US20150354096A1 - Processing of chemically modified cellulosic fibres - Google Patents
Processing of chemically modified cellulosic fibres Download PDFInfo
- Publication number
- US20150354096A1 US20150354096A1 US14/654,498 US201314654498A US2015354096A1 US 20150354096 A1 US20150354096 A1 US 20150354096A1 US 201314654498 A US201314654498 A US 201314654498A US 2015354096 A1 US2015354096 A1 US 2015354096A1
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- US
- United States
- Prior art keywords
- fibres
- weight
- moisture content
- chemically modified
- web
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
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- 238000012545 processing Methods 0.000 title claims description 8
- 238000000034 method Methods 0.000 claims abstract description 60
- 239000000835 fiber Substances 0.000 claims abstract description 35
- 239000003960 organic solvent Substances 0.000 claims abstract description 19
- 238000005406 washing Methods 0.000 claims abstract description 14
- 238000001035 drying Methods 0.000 claims abstract description 13
- 229920002678 cellulose Polymers 0.000 claims abstract description 12
- 239000001913 cellulose Substances 0.000 claims abstract description 12
- 239000000203 mixture Substances 0.000 claims abstract description 12
- 238000006467 substitution reaction Methods 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000009960 carding Methods 0.000 claims description 14
- 230000003750 conditioning effect Effects 0.000 claims description 7
- 238000007385 chemical modification Methods 0.000 claims description 6
- 239000012298 atmosphere Substances 0.000 claims description 3
- 238000007789 sealing Methods 0.000 claims 3
- 230000001954 sterilising effect Effects 0.000 claims 3
- 238000004320 controlled atmosphere Methods 0.000 claims 1
- 235000012976 tarts Nutrition 0.000 abstract 1
- 239000004744 fabric Substances 0.000 description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 10
- 229920003043 Cellulose fiber Polymers 0.000 description 8
- 230000001143 conditioned effect Effects 0.000 description 8
- 229920002134 Carboxymethyl cellulose Polymers 0.000 description 6
- -1 alkyl sulphonate Chemical compound 0.000 description 5
- 239000001768 carboxy methyl cellulose Substances 0.000 description 5
- 235000010948 carboxy methyl cellulose Nutrition 0.000 description 5
- 239000008112 carboxymethyl-cellulose Substances 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 238000012986 modification Methods 0.000 description 5
- 230000004048 modification Effects 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
- 239000002250 absorbent Substances 0.000 description 4
- 230000002745 absorbent Effects 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 238000005520 cutting process Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 229920000297 Rayon Polymers 0.000 description 2
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000004745 nonwoven fabric Substances 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- 229910052709 silver Inorganic materials 0.000 description 2
- 239000004332 silver Substances 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- 238000009864 tensile test Methods 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 1
- 229920000433 Lyocell Polymers 0.000 description 1
- 229920005439 Perspex® Polymers 0.000 description 1
- 229920001213 Polysorbate 20 Polymers 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 239000012445 acidic reagent Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000007605 air drying Methods 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 238000010936 aqueous wash Methods 0.000 description 1
- 239000002152 aqueous-organic solution Substances 0.000 description 1
- JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 description 1
- 229960001950 benzethonium chloride Drugs 0.000 description 1
- UREZNYTWGJKWBI-UHFFFAOYSA-M benzethonium chloride Chemical compound [Cl-].C1=CC(C(C)(C)CC(C)(C)C)=CC=C1OCCOCC[N+](C)(C)CC1=CC=CC=C1 UREZNYTWGJKWBI-UHFFFAOYSA-M 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- FOCAUTSVDIKZOP-UHFFFAOYSA-M chloroacetate Chemical compound [O-]C(=O)CCl FOCAUTSVDIKZOP-UHFFFAOYSA-M 0.000 description 1
- 229940089960 chloroacetate Drugs 0.000 description 1
- FOCAUTSVDIKZOP-UHFFFAOYSA-N chloroacetic acid Chemical compound OC(=O)CCl FOCAUTSVDIKZOP-UHFFFAOYSA-N 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000001010 compromised effect Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- CCIVGXIOQKPBKL-UHFFFAOYSA-M ethanesulfonate Chemical compound CCS([O-])(=O)=O CCIVGXIOQKPBKL-UHFFFAOYSA-M 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000011888 foil Substances 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- TWNIBLMWSKIRAT-VFUOTHLCSA-N levoglucosan Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@H]2CO[C@@H]1O2 TWNIBLMWSKIRAT-VFUOTHLCSA-N 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000010297 mechanical methods and process Methods 0.000 description 1
- 230000005226 mechanical processes and functions Effects 0.000 description 1
