TWI569813B - Plant polysaccharide extract for moisturizer - Google Patents

Plant polysaccharide extract for moisturizer Download PDF

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TWI569813B
TWI569813B TW099117540A TW99117540A TWI569813B TW I569813 B TWI569813 B TW I569813B TW 099117540 A TW099117540 A TW 099117540A TW 99117540 A TW99117540 A TW 99117540A TW I569813 B TWI569813 B TW I569813B
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plant
polysaccharide
polysaccharide extract
extract
solution
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TW201143810A (en
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林先文
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聯群生技有限公司
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Description

用於保濕之植物多醣體萃取物Plant polysaccharide extract for moisturizing

本發明係關於一種用於保濕之植物多醣體[polysaccharide]萃取物;特別是關於自植物種子或植物種皮以適當萃取方式取得之多醣體萃取物。The present invention relates to a plant polysaccharide extract for moisturizing; in particular to a polysaccharide extract obtained by appropriate extraction from plant seeds or plant seed coats.

習用以植物種子進行萃取方法及其萃取物,如美國專利第4,980,186號之〝假塑性黃芥末樹膠[Pseudoplastic yellow mustard gum]〞發明專利案,其揭示一種自黃芥末種子萃取樹膠方法,其包含:首先將該黃芥末種子以逐漸增加溫度[elevated temperature]的水溶液逐步進行萃取處理,以取得一萃取物溶液。A method for extracting plant seeds and extracts thereof, such as the Pseudoplastic yellow mustard gum method of the U.S. Patent No. 4,980,186, which discloses a method for extracting gum from yellow mustard seeds, comprising: First, the yellow mustard seeds are gradually subjected to extraction treatment with an aqueous solution of increasing temperature to obtain an extract solution.

接著,將該第4,980,186號之萃取物溶液以適當機械性分離方式進行分離處理,以取得一水性萃取物[aqueous extract]。此時,該機械性分離方式包含有孔離心[perforated centrifuge]分離技術及狹縫離心[slitted centrifuge]分離技術等。將該水性萃取物以沉澱[precipitation]及乾燥[drying]方式進行適當處理。Next, the extract solution of No. 4,980,186 is subjected to separation treatment in an appropriate mechanical separation manner to obtain an aqueous extract. At this time, the mechanical separation method includes a perforated centrifuge separation technique and a slitted centrifuge separation technique. The aqueous extract was appropriately treated in the form of precipitation and drying.

目前許多含於各種植物種子之特定化合物[例如:多醣體或其它化合物]可能具有高度經濟價值,且需要自該植物種子適當取出該具高度經濟價值之化合物,在避免發生物理性或化學性破壞之下將該化合物再進行適當加工形成高經濟價值的產品。Many specific compounds (eg, polysaccharides or other compounds) present in various plant seeds may be of high economic value and require the removal of such highly economically valuable compounds from the plant seeds in order to avoid physical or chemical damage. The compound is then further processed to form a product of high economic value.

舉例而言,含於各種植物種子之多醣體或其它化合物可應用或加入於化妝品或保養品。然而,含於植物種子之化合物需要確認分析其特性及經濟價值,方可瞭解如何萃取及應用該化合物。因此,目前在各種植物種子中存在許多需要取出具高經濟價值化合物之需求。For example, polysaccharides or other compounds contained in various plant seeds can be applied or added to cosmetics or skin care products. However, compounds containing plant seeds need to be confirmed for their properties and economic value in order to understand how to extract and apply the compound. Therefore, there is currently a need in many plant seeds for the need to remove compounds of high economic value.

有鑑於此,本發明為了滿足上述需求,其提供一種用於保濕之植物多醣體萃取物,其選擇自植物種子或植物種皮以適當萃取方式取得具保濕功能之多醣體萃取物,以達成萃取可用於保濕多醣體之目的。In view of the above, in order to meet the above needs, the present invention provides a plant polysaccharide extract for moisturizing, which is selected from a plant seed or a plant seed coat to obtain a moisturizing polysaccharide extract by appropriate extraction to obtain an extract. For the purpose of moisturizing polysaccharides.

本發明之主要目的係提供一種用於保濕之植物多醣體萃取物,其選擇自植物種子或植物種皮以適當萃取方式取得具保濕功能之多醣體萃取物,以達成萃取可用於保濕多醣體之目的。The main object of the present invention is to provide a plant polysaccharide extract for moisturizing, which is selected from a plant seed or a plant seed coat to obtain a moisturizing polysaccharide extract by appropriate extraction to achieve the purpose of extracting and moisturizing the polysaccharide. .

