US1003702A - Volatilizer apparatus. - Google Patents

Volatilizer apparatus. Download PDF

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US1003702A
US1003702A US60454811A US1911604548A US1003702A US 1003702 A US1003702 A US 1003702A US 60454811 A US60454811 A US 60454811A US 1911604548 A US1911604548 A US 1911604548A US 1003702 A US1003702 A US 1003702A
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volatilizer
briquets
furnace
ovens
oven
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US60454811A
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Robert A Carter Jr
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10BDESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B53/00Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form
    • C10B53/06Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form of oil shale and/or or bituminous rocks

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  • This invention relates to volatilizers for driving off the volatile matter in briquets and similar articles, so that they are rendered smokeless and odorless.
  • my invention I subject the briquets so formed to a continuous process whereby they are treated in my improved volatilizer, the gases or smoke given off in their treatment being utilized to carry on the process, rendering it continuous and extremely economical in that the briquets are fed forward by their own gravity, and, after the volatilizer has been properly heated and brought to the proper temperature, the further primary heat vof the volatilizer may be dispensed with, the entire process being then carried on by the gases given off by the briquets themselves,
  • Figure 1 is a longitudinal vertical section substantially on the line 1--1 of Fig. 3;
  • Fig. 2 is a transverse vertical section substantially on the line 2-2 of Fig. 1;
  • Fig. 3 is a transverse fragmentary .view substantially on the line 33 of Fig. 1;
  • Fig. 4 is a longitudinal vertical section substantially on the line 44 of Fig. 3.
  • clined oven 1 or 2 as the case may be, or i any multiple of this number, as may be found convenient or expedient.
  • These inclined ovens 1, 1 and 2, 2 are formed of fireclay and are arranged in the volatilizer 3, which is formed of fire-brick, so that their front ends 4, 4 will be higher than their rear ends 5, 5.
  • the degree of inclination is such that the briquets (5, 6 are to be made to pass through the volatilizer 3 in a continuous stream by gravity.
  • the different gangs are substantially duplicates of each other and for the sake of brevity merely one gang will be described, it, of course, being understood that any multiple of such gangs may be used.
  • the fire brick inclined ovens 1, 1 are supported on the fire brick angular blocks 7 (Figs. 1, 2 and 3), some of which are mounted on transverse walls 40, 40 of the volatilizer 3 and others are mounted on other fire brick blocks 8 carried by the volatilizer.
  • These blocks 7 are arranged at different elevations in the volatilizer 3 to correspond with the degree of inclination of thefire brick ovens 1 which rest upon them. As shown in Fig. 1 they are arranged at an elevation with relation to each other so as to give the fire-brick oven 1 substantially a 37 inclination.
  • bafile plates 13, 13 on the fire brick shelves 41 41 extendin them,. up until they make contact with t e roof 12 of the interior flue 14 of the volatilizer 3.
  • Two such bafile plates 13 are shown in Fig. 1, though, of course, it is eater or less number may be used as may e found convenient or expedient.
  • In each one of these baflle permit a small portion of the products ofcombustion'to pass through the baflle plate, 5 but not a suflicient quantity to be objectionable.
  • These sight holes 15 may be omitted, if desired.
  • the briquets 6, 6 are dumped by hand or b any suitable machinery into the hopper 2;, some of them falling upon the shelf 28 and being deflected into the upper inclined ovens 2, 2, while theremaining port-ion of the briquets follow the lower-portion 29 of the hopper and are thence caused to pass through the inclined ovens 1, 1. As they dependent upon the inclination of the dif- 'ferent ovens, they are, in the beginning of the operation, subjected to the heat of the roducts of primary combustion from the urnace 17. In the upper part of each of the ovens 1, 1 and 2, 2 openings or ports.
  • each secondary air port having preferably two openings. 32, 32 'in-the path of the products of primary combustion which follow their circuitous route over and around the inclined ovens 1, 1 and 2, 2.
  • the necessary lair is supplied from the exterior ofthe volatilizer 3 passing through the openings, or
  • this furnace may be allowed to die down or go out, as it is not necessary for the further treatment of the briquets to be fed to the volatilizer, as the gases given off from them pass through thediferent ports-30, 30 and mix with the air from the secondary air ports 32, 32 and burn with an intense heat and themselves pass over and around and follow the circuitous path of the products of combustion previously described, and in this manner the waste gases driven off from the briquets is used to firethe volatilizer, and to complete the further treatment of the briquets which pass automatically down the different fire brick ovens 1, 1 and 2, 2 in a continuous stream. It is therefore clear that after the process is once started the briquets are.