- 229940127554 medical product Drugs 0.000 description 1
- 230000000116 mitigating effect Effects 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 239000004926 polymethyl methacrylate Substances 0.000 description 1
- 239000000256 polyoxyethylene sorbitan monolaurate Substances 0.000 description 1
- 235000010486 polyoxyethylene sorbitan monolaurate Nutrition 0.000 description 1
- 238000004080 punching Methods 0.000 description 1
- 239000004627 regenerated cellulose Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- VILMUCRZVVVJCA-UHFFFAOYSA-M sodium glycolate Chemical compound [Na+].OCC([O-])=O VILMUCRZVVVJCA-UHFFFAOYSA-M 0.000 description 1
- 239000007779 soft material Substances 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 238000007601 warm air drying Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Images
Classifications
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
- D01F2/24—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F13/00—Bandages or dressings; Absorbent pads
- A61F13/00051—Accessories for dressings
- A61F13/00063—Accessories for dressings comprising medicaments or additives, e.g. odor control, PH control, debriding, antimicrobic
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F13/00—Bandages or dressings; Absorbent pads
- A61F13/01—Non-adhesive bandages or dressings
- A61F13/01008—Non-adhesive bandages or dressings characterised by the material
- A61F13/01012—Non-adhesive bandages or dressings characterised by the material being made of natural material, e.g. cellulose-, protein-, collagen-based
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F13/00—Bandages or dressings; Absorbent pads
- A61F13/02—Adhesive bandages or dressings
- A61F13/0276—Apparatus or processes for manufacturing adhesive dressings or bandages
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/22—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing macromolecular materials
- A61L15/28—Polysaccharides or their derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/42—Use of materials characterised by their function or physical properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B55/00—Preserving, protecting or purifying packages or package contents in association with packaging
- B65B55/02—Sterilising, e.g. of complete packages
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01G—PRELIMINARY TREATMENT OF FIBRES, e.g. FOR SPINNING
- D01G15/00—Carding machines or accessories; Card clothing; Burr-crushing or removing arrangements associated with carding or other preliminary-treatment machines
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/425—Cellulose series
- D04H1/4258—Regenerated cellulose series
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/44—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling
- D04H1/46—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B1/00—Applying liquids, gases or vapours onto textile materials to effect treatment, e.g. washing, dyeing, bleaching, sizing or impregnating
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/38—Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
- D06M13/21—Halogenated carboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/272—Unsaturated compounds containing sulfur atoms
- D06M13/278—Vinylsulfonium compounds; Vinylsulfone or vinylsulfoxide compounds
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- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H13/00—Pulp or paper, comprising synthetic cellulose or non-cellulose fibres or web-forming material
- D21H13/02—Synthetic cellulose fibres
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F13/00—Bandages or dressings; Absorbent pads
- A61F2013/00361—Plasters
- A61F2013/00902—Plasters containing means
- A61F2013/0091—Plasters containing means with disinfecting or anaesthetics means, e.g. anti-mycrobic
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- A—HUMAN NECESSITIES
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- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F13/00—Bandages or dressings; Absorbent pads
- A61F2013/00361—Plasters
- A61F2013/00902—Plasters containing means
- A61F2013/00936—Plasters containing means metal
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
Definitions
- This invention relates to chemically modified cellulosic fibres and processes for making nonwoven fibre webs from them.
- chemically modified cellulosic fibres which may be carded on a carding machine to produce a web.
- the fibres may be ultimately processed into nonwoven fabrics for instance by needling or entangling the web, the fabrics being suitable for use in absorbent personal products or absorbent medical products such as wound dressings.
- carding processes suitable for forming webs of chemically modified cellulosic fibres or blends of chemically modified fibres with other non-gelling fibres, for example viscose or Tencel or other cellulosic fibres.
- Absorbent cellulosic fibres are well known.
- GB-A-2220881 and GB-A-2094802 describe the production of carboxymethyl cellulose fibres from regenerated cellulose fibres (viscose rayon) fibres or from cotton.