為了達成上述目的,本發明之用於保濕之植物多醣體萃取物包含至少一種多醣體,該多醣體存在於一植物種子或一植物種皮,以水溶液萃取方式取得一萃取溶液,再自該萃取溶液以適當分離技術取得一初步多醣體溶液,再將該初步多醣體溶液製成該多醣體萃取物。In order to achieve the above object, the plant polysaccharide extract for moisturizing of the present invention comprises at least one polysaccharide body which is present in a plant seed or a plant seed coat, obtains an extraction solution by aqueous solution extraction, and then extracts the solution from the aqueous solution. A preliminary polysaccharide solution is obtained by a suitable separation technique, and the preliminary polysaccharide solution is then made into the polysaccharide extract.

本發明較佳實施例之該多醣體包含鼠李糖、阿拉伯膠糖、半乳糖、葡萄糖、甘露糖及木質糖等中性糖。In the preferred embodiment of the invention, the polysaccharide comprises neutral sugars such as rhamnose, gum arabic, galactose, glucose, mannose and xylose.

本發明較佳實施例之該植物種子或植物種皮為芸香科植物種子或植物種皮。In the preferred embodiment of the invention, the plant seed or plant seed coat is a Rutaceae plant seed or a plant seed coat.

本發明較佳實施例之該萃取溶液以冷水萃取方式自該植物種子或植物種皮萃取而取得。In the preferred embodiment of the invention, the extraction solution is obtained by extraction from the plant seed or plant seed coat by cold water extraction.

本發明較佳實施例之該初步多醣體溶液以離心分離技術及過濾技術自該萃取溶液取得。In the preferred embodiment of the present invention, the preliminary polysaccharide solution is obtained from the extraction solution by a centrifugal separation technique and a filtration technique.

本發明較佳實施例之該初步多醣體溶液以冷凍乾燥法製成該多醣體萃取物。The preliminary polysaccharide solution of the preferred embodiment of the invention is lyophilized to produce the polysaccharide extract.

本發明較佳實施例之該多醣體萃取物為一多醣體粉末。In the preferred embodiment of the invention, the polysaccharide extract is a polysaccharide powder.

為了充分瞭解本發明,於下文將例舉較佳實施例並配合所附圖式作詳細說明,且其並非用以限定本發明。In order to fully understand the present invention, the preferred embodiments of the present invention are described in detail below and are not intended to limit the invention.

本發明較佳實施例之用於保濕之植物多醣體萃取物可應用於各種化妝品或保養品,但其並非用以限定本發明之範圍。另外,本發明較佳實施例之用於保濕之植物多醣體萃取物可製成各種形式的產品,例如:粉末產品,但其並非用以限定本發明之範圍。The plant polysaccharide extract for moisturizing according to a preferred embodiment of the present invention can be applied to various cosmetic or skin care products, but it is not intended to limit the scope of the present invention. Further, the plant polysaccharide extract for moisturizing according to a preferred embodiment of the present invention can be made into various forms of products, such as powder products, but it is not intended to limit the scope of the present invention.

第1圖揭示本發明較佳實施例在製造用於保濕之植物多醣體萃取物之流程示意圖。請參照第1圖所示,本發明較佳實施例之用於保濕之植物多醣體萃取物製造方法包含第一步驟S1:以適當方式製備一植物種子或一植物種皮,且以適當方式保存該植物種子或植物種皮。本發明較佳實施例之該植物種子或植物種皮為芸香科[Rutaceae]植物種子或植物種皮,例如:包含柚子、白柚子等,但其並非用以限制本發明。BRIEF DESCRIPTION OF THE DRAWINGS Figure 1 is a schematic view showing the flow of a plant polysaccharide extract for moisturizing according to a preferred embodiment of the present invention. Referring to Fig. 1, a method for producing a plant polysaccharide extract for moisturizing according to a preferred embodiment of the present invention comprises a first step S1: preparing a plant seed or a plant seed coat in an appropriate manner, and storing the plant in an appropriate manner. Plant seeds or plant seed coats. In the preferred embodiment of the present invention, the plant seed or plant seed coat is a Rutaceae plant seed or plant seed coat, for example, comprising grapefruit, white grapefruit, etc., but it is not intended to limit the present invention.

