UA81221C2 - Process and plant for the heterogeneous synthesis of chemical compounds - Google Patents
Process and plant for the heterogeneous synthesis of chemical compounds Download PDFInfo
- Publication number
- UA81221C2 UA81221C2 UA2003098878A UA2003098878A UA81221C2 UA 81221 C2 UA81221 C2 UA 81221C2 UA 2003098878 A UA2003098878 A UA 2003098878A UA 2003098878 A UA2003098878 A UA 2003098878A UA 81221 C2 UA81221 C2 UA 81221C2
- Authority
- UA
- Ukraine
- Prior art keywords
- reaction zone
- reaction
- heat exchange
- fed
- differs
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 30
- 238000003786 synthesis reaction Methods 0.000 title claims abstract description 22
- 230000015572 biosynthetic process Effects 0.000 title claims abstract description 21
- 150000001875 compounds Chemical class 0.000 title abstract description 9
- 238000006243 chemical reaction Methods 0.000 claims abstract description 113
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 66
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 32
- 239000003054 catalyst Substances 0.000 claims abstract description 18
- 229910021529 ammonia Inorganic materials 0.000 claims abstract description 16
- 239000000376 reactant Substances 0.000 claims abstract description 15
- 230000003197 catalytic effect Effects 0.000 claims abstract description 5
- 239000003153 chemical reaction reagent Substances 0.000 claims description 18
- 238000009434 installation Methods 0.000 claims description 14
- 239000011541 reaction mixture Substances 0.000 claims description 13
- 239000002826 coolant Substances 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims 2
- 239000012530 fluid Substances 0.000 abstract description 7
- 238000010586 diagram Methods 0.000 description 5
- 239000000126 substance Substances 0.000 description 4
- -1 methanol and ammonia Chemical class 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 238000009826 distribution Methods 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 238000009776 industrial production Methods 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 238000005476 soldering Methods 0.000 description 1
- 238000001308 synthesis method Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/02—Preparation, purification or separation of ammonia
- C01C1/04—Preparation of ammonia by synthesis in the gas phase
- C01C1/0405—Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst
- C01C1/0417—Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst characterised by the synthesis reactor, e.g. arrangement of catalyst beds and heat exchangers in the reactor
- C01C1/0423—Cold wall reactors
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/0207—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly horizontal
- B01J8/0214—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly horizontal in a cylindrical annular shaped bed
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/0285—Heating or cooling the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
- B01J8/0403—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal
- B01J8/0407—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal through two or more cylindrical annular shaped beds
- B01J8/0415—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal through two or more cylindrical annular shaped beds the beds being superimposed one above the other
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
- B01J8/0496—Heating or cooling the reactor
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/02—Preparation, purification or separation of ammonia
- C01C1/04—Preparation of ammonia by synthesis in the gas phase
- C01C1/0405—Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/15—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
- C07C29/151—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases
- C07C29/152—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases characterised by the reactor used
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
- F28D9/00—Heat-exchange apparatus having stationary plate-like or laminated conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
- F28D9/0006—Heat-exchange apparatus having stationary plate-like or laminated conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the plate-like or laminated conduits being enclosed within a pressure vessel
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
- B01J2208/0015—Plates; Cylinders
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00309—Controlling the temperature by indirect heat exchange with two or more reactions in heat exchange with each other, such as an endothermic reaction in heat exchange with an exothermic reaction
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/19—Details relating to the geometry of the reactor
- B01J2219/194—Details relating to the geometry of the reactor round
- B01J2219/1941—Details relating to the geometry of the reactor round circular or disk-shaped
- B01J2219/1943—Details relating to the geometry of the reactor round circular or disk-shaped cylindrical
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Fluid Mechanics (AREA)
- Inorganic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Thermal Sciences (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP01126840A EP1310475A1 (en) | 2001-11-11 | 2001-11-11 | Process and plant for the heterogeneous synthesis of chemical compounds |