- carboxymethyl cellulose fibre of greater absorbency and strength can be produced from solvent-spun cellulose fibre.
- Such fibres are described in EP 0616650 and are manufactured by reacting solvent spun cellulose fibre with a strong alkali and a monochloroacetic acid reagent.
- alternative chemical modification of cellulose fibres is possible and also has the effect of increasing the absorbency of the cellulose fibre.
- the cellulose fibre can for instance be modified by sulphonation, for example by substitution with an alkyl sulphonate at one or more of the hydroxyl groups on the anhydroglucose monomers that make up the cellulose backbone forming ether linkages.
- Modified cellulose of this type is known as cellulose sulphonate or cellulose alkyl sulphonate some of the insoluble forms of which are described in WO2012/061225.
- Modifying the cellulose fibre requires the fibre to be exposed to one or more reagents which modify the cellulose by substitution, the degree of substitution determining the absorbency and solubility of the fibre. As the degree of substitution is increased the modified cellulose becomes increasingly soluble. As the solubility increases, absorbency also increases.
- the chemically modified fibres need to be insoluble and retain some of their fibrous form when exposed to wound fluid and consequently a balance needs to be found between solubility and absorbency.
- the chemically modified fibre can be in the form of a tow, filament, sliver, yarn or staple fibre, woven, non-woven or knitted fabric.
- an aqueous wash is generally used initially, preferably a mixture of water with a water-miscible organic solvent such as water and IMS, the major portion of the wash being organic solvent.
- the wash may contain an organic hydroxyl compound, a surfactant, and/or acid.
- the organic hydroxyl compound is a compound containing at least one alcoholic hydroxyl group, for example ethanol, methanol or another low molecular weight alcohol and/or a compound such as ethylene glycol or propylene glycol.
- the final wash or finish typically comprises a large percentage of alcohol for instance, 99% industrial alcohol and 1% emulsifier or 100% alcohol.
- the fibres are dried at low temperature for instance as described in EP 0680344, by forced air drying or radiant heat drying.
- the drying of the fibres requires the solvents that are released to be managed from an environmental and safety perspective. It would be desirable to reduce the percentage of organic solvents used in the washing process so that environmental and safety standards can be readily met. There are also potential cost and efficiency advantages to using a lower percentage of organic solvents as the cost of materials and duty are reduced.
- Fibre breakage can also adversely affect the staple length which has the effect of reducing the strength of a carded web and nonwoven fabric made from the fibres. It is possible that fibre breakage leads to a failed card process where no non-woven mat is produced. A weaker product can be more difficult to remove from the wound as the integrity of the dressing can be compromised.
- the invention provides a chemically modified cellulosic web of fibres having a tensile strength of at least 3N per cm (N/cm) in the cross direction produced by processing fibres having a moisture content of at least 7% by weight.
- Controlling the moisture content of the fibres either by controlling the drying process following washing of the modified fibres as part of the chemical modification process or by conditioning the fibres to increase their moisture content to at least 7% subsequent to drying, increases the tensile strength of the fibres to the point where it is possible to process the fibres for example on a carding machine to produce a non-woven fibre web without the production of excessive fly or shedding from a fabric produced from the web.
- the moisture content of the fibres is kept at between 11 and 20% by controlling the drying process following washing of the modified fibres as part of the chemical modification process.
- the tensile strength is measured in the cross direction on needled webs having a basis weight in the range of 80 to 120 gsm.
- the invention provides, in a further aspect, a process for producing a non-woven web of chemically modified cellulosic fibres comprising the steps of:
- the fibres are typically those resulting from a modification process using a wash or final rinse comprising less than 99% by weight such as 95% by weight of organic solvent in the wash liquor.
- the fibres can be processed into a consolidated form that allows a fabric to be produced by conventional carding means while mitigating the problem of fibre breakage and fly in the environment of the fabric production plant.
- a consolidated form could for example be a yarn, sliver, woven, non-woven or knitted fabric.
- the moisture content of the modified cellulosic fibres is increased by exposing the fibres to a moisture rich environment for at least 24 hours.
- the drying of the fibres at the end of the chemical modification process can be controlled so that the moisture content of the fibres is maintained above 7% until the fibres are subjected to further processing such as with textiling machinery for instance by carding and needling.
