UA89507C2 - Способ и устройство для получения серосодержащих азотных удобрений - Google Patents
Способ и устройство для получения серосодержащих азотных удобрений Download PDFInfo
- Publication number
- UA89507C2 UA89507C2 UAA200705193A UAA200705193A UA89507C2 UA 89507 C2 UA89507 C2 UA 89507C2 UA A200705193 A UAA200705193 A UA A200705193A UA A200705193 A UAA200705193 A UA A200705193A UA 89507 C2 UA89507 C2 UA 89507C2
- Authority
- UA
- Ukraine
- Prior art keywords
- ammonium nitrate
- fertilizer
- nitrate
- lime
- sulfur
- Prior art date
Links
- 239000003337 fertilizer Substances 0.000 title abstract description 25
- 238000000034 method Methods 0.000 title abstract description 15
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 title description 12
- 229910052757 nitrogen Inorganic materials 0.000 title description 8
- ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 abstract description 38
- 238000004519 manufacturing process Methods 0.000 abstract description 14
- 239000010440 gypsum Substances 0.000 abstract description 10
- 229910052602 gypsum Inorganic materials 0.000 abstract description 10
- 239000000618 nitrogen fertilizer Substances 0.000 abstract description 10
- 238000005469 granulation Methods 0.000 abstract description 9
- 230000003179 granulation Effects 0.000 abstract description 9
- 239000000725 suspension Substances 0.000 abstract description 7
- 238000006243 chemical reaction Methods 0.000 abstract description 5
- 238000000926 separation method Methods 0.000 abstract description 3
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000012530 fluid Substances 0.000 abstract 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 22
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 description 21
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 21
- 239000011593 sulfur Substances 0.000 description 21
- 229910052717 sulfur Inorganic materials 0.000 description 21
- 238000005576 amination reaction Methods 0.000 description 18
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 15
- BNJOQKFENDDGSC-UHFFFAOYSA-N octadecanedioic acid Chemical compound OC(=O)CCCCCCCCCCCCCCCCC(O)=O BNJOQKFENDDGSC-UHFFFAOYSA-N 0.000 description 11
- 229910021529 ammonia Inorganic materials 0.000 description 10
- 230000003993 interaction Effects 0.000 description 8
- ZHJGWYRLJUCMRT-UHFFFAOYSA-N 5-[6-[(4-methylpiperazin-1-yl)methyl]benzimidazol-1-yl]-3-[1-[2-(trifluoromethyl)phenyl]ethoxy]thiophene-2-carboxamide Chemical compound C=1C=CC=C(C(F)(F)F)C=1C(C)OC(=C(S1)C(N)=O)C=C1N(C1=C2)C=NC1=CC=C2CN1CCN(C)CC1 ZHJGWYRLJUCMRT-UHFFFAOYSA-N 0.000 description 6
- 229910019142 PO4 Inorganic materials 0.000 description 6
- NFJCQBGAUBIGKV-UHFFFAOYSA-N nitro dihydrogen phosphate Chemical compound OP(O)(=O)O[N+]([O-])=O NFJCQBGAUBIGKV-UHFFFAOYSA-N 0.000 description 6
- 239000010452 phosphate Substances 0.000 description 6
- 238000000354 decomposition reaction Methods 0.000 description 5
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 5
- 238000009434 installation Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 238000010586 diagram Methods 0.000 description 3
- 239000008187 granular material Substances 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 2
- 229910002651 NO3 Inorganic materials 0.000 description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
- 235000011941 Tilia x europaea Nutrition 0.000 description 2
- -1 anhydrous gypsum anhydride Chemical class 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 238000010924 continuous production Methods 0.000 description 2
- 239000004571 lime Substances 0.000 description 2
- 238000006386 neutralization reaction Methods 0.000 description 2
- 229910017604 nitric acid Inorganic materials 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- 101100460157 Drosophila melanogaster nenya gene Proteins 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- WZLMXYBCAZZIRQ-UHFFFAOYSA-N [N].[P].[K] Chemical compound [N].[P].[K] WZLMXYBCAZZIRQ-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 1
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 1
- 235000011130 ammonium sulphate Nutrition 0.000 description 1
- 150000008064 anhydrides Chemical class 0.000 description 1
- 235000013405 beer Nutrition 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Inorganic materials [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 1
- 101150116749 chuk gene Proteins 0.000 description 1
- 238000012733 comparative method Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical class [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 159000000003 magnesium salts Chemical class 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 125000002467 phosphate group Chemical group [H]OP(=O)(O[H])O[*] 0.000 description 1
