) * | 1957-08-01 | 1963-01-29 | Colgate Palmolive Co | Prepartion of liquid detergent compositions |
| US3111218A (en) * | 1958-05-26 | 1963-11-19 | United States Steel Corp | Method of drawing wire and a lubricant therefor |
| US3173877A (en) * | 1957-09-09 | 1965-03-16 | Wyandotte Chemicals Corp | Detergent compositions comprising inorganic esters of epoxyhydrocarbon polymers |
| US3219584A (en) * | 1961-06-09 | 1965-11-23 | Alexander J Stirton | Wetting agents and surface active compositions therefrom |
| US4288427A (en) * | 1979-08-21 | 1981-09-08 | The Gillette Company | Conditioning shampoo composition and ingredient therefor |
| US5607678A (en) * | 1994-08-24 | 1997-03-04 | The Procter & Gamble Company | Mild shower gel composition comprising unique thickener system which imparts improved lathering properties and modified rinse feel |
| US5632978A (en) * | 1994-08-24 | 1997-05-27 | The Procter & Gamble Company | Mild shower gel composition comprising fatty alcohol which imparts improved lathering and thickening properties |
| US5674511A (en) * | 1994-12-06 | 1997-10-07 | The Procter & Gamble Company | Shelf stable skin cleansing liquid with gel forming polymer, lipid and crystalline ethylene glycol fatty acid ester |
| US5738623A (en) * | 1995-07-28 | 1998-04-14 | Aquatrols Corporation Of America, Inc. | Application of dry spreadable water dispersible granule compositions |
| US5759943A (en) * | 1995-07-28 | 1998-06-02 | Rhone-Poulenc Inc. | Dry spreadable water dispersible granule compositions |
| US5869070A (en) * | 1994-12-06 | 1999-02-09 | The Procter & Gamble Company | Shelf stable skin cleansing liquid with gel forming polymer and lipid |
| US5883059A (en) * | 1995-01-09 | 1999-03-16 | The Procter & Gamble Company | Three in one ultra mild lathering antibacterial liquid personal cleansing composition |
| US6375969B1 (en) | 1996-09-25 | 2002-04-23 | Rhodia Inc. | Broadcast carriers for pesticides and their use |
| US6416775B1 (en) | 1996-09-25 | 2002-07-09 | Aquatrols Holding Co., Inc. | Dry spreadable carrier for pesticides |
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| BE498391A (enrdf_load_html_response) | |
| GB596560A (en) | 1948-01-06 |
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