- the carded, needled fibre web has a tensile strength of from 3N/cm to 25 N/cm, more preferably from 7N/cm to 25N/cm and most preferably from 10N/cm to 25N/cm.
- the tensile strength of the carded, needled web is measured by cutting five specimens to a size of 25 mm ⁇ 75 mm with the long dimension being in the direction to be tested. Tensile testing is carried out at a gauge length (effective test fabric length) of 50 mm. One end of the sample is fixed in an upper jaw of a tensile testing machine and allowed to dangle into the lower jaw. The sample is then fixed by closing the jaws without stretching the sample or allowing it to be slack. The crosshead speed is set to 100 mm/min and the sample pulled to break. The tensile strength is calculated by dividing the force at break by the sample width in cm.
- the moisture content of the fibres prior to processing with textiling machinery is from 7% to 20% by weight and more preferably from 11% to 18%. More preferably the moisture content is from 11.5% and 15% by weight and most preferably it is between 12 and 15% by weight. A moisture content of 12.5% to 15% is particularly preferred and 15% is most preferred.
- moisture content is meant the amount of moisture (measured by weight) contained in the sample of fibres as a percentage of its conditioned weight and measured by the loss on drying.
- the moisture content of the fibres is measured by calculating the loss on drying using a moisture balance operated in accordance with the instrument manual.
- a moisture balance operated in accordance with the instrument manual.
- comparative measurements of moisture content can be made using a moisture meter for instance an Aquaboy (TEMI).
- carding in the present invention is meant a mechanical process that disentangles, cleans and intermixes fibres to produce a continuous web or sliver suitable for further processing.
- the invention provides a chemically modified cellulosic fibre having a moisture content of at least 7% by weight.
- FIG. 1 shows the fibre moisture content vs tensile strength of carded needled fabric in the transverse (cross) direction before and after moisture conditioning to increase the moisture content.
- the column headed IDA in the table of FIG. 1 refers to the percentage of IDA (industrial denatured alcohols) used in the wash liquor as part of the modification process.
- the columns headed % refer to the % moisture in the fibre and N/cm to the tensile strength of the resulting carded needled web in the transverse direction. It can be seen from FIG. 1 that decreasing the % of IDA in the wash liquor has a negative influence on tensile strength for carded and needled webs made from unconditioned fibres. It can also be seen that once the moisture content of those fibres is raised to more than 11%, such as 12.5 to 14% moisture those tensile strength values of the carded needled web increase.
- Dressings were prepared by modification of solvent spun cellulose tow to a degree of substitution of 0.3 to form carboxymethylcellulose, neutralising to a pH of 5.5 with an organic acid. Adding 1.2% cationic silver by an ion exchange process in a largely organic solvent such as by the process described in Ep1343510, washing in an aqueous organic solution containing sodium chloride and di-sodium EDTA for light stabilisation and to entrain approximately 0.4% EDTA.
- the dressings were removed from the packs and then subjected to various controlled environments.
- Samples were tested immediately after opening the packs. Samples removed from the other environments were sealed into plastic bags during removal, and then tested immediately. The plastic bags (also preconditioned in corresponding controlled environments) were used to maintain the humidity of the environment of the samples until the point of testing.
- LOD of the samples was determined using the Ohaus moisture balance MB23 operated in accordance with the instruction manual. A sample mass of greater than 1 gram was used. Samples were cut to fit within the weighing pan, ensuring there was adequate clearance from the heating element. A standardised method was used with a maximum temperature limit of 110° C. The endpoint was determined automatically when the sample mass stopped reducing and was stable. Under these conditions the fabric did not char. Typically, samples would be subjected to a 10 minute cycle.
- Loss on drying is the summation of all the volatile substances that can be removed by heating at 110° C. These include ethanol, water and to some degree acetic acid.
- fibres for use in wound dressings according to the invention can be successfully textiled between 42% and 50% RH at around 18 to 20° C.
- Trials suggest that fibres with 10.5% to 11.5% w/w moisture content can be carded efficiently.
- cellulose ethylsulphonate CES
- carboxymethyl cellulose CMC
- tow bundles were prepared to assess the moisture content.
- Fibres were oven dried at 105° C. for one hour prior to being conditioned at the chosen relative humidity for a minimum of 16 hours.
