US1207910A - Process of crystallizing brass surfaces. - Google Patents

Process of crystallizing brass surfaces. Download PDF

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Publication number
US1207910A
US1207910A US86672314A US1914866723A US1207910A US 1207910 A US1207910 A US 1207910A US 86672314 A US86672314 A US 86672314A US 1914866723 A US1914866723 A US 1914866723A US 1207910 A US1207910 A US 1207910A
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United States
Prior art keywords
brass
crystallizing
water
ounces
sawdust
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
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US86672314A
Inventor
Otto Roy Hasenohr
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JACOB DEHECK
Original Assignee
JACOB DEHECK
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Publication date
Application filed by JACOB DEHECK filed Critical JACOB DEHECK
Priority to US86672314A priority Critical patent/US1207910A/en
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Publication of US1207910A publication Critical patent/US1207910A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C1/00Making non-ferrous alloys
    • C22C1/12Making non-ferrous alloys by processing in a semi-solid state, e.g. holding the alloy in the solid-liquid phase

Definitions

  • T he present invention relates to improvements in a process for crystallizing brass sur-- faces whereby an ornamental surface is produced upon the exposed portions thereof, either upon sheet or cast brass, such surface to be finally lacquered so as to retain the desired flaked or crystallized surface and coloring accomplished by the present process.
  • the first step consists in dipping the cast or sheet brass in a solution containing one part of nitric acid and two parts of sulfuric acid. After remaining in this solution for a period of time approximately from five to ten seconds the brass is removed and rinsed in clear, cold water. This step of the process results in the removal of all scale, dust and grease and brightens thebrass.
  • the second step consists in dipping the brass thus affected by the nitric and sulfuric acids in 'a solution of 'water in which 8 ounces of potassium cyanid is dissolved to After the brass reeach gallon of water. mains in this solution for a predetermined period of time approximately from five to ten seconds the same is removed and dipped This step of the process prevents the brass from tarnishing.
  • a third step consists in placing the brass in sawdust which is dampened or moistened with a solution of water, in which to each half gallon thereof, there is 10 ounces of salammoniac and 2 ounces of blue vitriol. Care must be taken that the sawdust is not too moist, it merely being dampened. After topies of this patent may be obtained for Specification ofl'ietters Patent.
  • the fourth step in the process consists in lacquering the surface thus affected, by the various steps heretofore described with a chip lacquer, it preferably being placed thereupon to produce a brown shade.
  • the herein described process of crystallizing brass surfaces which consists first in dipping the brass in a solution containing one part of nitric acid and two parts of sulfuric acid and maintaining the brass in said solution from five to ten seconds, then removing the brass and washing it in cold water and dipping the brass in a solution containing eight ounces of potassium cyanid to a gallon of water, where the brass is kept for from five to ten seconds, after which the brass is Washed'in cold water, and then placing the brass in sawdust which contains a mixture consisting of ten ounces of salam moniac, two ounces of blue vitriol to a half gallon of water, the brass being kept in the sawdust for a period of from one to five minutes, after which it is washed in cold water and finally dried by dipping it in and removing it from boiling water.

Description

in cold, clear water.
. earns arnnar ra ion.
or 'rnann HAUTE, INDIANA, assrdnon or ONE-HALF TO JACOB JDEHECK, or TERBE HAUTE, moraine.
PROCESS OF CRYSTALLI IZING BRASS SURFACES.
Ito Drawing.
To all whom it may concern:
Be it known that l, O'r'ro ROY HAsnNonR, f;
' State of Indiana, have invented a new and useful Process of Grystallizing Brass Surfaces, of which the, following is a specification.
T he present invention relates to improvements in a process for crystallizing brass sur-- faces whereby an ornamental surface is produced upon the exposed portions thereof, either upon sheet or cast brass, such surface to be finally lacquered so as to retain the desired flaked or crystallized surface and coloring accomplished by the present process.
lln carrying out the present process, there are substantially four steps to produce the completed article.
The first step consists in dipping the cast or sheet brass in a solution containing one part of nitric acid and two parts of sulfuric acid. After remaining in this solution for a period of time approximately from five to ten seconds the brass is removed and rinsed in clear, cold water. This step of the process results in the removal of all scale, dust and grease and brightens thebrass.
The second step consists in dipping the brass thus affected by the nitric and sulfuric acids in 'a solution of 'water in which 8 ounces of potassium cyanid is dissolved to After the brass reeach gallon of water. mains in this solution for a predetermined period of time approximately from five to ten seconds the same is removed and dipped This step of the process prevents the brass from tarnishing.
A third step consists in placing the brass in sawdust which is dampened or moistened with a solution of water, in which to each half gallon thereof, there is 10 ounces of salammoniac and 2 ounces of blue vitriol. Care must be taken that the sawdust is not too moist, it merely being dampened. After topies of this patent may be obtained for Specification ofl'ietters Patent.
Patented nee. 12, rain.
Application filed. October 14, fem. sen-aim 0. 866,723.
, remaining in the sawdust approximately for apelriod of from one to five minutes the brass is removed from the sawdust and rinsed well in clear, cold water and finally dried-lay dipping in and removing from boiling water. This step of the process results in the crystallizing of the surface of the brass.
The fourth step in the process consists in lacquering the surface thus affected, by the various steps heretofore described with a chip lacquer, it preferably being placed thereupon to produce a brown shade.
It has been found with this process, that the surface of the brass either in sheet or cast brass is crystallized or flaked, and
. that a beautiful finish is accorded thereto if this process is carried out with care.
What is claimed is:
The herein described process of crystallizing brass surfaces, which consists first in dipping the brass in a solution containing one part of nitric acid and two parts of sulfuric acid and maintaining the brass in said solution from five to ten seconds, then removing the brass and washing it in cold water and dipping the brass in a solution containing eight ounces of potassium cyanid to a gallon of water, where the brass is kept for from five to ten seconds, after which the brass is Washed'in cold water, and then placing the brass in sawdust which contains a mixture consisting of ten ounces of salam moniac, two ounces of blue vitriol to a half gallon of water, the brass being kept in the sawdust for a period of from one to five minutes, after which it is washed in cold water and finally dried by dipping it in and removing it from boiling water.
In testimony that I claim the foregoing as my own, I have hereto affixed my signature in the presence of two witnesses.
' OTTO nor nasnnonn.
"Witnesses FRANK B. MILLnn, PERRY A. HALL.
five cents each, by addressing the Commissioner of Patents. Washington, D. G.
US86672314A 1914-10-14 1914-10-14 Process of crystallizing brass surfaces. Expired - Lifetime US1207910A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
US86672314A US1207910A (en) 1914-10-14 1914-10-14 Process of crystallizing brass surfaces.

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US86672314A US1207910A (en) 1914-10-14 1914-10-14 Process of crystallizing brass surfaces.

Publications (1)

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US1207910A true US1207910A (en) 1916-12-12

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