  • Such a discharging mechanism may be a screw. 47, the boot or reservoir, being provided with guides 48, 48 to guide the treated briquets into the path of the screw.
  • This discharging mechanism whether it be a screw such as 47, orany other form of discharging mechanism, also serves to assist in regulating the passage of thegreen briquets through .the ovens, by removing the treated briquets 115 a door 34 through which the treated briquets withdrawn by the discharging mechanism serves to regulate the passage of the green briquets through the ovens and the time that they are treated.
  • I On the upper part of the furnace 17 I preferably orm an arch 35. On this arch 35 I mount the support 9 which is provided with an aperture 36 so that the roducts of a combustion may. pass freely t rough the support 9 to equalize the pressure. I also preferably, though notnecessarily, provide the secondary air orts 31, 31 with any suitable form of va ves 49, 49 to regulate the supply of air passing through them.
  • a volatilizer comprising a fire brick structure, an inclined perforated oven mounted in the structure, a furnace mounted under the upper end of the oven, a flue connecting the furnace with the rear portion of the fire brick structure, a circuitous passage connected with the flue to insure the" products of primary combustion froin the furnace assmg back and forth over and around t e oven, primary air ports 'connected with the furnace, and secondar air ports inde endent of the furnace and eadmg at di erent pointsinto the circuitous flue or passage within the volatilizer.
  • a volatilizer comprisin a. fire brick structure having an incline oven perforated at different points throughout its length, a hopper connected with one end of. the oven, a. reservoir connected with the lower end of the oven, a furnace located at the front of the volatilizer, a flue leading from the furnace and connected with the rear of the volatilizer, passages connected with said flue and leading around the oven and one or more baflie plates to insure the products of combustion taking a circuitous route over and around the oven before passingjout of the stack.
  • a volatilizer comprising a hollow fire brick structure provided with shelves, a plurality of inclined fire brick ovens perforated at different points throu out their length mounted in said fire brici upon which the perforated ovens are mounted, fire brick tiles mounted on the shelves in the volatilizer, one or more additional inclined fire brick ovens carried by said tiles, one or more baflle plates mounted on said shelves to deflect the products of primary'and secondary combustion, a furnace, a fiuc connecting the furnace to the passage leading around the ovens, primary air ports connected with the furnace, and
  • a volatilizer comprising a hollow fire brick structure provided with shelves, a furnace mounted 1n the volatilizer and pro vided with an arch, a perforated support mounted on the arch, fire brick blocks mountedon the volatilizer, in'clined perforated ovens mounted upon said blocks, battle plates mounted on the shelves, a flue connected with the furnace and with a circuitous passage over and around the inclined ovens, primary air orts connected with the furnace and secon ary air ports connected with the said circuitous passage.
  • a volatilizer comprisin an inclined oven rovided with a plura ity of longitudina l perforations to permit the volatile gases in the briquets to be driven off at substantially the point where; they are 'evolved, a fire brick structure inclosing the oven, a furnace,'primary air ports, and a plurality of secondary air ports to convey structure, blocks air at different points along the len'gth of the oven to mix it ,with the difi'erent volatile gases driven off through the different open- witnesseses: 1 WALLACE YoUNo, EDGAR S. MURRAY.

Description

R. A. CARTER, J11. VOLATILIZEB APPARATUS.
1,003,702. Patented Sept. 19,1911.
3 SHEETS-SHEET 1.
WITNESSES 5 W.% l 2 MM I ATTORNEY 1 INVENTOR R. A. 0111111311, 1TB.
VOLATILIZER APPARATUS.
APPLIOATIUN FILED JAN. 26, 1911.
' 1,003,702. I Patented 1911.
Q? 11 N H g; Q mg R. A. CARTER, JR.
VOLATILIZER APPARATUS. APPLIOATION FILED 1,111. 25, 1011.
. 1,003,702. Patented Sept. 19,1911.