- the mass of the oven dried tow bundles (W 1 ) and the conditioned tow bundles (W 2 ) was taken to assess the moisture content of the fibres, using Equation 1.
- Fibres were tested at 45% RH, 65% RH, and 85% RH.
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Abstract
Description
- This invention relates to chemically modified cellulosic fibres and processes for making nonwoven fibre webs from them. In particular it relates to chemically modified cellulosic fibres which may be carded on a carding machine to produce a web. The fibres may be ultimately processed into nonwoven fabrics for instance by needling or entangling the web, the fabrics being suitable for use in absorbent personal products or absorbent medical products such as wound dressings. Also described are carding processes suitable for forming webs of chemically modified cellulosic fibres or blends of chemically modified fibres with other non-gelling fibres, for example viscose or Tencel or other cellulosic fibres.
- Absorbent cellulosic fibres are well known. For instance GB-A-2220881 and GB-A-2094802 describe the production of carboxymethyl cellulose fibres from regenerated cellulose fibres (viscose rayon) fibres or from cotton. It is also known that carboxymethyl cellulose fibre of greater absorbency and strength can be produced from solvent-spun cellulose fibre. Such fibres are described in EP 0616650 and are manufactured by reacting solvent spun cellulose fibre with a strong alkali and a monochloroacetic acid reagent. It is also known that alternative chemical modification of cellulose fibres is possible and also has the effect of increasing the absorbency of the cellulose fibre. The cellulose fibre can for instance be modified by sulphonation, for example by substitution with an alkyl sulphonate at one or more of the hydroxyl groups on the anhydroglucose monomers that make up the cellulose backbone forming ether linkages. Modified cellulose of this type is known as cellulose sulphonate or cellulose alkyl sulphonate some of the insoluble forms of which are described in WO2012/061225.
- Modifying the cellulose fibre requires the fibre to be exposed to one or more reagents which modify the cellulose by substitution, the degree of substitution determining the absorbency and solubility of the fibre. As the degree of substitution is increased the modified cellulose becomes increasingly soluble. As the solubility increases, absorbency also increases.
- For some applications, for instance for absorbent gelling wound dressings, the chemically modified fibres need to be insoluble and retain some of their fibrous form when exposed to wound fluid and consequently a balance needs to be found between solubility and absorbency. The chemically modified fibre can be in the form of a tow, filament, sliver, yarn or staple fibre, woven, non-woven or knitted fabric.
- Once the modification and neutralisation in acid has taken place, the fibres need to be washed to remove any unreacted alkali, chloroacetate, alkylsulphonate, other modifying agent or any by-products such as sodium chloride or sodium glycollate. An aqueous wash is generally used initially, preferably a mixture of water with a water-miscible organic solvent such as water and IMS, the major portion of the wash being organic solvent. The wash may contain an organic hydroxyl compound, a surfactant, and/or acid. The organic hydroxyl compound is a compound containing at least one alcoholic hydroxyl group, for example ethanol, methanol or another low molecular weight alcohol and/or a compound such as ethylene glycol or propylene glycol.
- The final wash or finish typically comprises a large percentage of alcohol for instance, 99% industrial alcohol and 1% emulsifier or 100% alcohol. After washing, the fibres are dried at low temperature for instance as described in EP 0680344, by forced air drying or radiant heat drying.
- As the washing step or steps to which the fibres are subjected following modification involve the use of relatively high percentages of organic solvents such as industrial alcohol, the drying of the fibres requires the solvents that are released to be managed from an environmental and safety perspective. It would be desirable to reduce the percentage of organic solvents used in the washing process so that environmental and safety standards can be readily met. There are also potential cost and efficiency advantages to using a lower percentage of organic solvents as the cost of materials and duty are reduced.
- We have found that reducing, for instance, the percentage of organic solvent in the wash liquor used to wash modified cellulose fibres results in fibres that have a lower tensile strength making them less suitable for processing on textile machinery such as a carding machine. The lower tensile strength can lead to the problem of fibre breakage on carding which gives higher levels of airborne lint or dust (fly) and greater shedding of broken fibre from the finished fabric. The higher level of fly necessitates increased cleaning and environment management in the fabric production process which in turn increases cost. There is also more wastage in the process as fibres tend to drop out of the fabric during the process of manufacture.