請再參照第1圖所示,本發明較佳實施例之用於保濕之植物多醣體萃取物製造方法包含第二步驟S2:自該植物種子或植物種皮以水溶液萃取方式萃取一預定時間,以取得一萃取溶液,且該萃取溶液為種子產生的黏液[seed mucilage]。本發明較佳實施例之該萃取溶液以冷水萃取方式取得,其中該冷水之溫度低於室溫[例如:25℃],但其並非用以限制本發明。Referring to FIG. 1 again, the method for producing a plant polysaccharide extract for moisturizing according to a preferred embodiment of the present invention comprises a second step S2: extracting from the plant seed or plant seed coat by aqueous solution extraction for a predetermined time, An extraction solution is obtained, and the extraction solution is a seed mucilage [seed mucilage]. In the preferred embodiment of the present invention, the extraction solution is obtained by cold water extraction, wherein the temperature of the cold water is lower than room temperature [for example, 25 ° C], but it is not intended to limit the present invention.

請再參照第1圖所示,本發明較佳實施例之用於保濕之植物多醣體萃取物製造方法包含第三步驟S3:自該萃取溶液以適當分離[separation]技術取得一初步多醣體溶液[preliminary polysaccharide liquid]。本發明較佳實施例之該初步多醣體溶液以離心[centrifugation]技術[例如:離心機[centrifugal device]]及過濾[filtration]技術[例如:過濾裝置]取得。Referring to FIG. 1 again, the method for producing a plant polysaccharide extract for moisturizing according to a preferred embodiment of the present invention comprises a third step S3: obtaining a preliminary polysaccharide solution from the extraction solution by appropriate separation technique [separation] technique [preliminary polysaccharide liquid]. The preliminary polysaccharide solution of the preferred embodiment of the present invention is obtained by a centrifugation technique [e.g., a centrifuge device] and a filtration technique [e.g., a filtration device].

請再參照第1圖所示,本發明較佳實施例之用於保濕之植物多醣體萃取物製造方法包含第四步驟S4:將該初步多醣體溶液製成該多醣體萃取物。本發明較佳實施例之該多醣體萃取物包含至少一種多醣體,但其並非用以限制本發明。 Referring to FIG. 1 again, the method for producing a plant polysaccharide extract for moisturizing according to a preferred embodiment of the present invention comprises a fourth step S4: preparing the preliminary polysaccharide solution into the polysaccharide extract. The polysaccharide extract of the preferred embodiment of the invention comprises at least one polysaccharide, but it is not intended to limit the invention.

請再參照第1圖所示,本發明較佳實施例之該初步多醣體溶液以冷凍乾燥法〔freeze drying〕或冷凍真空乾燥法〔vacuum freeze drying〕製造加工該多醣體萃取物,以製成一多醣體產品。此時,本發明較佳實施例之該多醣體萃取物為一多醣體粉末。 Referring to FIG. 1 again, in the preferred embodiment of the present invention, the preliminary polysaccharide solution is processed by freeze drying or vacuum freeze drying to produce the polysaccharide extract. A polysaccharide product. At this time, the polysaccharide extract of the preferred embodiment of the present invention is a polysaccharide powder.

第2圖揭示本發明較佳實施例含用於保濕之植物多醣體萃取物之多醣體組成之成份分析示意圖。舉例而言,該植物種子或植物種皮為芸香科植物種子或植物種皮。請參照第2圖所示,本發明較佳實施例之該多醣體萃取物之多醣體取自柚子種子皮,由中性糖組成,其包含鼠李糖〔rhammose〕、阿拉伯膠糖〔arabinose〕、半乳糖〔galactose〕、葡萄糖〔glucose〕、甘露糖〔mannose〕及/或木質糖〔xylose〕等中性糖。 Fig. 2 is a schematic view showing the composition analysis of the polysaccharide composition of the plant polysaccharide extract for moisturizing according to a preferred embodiment of the present invention. For example, the plant seed or plant seed coat is a Rutaceae plant seed or a plant seed coat. Referring to Fig. 2, the polysaccharide of the polysaccharide extract of the preferred embodiment of the present invention is taken from grapefruit seed skin and composed of neutral sugar, which comprises rhammose and arabine. Neutral sugars such as galactose, glucose, mannose, and/or xylose.