3 BHEETB'BEEET 3.
13 1 K A 3 13 1s 2 1 11 1 r r & 11 13' 4' 11 g r 5 1 4] 1% l 11" 4- Cl: lllfllfllllflfllllij ul 54 I x 4 9 31\ 1 1 33 mil *1 WITNESSES INVENTOB ATTORNEY To all whom 'it may concern:
ROBERT CARTER, JR, OF NEW YORK, N. Y.
VOLATILIZER APPARATUS.
Specification of Letters Patent.
Application filed January 25, 1911.
Patented Sept. 19, 1911.'
Serial No. 604.548.
Be it known that I, ROBERT A. CARTER, Jr., a citizen of the United States, and a resident of New York city, in the county of Queens and State of. New York,'have invented certain new and useful Improveas breeze, is mixed with an ments in Volatilizer Apparatus, of which the following is a specification, taken in connection with the accompanying drawings, which form a part of the same.
This invention relates to volatilizers for driving off the volatile matter in briquets and similar articles, so that they are rendered smokeless and odorless.
In the commercial manufacture of briquets wherein finely powdered coal or powdered coke, both of which are waste products, the latter being known commercially suitable binder such as coal tar, coal tar pitch, or oil tar, or oil tar pitch, and properly shaped to form briquets, it has been found in practice that the briquets give off a large quantity of smoke and the binder, in addition to giving off this objectionable volume of smoke, also has a disagreeable odor which materially reduces the sale of the briquets. By my invention I subject the briquets so formed to a continuous process whereby they are treated in my improved volatilizer, the gases or smoke given off in their treatment being utilized to carry on the process, rendering it continuous and extremely economical in that the briquets are fed forward by their own gravity, and, after the volatilizer has been properly heated and brought to the proper temperature, the further primary heat vof the volatilizer may be dispensed with, the entire process being then carried on by the gases given off by the briquets themselves,
. so that after the volatilizer is once started it requires very little attention and automatically treats the briquets and renders them smokeless and odorless.
In the accompanying drawings, in which one form of my improved volatilizer is shown, the same referencenumerals refer to similar parts in the several figures.
Figure 1 is a longitudinal vertical section substantially on the line 1--1 of Fig. 3; Fig. 2 is a transverse vertical section substantially on the line 2-2 of Fig. 1; Fig. 3 is a transverse fragmentary .view substantially on the line 33 of Fig. 1; and Fig. 4 is a longitudinal vertical section substantially on the line 44 of Fig. 3.
to be understood that a,
clined oven 1 or 2, as the case may be, or i any multiple of this number, as may be found convenient or expedient. These inclined ovens 1, 1 and 2, 2 are formed of fireclay and are arranged in the volatilizer 3, which is formed of fire-brick, so that their front ends 4, 4 will be higher than their rear ends 5, 5. The degree of inclination is such that the briquets (5, 6 are to be made to pass through the volatilizer 3 in a continuous stream by gravity. In practice I have found that excellent results are had when theovens 1 and 2 are arranged at substantially 37 degrees inclination, though this, of course, may be varied. The different gangs are substantially duplicates of each other and for the sake of brevity merely one gang will be described, it, of course, being understood that any multiple of such gangs may be used.
The fire brick inclined ovens 1, 1 are supported on the fire brick angular blocks 7 (Figs. 1, 2 and 3), some of which are mounted on transverse walls 40, 40 of the volatilizer 3 and others are mounted on other fire brick blocks 8 carried by the volatilizer. These blocks 7 are arranged at different elevations in the volatilizer 3 to correspond with the degree of inclination of thefire brick ovens 1 which rest upon them. As shown in Fig. 1 they are arranged at an elevation with relation to each other so as to give the fire-brick oven 1 substantially a 37 inclination.
Upon shelves 41, 41 formed on the interior of the volatilizer I mount fire brick tiles 11, 11. These tiles partly surround the ovens 1, 1 and support the upper vens' 2, 2. These tiles ll do not extend up to the roof 12 of the interior flue 14 of the volatilizer 3, Fig. 1. At intervals I mount bafile plates 13, 13 on the fire brick shelves 41, 41 extendin them,. up until they make contact with t e roof 12 of the interior flue 14 of the volatilizer 3. Two such bafile plates 13 are shown in Fig. 1, though, of course, it is eater or less number may be used as may e found convenient or expedient. In each one of these baflle permit a small portion of the products ofcombustion'to pass through the baflle plate, 5 but not a suflicient quantity to be objectionable. These sight holes 15 may be omitted, if desired.