- Fibre breakage can also adversely affect the staple length which has the effect of reducing the strength of a carded web and nonwoven fabric made from the fibres. It is possible that fibre breakage leads to a failed card process where no non-woven mat is produced. A weaker product can be more difficult to remove from the wound as the integrity of the dressing can be compromised.
- We have now found that it is possible to mitigate the problem of low tensile strength in modified fibres by controlled management of the moisture content of the fibres.
- Accordingly the invention provides a chemically modified cellulosic web of fibres having a tensile strength of at least 3N per cm (N/cm) in the cross direction produced by processing fibres having a moisture content of at least 7% by weight.
- Controlling the moisture content of the fibres, either by controlling the drying process following washing of the modified fibres as part of the chemical modification process or by conditioning the fibres to increase their moisture content to at least 7% subsequent to drying, increases the tensile strength of the fibres to the point where it is possible to process the fibres for example on a carding machine to produce a non-woven fibre web without the production of excessive fly or shedding from a fabric produced from the web. Preferably the moisture content of the fibres is kept at between 11 and 20% by controlling the drying process following washing of the modified fibres as part of the chemical modification process.
- Preferably the tensile strength is measured in the cross direction on needled webs having a basis weight in the range of 80 to 120 gsm.
- Accordingly the invention provides, in a further aspect, a process for producing a non-woven web of chemically modified cellulosic fibres comprising the steps of:
- (i) obtaining chemically modified cellulosic fibres with a moisture content of at least 7%;
- (ii) carding the fibres to make a nonwoven web of fibres.
- The fibres are typically those resulting from a modification process using a wash or final rinse comprising less than 99% by weight such as 95% by weight of organic solvent in the wash liquor. By controlling the moisture content, the fibres can be processed into a consolidated form that allows a fabric to be produced by conventional carding means while mitigating the problem of fibre breakage and fly in the environment of the fabric production plant. A consolidated form could for example be a yarn, sliver, woven, non-woven or knitted fabric.
- When the fibres are to be processed using textiling machinery, if it is found that the moisture content of the fibres is too low, the moisture content of the modified cellulosic fibres is increased by exposing the fibres to a moisture rich environment for at least 24 hours. Alternatively the drying of the fibres at the end of the chemical modification process can be controlled so that the moisture content of the fibres is maintained above 7% until the fibres are subjected to further processing such as with textiling machinery for instance by carding and needling.
- Preferably the carded, needled fibre web has a tensile strength of from 3N/cm to 25 N/cm, more preferably from 7N/cm to 25N/cm and most preferably from 10N/cm to 25N/cm.
- The tensile strength of the carded, needled web is measured by cutting five specimens to a size of 25 mm×75 mm with the long dimension being in the direction to be tested. Tensile testing is carried out at a gauge length (effective test fabric length) of 50 mm. One end of the sample is fixed in an upper jaw of a tensile testing machine and allowed to dangle into the lower jaw. The sample is then fixed by closing the jaws without stretching the sample or allowing it to be slack. The crosshead speed is set to 100 mm/min and the sample pulled to break. The tensile strength is calculated by dividing the force at break by the sample width in cm.
- Preferably the moisture content of the fibres prior to processing with textiling machinery is from 7% to 20% by weight and more preferably from 11% to 18%. More preferably the moisture content is from 11.5% and 15% by weight and most preferably it is between 12 and 15% by weight. A moisture content of 12.5% to 15% is particularly preferred and 15% is most preferred.
- By the term moisture content is meant the amount of moisture (measured by weight) contained in the sample of fibres as a percentage of its conditioned weight and measured by the loss on drying.
- The moisture content of the fibres is measured by calculating the loss on drying using a moisture balance operated in accordance with the instrument manual. For convenience, during the process for making the fibres, comparative measurements of moisture content can be made using a moisture meter for instance an Aquaboy (TEMI).
- By the term carding in the present invention is meant a mechanical process that disentangles, cleans and intermixes fibres to produce a continuous web or sliver suitable for further processing.
- In a further aspect of the invention, the invention provides a chemically modified cellulosic fibre having a moisture content of at least 7% by weight.
- The invention will now be illustrated by the following examples.