| PCT/EP2002/011027 WO2003042143A1 (en) | 2001-11-11 | 2002-10-02 | Process and plant for the heterogeneous synthesis of chemical compounds |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UA81221C2 true UA81221C2 (en) | 2007-12-25 |
Family
ID=8179218
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UA2003098878A UA81221C2 (en) | 2001-11-11 | 2002-02-10 | Process and plant for the heterogeneous synthesis of chemical compounds |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US6946494B2 (xx) |
| EP (2) | EP1310475A1 (xx) |
| CN (1) | CN1305822C (xx) |
| AR (1) | AR037344A1 (xx) |
| AT (1) | ATE468312T1 (xx) |
| AU (1) | AU2002363759B2 (xx) |
| BR (2) | BR0209799A (xx) |
| CA (1) | CA2433846C (xx) |
| DE (1) | DE60236448D1 (xx) |
| EG (1) | EG23247A (xx) |
| MX (1) | MXPA03006821A (xx) |
| MY (1) | MY131898A (xx) |
| RU (1) | RU2310641C2 (xx) |
| UA (1) | UA81221C2 (xx) |
| WO (1) | WO2003042143A1 (xx) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1153653A1 (en) * | 2000-05-11 | 2001-11-14 | Methanol Casale S.A. | Reactor for exothermic or endothermic heterogeneous reactions |
| EP1221339A1 (en) * | 2001-01-05 | 2002-07-10 | Methanol Casale S.A. | Catalytic reactor with heat exchanger for exothermic and endothermic heterogeneous chemical reactions |
| EP1236505A1 (en) * | 2001-02-27 | 2002-09-04 | Methanol Casale S.A. | Method for carrying out chemical reactions in pseudo-isothermal conditions |
| MX2007001173A (es) * | 2004-01-15 | 2007-09-25 | Methanol Casale Sa | Reactor catalitico de lecho fijo. |
| CN102247792A (zh) * | 2011-04-30 | 2011-11-23 | 甘肃银光聚银化工有限公司 | 一种新型多相搅拌反应器 |
| EP3212319A1 (en) * | 2014-10-30 | 2017-09-06 | SABIC Global Technologies B.V. | Reactor comprising radially placed cooling plates and methods of using same |
| EP3050849A1 (en) | 2015-01-27 | 2016-08-03 | Casale SA | A process for the synthesis of ammonia |
| MX2018015211A (es) * | 2016-06-21 | 2019-04-25 | Topsoe Haldor As | Convertidor de flujo axial/radial. |
| EP3401006A1 (en) * | 2017-05-11 | 2018-11-14 | Casale Sa | Multi-bed catalytic converter with inter-bed cooling |
| AR113649A1 (es) * | 2017-12-20 | 2020-05-27 | Haldor Topsoe As | Convertidor de flujo axial enfriado |
| AR113648A1 (es) | 2017-12-20 | 2020-05-27 | Haldor Topsoe As | Convertidor de flujo axial adiabático |
| WO2020156994A1 (en) * | 2019-02-01 | 2020-08-06 | Haldor Topsøe A/S | Use of plate heat exchangers in combination with exothermal reactors |
| CN109999749A (zh) * | 2019-03-15 | 2019-07-12 | 中国煤层气集团有限公司 | 两相或多相反应容器 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2153437B2 (de) | 1971-10-27 | 1974-11-21 | Metallgesellschaft Ag, 6000 Frankfurt | Reaktor zur Herstellung von Methanol |
| DE3201776A1 (de) * | 1982-01-21 | 1983-09-08 | Krupp-Koppers Gmbh, 4300 Essen | Verfahren zur gleichzeitigen erzeugung von methanol- und ammoniak-synthesegas. |
| GB2203427B (en) | 1986-07-24 | 1990-05-09 | Inst Neftechimicheskogo Sintez | Method of preparing methanol |
| DE19605572A1 (de) * | 1996-02-15 | 1997-08-21 | Metallgesellschaft Ag | Verfahren zum Erzeugen von Methanol |
-
2001
- 2001-11-11 EP EP01126840A patent/EP1310475A1/en not_active Withdrawn
-
2002
- 2002-02-10 UA UA2003098878A patent/UA81221C2/uk unknown
- 2002-09-23 MY MYPI20023523A patent/MY131898A/en unknown
- 2002-10-02 BR BR0209799-0A patent/BR0209799A/pt not_active IP Right Cessation
- 2002-10-02 AU AU2002363759A patent/AU2002363759B2/en not_active Ceased
- 2002-10-02 CA CA2433846A patent/CA2433846C/en not_active Expired - Fee Related
- 2002-10-02 MX MXPA03006821A patent/MXPA03006821A/es active IP Right Grant
- 2002-10-02 WO PCT/EP2002/011027 patent/WO2003042143A1/en not_active Application Discontinuation
- 2002-10-02 EP EP02802977A patent/EP1444186B1/en not_active Expired - Lifetime
- 2002-10-02 BR BRPI0209799-0A patent/BRPI0209799B1/pt unknown
- 2002-10-02 AT AT02802977T patent/ATE468312T1/de not_active IP Right Cessation
- 2002-10-02 DE DE60236448T patent/DE60236448D1/de not_active Expired - Lifetime
- 2002-10-02 RU RU2003128885/04A patent/RU2310641C2/ru not_active IP Right Cessation
- 2002-10-02 CN CNB028039122A patent/CN1305822C/zh not_active Expired - Fee Related
- 2002-10-02 US US10/471,350 patent/US6946494B2/en not_active Expired - Lifetime
- 2002-11-08 AR ARP020104290A patent/AR037344A1/es active IP Right Grant
- 2002-11-10 EG EG2002111228A patent/EG23247A/xx active
Also Published As
| Publication number | Publication date |
|---|---|
| CA2433846C (en) | 2010-08-17 |
| US6946494B2 (en) | 2005-09-20 |
| EG23247A (en) | 2004-09-29 |
| MY131898A (en) | 2007-09-28 |
| ATE468312T1 (de) | 2010-06-15 |
| DE60236448D1 (de) | 2010-07-01 |
| EP1310475A1 (en) | 2003-05-14 |
| CA2433846A1 (en) | 2003-05-22 |
| BR0209799A (pt) | 2004-06-01 |
| MXPA03006821A (es) | 2003-12-04 |
| AU2002363759B2 (en) | 2008-06-05 |
| RU2310641C2 (ru) | 2007-11-20 |
| CN1498199A (zh) | 2004-05-19 |
| BRPI0209799B1 (pt) | 2019-07-02 |
| WO2003042143A1 (en) | 2003-05-22 |
| CN1305822C (zh) | 2007-03-21 |
| RU2003128885A (ru) | 2005-04-10 |
| US20040204507A1 (en) | 2004-10-14 |
| EP1444186B1 (en) | 2010-05-19 |
| EP1444186A1 (en) | 2004-08-11 |
| AR037344A1 (es) | 2004-11-03 |
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