At the front/16 of the volatilizer and beneath the upper ends 4, 4 of the different inclined ovens I mount a furnace 17' with grate bars 18, a'fuel door 119, and with primary air ports 20, 20. To dry out the volatilizer and to heatit up to the proper temperature so that it can start to volatilize automatically without any primary firing, I make a fire in the furnace 17 of coals, or some other fuel, and permit a certain amount of air to pass through the primary air ports 20, 20 u through the bed of coals so as to form 0. The products of combustion from this furnace 17, including the CO, pass through the flues 118, 118 and into the vertical flues 19, 42 passing'around and 'over lower ends 5, 5 and thence up to the roof 12 of the main passage 14 of the volatilizer, and along this roof until they meet the first baflle plat e 13', Fig. 1. They are then deflected downward through thepassages 21, 43 into the vertical passages 22, 44 back to the roof 12 of the main passage 14 along which they pass until they meet the second baflie plate 13 and are thence again deflected downward into the passages 23, 45 and caused then tov pass into the passages 24,
46 out through the stack 25, their passage being regulated by the damper 26 which controls the pressure of the gasesand products of combustion within the volatilizer 3, and the oven or ovens.
The briquets 6, 6 are dumped by hand or b any suitable machinery into the hopper 2;, some of them falling upon the shelf 28 and being deflected into the upper inclined ovens 2, 2, while theremaining port-ion of the briquets follow the lower-portion 29 of the hopper and are thence caused to pass through the inclined ovens 1, 1. As they dependent upon the inclination of the dif- 'ferent ovens, they are, in the beginning of the operation, subjected to the heat of the roducts of primary combustion from the urnace 17. In the upper part of each of the ovens 1, 1 and 2, 2 openings or ports.
circuitous path previously described, and
the briquets 6, 6 and thereafter proceed' the different ovens 1, 1 and 2, 2 near their pass down these inclined ovens 1, 1 and 2, 2 their flow being entirely due to gravity and P thence through the stack 25.. In addition to theprimary air ports 20,20 I form secondary' air ports 31, 31, Figs. 1 and 4, each secondary air port having preferably two openings. 32, 32 'in-the path of the products of primary combustion which follow their circuitous route over and around the inclined ovens 1, 1 and 2, 2. Through these secondary air ports 31, 31- the necessary lair is supplied from the exterior ofthe volatilizer 3 passing through the openings, or
ports 32, 32 to mix with the products of primary combustion from the furnace 17 and later with the ases driven off from the briquets 6, 6 WlllCh are being treated. The chemical action may be briefly stated to be that at first carbon monoxid CO is formed by combination of air with the fuel of thefire and later carbon dioxid CO by the combination of the CO With the air passing in through the secondary air ports. After the volatilizer has been started and .the process of treating the briquets has been initially begun-from theheat derived from the furnace 17, this furnace may be allowed to die down or go out, as it is not necessary for the further treatment of the briquets to be fed to the volatilizer, as the gases given off from them pass through thediferent ports-30, 30 and mix with the air from the secondary air ports 32, 32 and burn with an intense heat and themselves pass over and around and follow the circuitous path of the products of combustion previously described, and in this manner the waste gases driven off from the briquets is used to firethe volatilizer, and to complete the further treatment of the briquets which pass automatically down the different fire brick ovens 1, 1 and 2, 2 in a continuous stream. It is therefore clear that after the process is once started the briquets are.
treated automatically with their own waste gases and that all that is essential is to feed the briquets into the hopper 27 and remove the treated briquets at intervals, or continuously, as the case may be, from the boot or reservoir 33 arranged at the end of the inclined ovens 1, 1 and 2, 2. This boot 33 is of course gas tight and is provided with may be removed at intervals as desired. Preferably, however, some dlscharging, mechanism 1s provlded to continuously, or
intermittently, remove the treated briquetsfrom the boot or'reservoir 33. Such a discharging mechanism may be a screw. 47, the boot or reservoir, being provided with guides 48, 48 to guide the treated briquets into the path of the screw. This discharging mechanism whether it be a screw such as 47, orany other form of discharging mechanism, also serves to assist in regulating the passage of thegreen briquets through .the ovens, by removing the treated briquets 115 a door 34 through which the treated briquets withdrawn by the discharging mechanism serves to regulate the passage of the green briquets through the ovens and the time that they are treated.