- Comparison of the moisture content of fibres vs their tensile strengths once carded and needled was made by measuring the initial moisture content of dried modified cellulosic fibres produced using washes of varying alcohol content. That initial moisture content was then increased by conditioning the fibres in a moist atmosphere for 24 hours at a relative humidity of 55 to 60% and the tensile strength of the needled fabric measured again.
FIG. 1 shows the fibre moisture content vs tensile strength of carded needled fabric in the transverse (cross) direction before and after moisture conditioning to increase the moisture content. - The results show that the moisture content of the fibres influences the tensile strength of the resulting carded and needled web. The column headed IDA in the table of
FIG. 1 refers to the percentage of IDA (industrial denatured alcohols) used in the wash liquor as part of the modification process. The columns headed % refer to the % moisture in the fibre and N/cm to the tensile strength of the resulting carded needled web in the transverse direction. It can be seen fromFIG. 1 that decreasing the % of IDA in the wash liquor has a negative influence on tensile strength for carded and needled webs made from unconditioned fibres. It can also be seen that once the moisture content of those fibres is raised to more than 11%, such as 12.5 to 14% moisture those tensile strength values of the carded needled web increase. - Effect of moisture content on the tensile strength of silver containing wound dressings.
- Dressings were prepared by modification of solvent spun cellulose tow to a degree of substitution of 0.3 to form carboxymethylcellulose, neutralising to a pH of 5.5 with an organic acid. Adding 1.2% cationic silver by an ion exchange process in a largely organic solvent such as by the process described in Ep1343510, washing in an aqueous organic solution containing sodium chloride and di-sodium EDTA for light stabilisation and to entrain approximately 0.4% EDTA. Followed by washing in organic solvent wash containing fibre finishing agents including tween 20 and benzethonium chloride (to give 0.135% wt/wt BeCl on the finished product) and subsequently warm air drying, cutting to staple and processing into a nonwoven felt by carding and a needle punching process. The dressings were cut to size from the web and packaged in a light, moisture and vapour impermeable heat sealed foil pouch.
- The dressings were removed from the packs and then subjected to various controlled environments.
- Controlled Environments
-
- Ambient as packed, tested without any preconditioning
- Zero humidity: Stored in a square desiccator with 3 perforated perspex shelves above a layer of silica gel desiccant, conditioned for a minimum of 5 days
- 25° C./60% RH, for a minimum of 6 days
- 30° C./65% RH, for a minimum of 6 days
- 40° C./75% RH, for a minimum of 6 days
- Samples (ambient as packed) were tested immediately after opening the packs. Samples removed from the other environments were sealed into plastic bags during removal, and then tested immediately. The plastic bags (also preconditioned in corresponding controlled environments) were used to maintain the humidity of the environment of the samples until the point of testing.
- Loss on Drying (LOD)
- LOD of the samples was determined using the Ohaus moisture balance MB23 operated in accordance with the instruction manual. A sample mass of greater than 1 gram was used. Samples were cut to fit within the weighing pan, ensuring there was adequate clearance from the heating element. A standardised method was used with a maximum temperature limit of 110° C. The endpoint was determined automatically when the sample mass stopped reducing and was stable. Under these conditions the fabric did not char. Typically, samples would be subjected to a 10 minute cycle.
- Fabric Thickness (Loft)
- Samples were tested using the Hampden Soft Materials Thickness Gauge, Model FMTml-4D, S/N 14082. Fabric thickness (sometimes referred to as loft) was determined for 6 dressings per batch.
- Fabric Dry Tensile Strength
- 2.5 cm×7.5 cm rectangular strips were cut from along the length (machine direction) and across the width (transverse direction) using a ribbon cutting die and press. Samples were conditioned as described Table 1. The peak force and the extension at which that force occurred were recorded when a 50 mm test length was stretched at a constant separation rate of 100 mm per minute.
- Results
-
TABLE 1 Relationship between absolute and relative humidity 25° C./ 30° C./ 40° C./ Conditioning Dry Ambient 60% RH 65% RH 75% RH Moisture 0.00 9.50 13.81 19.71 38.29 (g/m3) Thickness 0.170 0.190 0.198 0.183 0.202 (mm) LOD % 9.28 1.93 14.17 15.27 18.10 Tensile 3.10 5.19 5.80 5.36 7.75 Machine (N/cm) Tensile 5.15 6.53 11.12 10.23 14.28 Transverse (N/Cm) GSM 91 102 105 98 108 (g/m2) - Loss on drying is the summation of all the volatile substances that can be removed by heating at 110° C. These include ethanol, water and to some degree acetic acid.