- 159000000001 potassium salts Chemical class 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 150000004685 tetrahydrates Chemical class 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B11/00—Fertilisers produced by wet-treating or leaching raw materials either with acids in such amounts and concentrations as to yield solutions followed by neutralisation, or with alkaline lyes
- C05B11/04—Fertilisers produced by wet-treating or leaching raw materials either with acids in such amounts and concentrations as to yield solutions followed by neutralisation, or with alkaline lyes using mineral acid
- C05B11/06—Fertilisers produced by wet-treating or leaching raw materials either with acids in such amounts and concentrations as to yield solutions followed by neutralisation, or with alkaline lyes using mineral acid using nitric acid (nitrophosphates)
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C1/00—Ammonium nitrate fertilisers
- C05C1/02—Granulation; Pelletisation; Stabilisation; Colouring
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C5/00—Fertilisers containing other nitrates
- C05C5/04—Fertilisers containing other nitrates containing calcium nitrate
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/10—Solid or semi-solid fertilisers, e.g. powders
- C05G5/12—Granules or flakes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Fertilizers (AREA)
Abstract
Способ получения серосодержащего азотного удобрения, в котором поддают взаимодействию нитрат кальция в смесителе с серосодержащим соединением с образованием суспензии, содержащей безводный ангидрит гипса, и гранулируют полученную суспензию.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102004055648A DE102004055648A1 (de) | 2004-11-12 | 2004-11-12 | Verfahren und Vorrichtung zur Gewinnung schwefelhaltiger Stickstoffdünger |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UA89507C2 true UA89507C2 (ru) | 2010-02-10 |
Family
ID=35945249
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UAA200705193A UA89507C2 (ru) | 2004-11-12 | 2005-08-11 | Способ и устройство для получения серосодержащих азотных удобрений |
Country Status (7)
| Country | Link |
|---|---|
| EP (1) | EP1817268B1 (ru) |
| DE (1) | DE102004055648A1 (ru) |
| ES (1) | ES2623858T3 (ru) |
| PL (1) | PL1817268T4 (ru) |
| RU (1) | RU2400459C2 (ru) |
| UA (1) | UA89507C2 (ru) |
| WO (1) | WO2006050936A1 (ru) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4510620B2 (ja) | 2002-07-08 | 2010-07-28 | コーニンクレッカ フィリップス エレクトロニクス エヌ ヴィ | ガラス成分を有する電灯 |
| CN101348401B (zh) * | 2008-09-03 | 2011-07-13 | 山西省交城红星化工有限公司 | 硝酸铵钙包衣肥的制备方法 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB366035A (en) * | 1929-07-26 | 1932-01-27 | Ruhrchemie Ag | Process for the production of a solid non-hygroscopic ammonium sulphate saltpetre |
| GB800208A (en) * | 1955-04-01 | 1958-08-20 | Fisons Ltd | Granular products |
| NL6802841A (ru) * | 1968-02-29 | 1969-09-02 | ||
| NL6818164A (ru) * | 1968-12-18 | 1970-06-22 | ||
| AT306754B (de) * | 1971-03-29 | 1973-04-25 | Chemie Linz Ag | Überwiegend aus freiem Ammonnitrat bestehendes, granuliertes, gespritztes oder geprilltes Düngemittel |
| US5098461A (en) * | 1989-12-28 | 1992-03-24 | Tennessee Valley Authority | Phosphatic and nitrogen fertilizers via HNO3 processing |
| WO2001098233A1 (en) * | 2000-06-20 | 2001-12-27 | Norsk Hydro Asa | Process for producing a ns-fertilizer |
| RU2186751C1 (ru) * | 2001-02-16 | 2002-08-10 | Серебряков Александр Иванович | Способ получения сложного удобрения, содержащего азот, кальций и серу |
-
2004
- 2004-11-12 DE DE102004055648A patent/DE102004055648A1/de not_active Withdrawn
-
2005
- 2005-08-11 UA UAA200705193A patent/UA89507C2/ru unknown
- 2005-11-08 WO PCT/EP2005/012028 patent/WO2006050936A1/de active Search and Examination
- 2005-11-08 RU RU2007117570/15A patent/RU2400459C2/ru active
- 2005-11-08 PL PL05802397T patent/PL1817268T4/pl unknown
- 2005-11-08 ES ES05802397.9T patent/ES2623858T3/es active Active
- 2005-11-08 EP EP05802397.9A patent/EP1817268B1/de active Active
Also Published As
| Publication number | Publication date |
|---|---|
| WO2006050936A1 (de) | 2006-05-18 |
| DE102004055648A1 (de) | 2006-05-18 |
| EP1817268B1 (de) | 2017-01-04 |
| ES2623858T3 (es) | 2017-07-12 |
| RU2007117570A (ru) | 2008-12-20 |
| RU2400459C2 (ru) | 2010-09-27 |
| PL1817268T3 (pl) | 2017-07-31 |
| PL1817268T4 (pl) | 2017-07-31 |
| EP1817268A1 (de) | 2007-08-15 |
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