On the upper part of the furnace 17 I preferably orm an arch 35. On this arch 35 I mount the support 9 which is provided with an aperture 36 so that the roducts of a combustion may. pass freely t rough the support 9 to equalize the pressure. I also preferably, though notnecessarily, provide the secondary air orts 31, 31 with any suitable form of va ves 49, 49 to regulate the supply of air passing through them.
Having thus described this invention in connection with an illustrative embodiment thereof to the details of which I do not desire to be limited, what is claimed as new Patent is set forth in the appended claims.
I claim v 1. A volatilizer comprising a fire brick structure, an inclined perforated oven mounted in the structure, a furnace mounted under the upper end of the oven, a flue connecting the furnace with the rear portion of the fire brick structure, a circuitous passage connected with the flue to insure the" products of primary combustion froin the furnace assmg back and forth over and around t e oven, primary air ports 'connected with the furnace, and secondar air ports inde endent of the furnace and eadmg at di erent pointsinto the circuitous flue or passage within the volatilizer. N
2. A volatilizer comprisin a. fire brick structure having an incline oven perforated at different points throughout its length, a hopper connected with one end of. the oven, a. reservoir connected with the lower end of the oven, a furnace located at the front of the volatilizer, a flue leading from the furnace and connected with the rear of the volatilizer, passages connected with said flue and leading around the oven and one or more baflie plates to insure the products of combustion taking a circuitous route over and around the oven before passingjout of the stack.
3. A volatil'zer com rising a fire brick structure having an inclined perforated 1 oven, a hopper connected with one end of the oven, a reservoir connected with the lower end of the oven, a furnace and stack located at the front of the volatilizer, primary air orts connected with the furnace, a fine lea ing from the furnace and connecting with the rear of the volatilizer, one
"or more secondary air ports connected with the main passa e of the volatilizer to permit air into sai passage independent of the furnace.
4. A volatilizer comprising a hollow fire brick structure provided with shelves, a plurality of inclined fire brick ovens perforated at different points throu out their length mounted in said fire brici upon which the perforated ovens are mounted, fire brick tiles mounted on the shelves in the volatilizer, one or more additional inclined fire brick ovens carried by said tiles, one or more baflle plates mounted on said shelves to deflect the products of primary'and secondary combustion, a furnace, a fiuc connecting the furnace to the passage leading around the ovens, primary air ports connected with the furnace, and
secondary air ports connected with the passage around the oven or ovens.
5. A volatilizer comprising a hollow fire brick structure provided with shelves, a furnace mounted 1n the volatilizer and pro vided with an arch, a perforated support mounted on the arch, fire brick blocks mountedon the volatilizer, in'clined perforated ovens mounted upon said blocks, battle plates mounted on the shelves, a flue connected with the furnace and with a circuitous passage over and around the inclined ovens, primary air orts connected with the furnace and secon ary air ports connected with the said circuitous passage.
6. A volatilizer comprisin an inclined oven rovided with a plura ity of longitudina l perforations to permit the volatile gases in the briquets to be driven off at substantially the point where; they are 'evolved, a fire brick structure inclosing the oven, a furnace,'primary air ports, and a plurality of secondary air ports to convey structure, blocks air at different points along the len'gth of the oven to mix it ,with the difi'erent volatile gases driven off through the different open- Witnesses: 1 WALLACE YoUNo, EDGAR S. MURRAY.
US60454811A 1911-01-25 1911-01-25 Volatilizer apparatus. Expired - Lifetime US1003702A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3148128A (en) * 1961-07-10 1964-09-08 Kemmerer Coal Company Adjustable slope char oven
US3171795A (en) * 1961-06-27 1965-03-02 Kemmerer Coal Company Apparatus for carbonizing carbonaceous material
US4126518A (en) * 1976-08-20 1978-11-21 Etablissement Capitrop Method and inclined chamber furnace for carbonizing fluent carbon-containing material

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3171795A (en) * 1961-06-27 1965-03-02 Kemmerer Coal Company Apparatus for carbonizing carbonaceous material
US3148128A (en) * 1961-07-10 1964-09-08 Kemmerer Coal Company Adjustable slope char oven
US4126518A (en) * 1976-08-20 1978-11-21 Etablissement Capitrop Method and inclined chamber furnace for carbonizing fluent carbon-containing material

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