- For this particular fibre, for this example, textile trials have shown that fibres for use in wound dressings according to the invention can be successfully textiled between 42% and 50% RH at around 18 to 20° C. Trials suggest that fibres with 10.5% to 11.5% w/w moisture content can be carded efficiently.
- The results show that tensile strength, loft and LOD are all functions of equilibrium moisture content. The results suggest that fibres with a moisture content of greater than 9% will be able to be textiled to produce dressings suitable for use in the present invention.
- Two gelling fibre types were used in this study; cellulose ethylsulphonate (CES) and carboxymethyl cellulose (CMC).
-
TABLE 1 Summary of gelling fibres used Gelling Fibre CES fibre tow CMC fibre tow - Methods
- Single fibres were mounted onto card windows as described in BS EN 5079:1996.
- In addition, tow bundles were prepared to assess the moisture content.
- Fibres were oven dried at 105° C. for one hour prior to being conditioned at the chosen relative humidity for a minimum of 16 hours. The mass of the oven dried tow bundles (W1) and the conditioned tow bundles (W2) was taken to assess the moisture content of the fibres, using Equation 1.
-
- Single fibre tensile strength of the conditioned samples was undertaken using the method described in BS EN 5079:1996.
- Fibres were tested at 45% RH, 65% RH, and 85% RH.
- Results
- Results found that a significantly higher (P≦0.05) tensile strength was seen in the samples conditioned at 65% RH than those conditioned at 45% RH and 85% RH as shown in Table 2.
-
TABLE 2 Summary of results Relative Humidity of Atmosphere (%) Ambient 45 65 85 CES Moisture Content in fibre (%) 9 15 22 w/w Mean Fibre Breaking Strength 4.85 6.16 3.79 (cN) Standard Deviation (cN) 1.08 3.61 1.21 T-Test against 65% RH data 0.016 N/A 0.000 P value CMC Moisture Content in fibre (%) 12 15 21 Mean Fibre Breaking Strength 6.04 8.24 4.16 (cN) Standard Deviation (cN) 2.65 6.06 1.55 T-Test against 65% RH data 0.029 N/A 0.000 P value
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2013
- 2013-12-20 JP JP2015548762A patent/JP2016507663A/en active Pending
- 2013-12-20 EP EP13821122.2A patent/EP2935688A2/en not_active Withdrawn
- 2013-12-20 KR KR1020157018450A patent/KR20150099776A/en not_active Application Discontinuation
- 2013-12-20 CN CN201380073403.2A patent/CN105008611A/en active Pending
- 2013-12-20 AU AU2013366038A patent/AU2013366038A1/en not_active Abandoned
- 2013-12-20 MX MX2015007771A patent/MX2015007771A/en unknown
- 2013-12-20 US US14/654,498 patent/US20150354096A1/en not_active Abandoned
- 2013-12-20 WO PCT/GB2013/053374 patent/WO2014096843A2/en active Application Filing
- 2013-12-20 BR BR112015014816A patent/BR112015014816A2/en not_active Application Discontinuation
- 2013-12-20 CA CA2895896A patent/CA2895896A1/en not_active Abandoned
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2018
- 2018-06-20 AU AU2018204434A patent/AU2018204434B2/en not_active Ceased
- 2018-11-29 JP JP2018223751A patent/JP2019065452A/en active Pending
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2020
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KR20150099776A (en) | 2015-09-01 |
JP2016507663A (en) | 2016-03-10 |
US11286601B2 (en) | 2022-03-29 |
US20200299865A1 (en) | 2020-09-24 |
EP2935688A2 (en) | 2015-10-28 |
CA2895896A1 (en) | 2014-06-26 |
JP2019065452A (en) | 2019-04-25 |
AU2018204434B2 (en) | 2020-05-14 |
CN105008611A (en) | 2015-10-28 |
BR112015014816A2 (en) | 2017-07-11 |
MX2015007771A (en) | 2015-09-04 |
AU2018204434A1 (en) | 2018-07-05 |
AU2013366038A1 (en) | 2015-07-16 |
WO2014096843A2 (en) | 2014-06-26 |
WO2014096843A3 (en) | 2014-09-18 |
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