請再參照第2圖所示,在多醣體組成之成份分析上,鼠李糖標示為A〔如箭頭所示〕、阿拉伯膠糖標示為B〔如箭頭所示〕、半乳糖標示為C〔如箭頭所示〕、葡萄糖標示為D〔如箭頭所示〕及甘露糖或木質糖標示為E〔如箭頭所示〕。 Please refer to Figure 2 again. In the analysis of the composition of polysaccharides, rhamnose is labeled as A (as indicated by the arrow), gum arabic is labeled as B (as indicated by the arrow), and galactose is labeled as C. As indicated by the arrow, glucose is labeled D (as indicated by the arrow) and mannose or xylose is labeled E (as indicated by the arrow).

前述較佳實施例僅舉例說明本發明及其技術特徵,該實施例之技術仍可適當進行各種實質等效修飾及/或替換方式予以實施;因此,本發明之權利範圍須視後附申請專利範圍所界定之範圍為準。 The foregoing preferred embodiments are merely illustrative of the invention and the technical features thereof, and the techniques of the embodiments can be carried out with various substantial equivalent modifications and/or alternatives; therefore, the scope of the invention is subject to the appended claims. The scope defined by the scope shall prevail.

S1...執行步驟S1. . . Steps

S2...執行步驟S2. . . Steps

S3...執行步驟S3. . . Steps

S4...執行步驟S4. . . Steps

第1圖:本發明較佳實施例在製造用於保濕之植物多醣體萃取物之流程示意圖。BRIEF DESCRIPTION OF THE DRAWINGS Fig. 1 is a schematic view showing the flow of a plant polysaccharide extract for moisturizing according to a preferred embodiment of the present invention.

第2圖:本發明較佳實施例含用於保濕之植物多醣體萃取物之多醣體組成之成份分析示意圖。Fig. 2 is a schematic view showing the composition analysis of the polysaccharide composition of the plant polysaccharide extract for moisturizing according to a preferred embodiment of the present invention.

S1...執行步驟S1. . . Steps

S2...執行步驟S2. . . Steps

S3...執行步驟S3. . . Steps

S4...執行步驟S4. . . Steps

Claims (10)

一種用於保濕之植物多醣體萃取物,其包含:至少一種多醣體,該多醣體存在於一植物種子或一植物種皮,以水溶液萃取方式取得一萃取溶液,再自該萃取溶液以適當分離技術取得一初步多醣體溶液,再將該初步多醣體溶液製成該多醣體萃取物,其特徵在於:該多醣體萃取物取自該植物種子或該植物種皮,且該植物種子或該植物種皮為芸香科植物種子或芸香科植物種皮,其中該芸香科植物種子或植物種皮選自柚子種子、柚子種子皮、白柚子種子或白柚子種子皮。 A plant polysaccharide extract for moisturizing, comprising: at least one polysaccharide body present in a plant seed or a plant seed coat, obtaining an extraction solution by aqueous solution extraction, and then extracting the solution from the extraction solution appropriately Obtaining a preliminary polysaccharide solution, and then preparing the preliminary polysaccharide solution into the polysaccharide extract, wherein the polysaccharide extract is taken from the plant seed or the plant seed coat, and the plant seed or the plant seed coat is A Rutaceae plant or a Rutaceae plant seed coat, wherein the Rutaceae plant seed or plant seed coat is selected from the group consisting of grapefruit seeds, grapefruit seed skin, white grapefruit seeds, or white grapefruit seed skin. 依申請專利範圍第1項所述之用於保濕之植物多醣體萃取物,其中該多醣體萃取物之多醣體由中性糖組成。 The plant polysaccharide extract for moisturizing according to claim 1, wherein the polysaccharide of the polysaccharide extract consists of neutral sugar. 依申請專利範圍第2項所述之用於保濕之植物多醣體萃取物,其中該多醣體包含中性糖之鼠李糖、阿拉伯膠糖、半乳糖、葡萄糖、甘露糖及/或木質糖。 The plant polysaccharide extract for moisturizing according to claim 2, wherein the polysaccharide comprises rhamnose, arabinose, galactose, glucose, mannose and/or xylose of neutral sugar. 依申請專利範圍第1項所述之用於保濕之植物多醣體萃取物,其中該植物多醣體萃取物添加於一化妝品或一保養品。 The plant polysaccharide extract for moisturizing according to claim 1, wherein the plant polysaccharide extract is added to a cosmetic or a skin care product. 依申請專利範圍第1項所述之用於保濕之植物多醣體萃取物,其中該萃取溶液以冷水萃取方式自該植物種子或植物種皮萃取而取得。 The plant polysaccharide extract for moisturizing according to claim 1, wherein the extraction solution is obtained by extracting from the plant seed or the plant seed coat by cold water extraction. 依申請專利範圍第1項所述之用於保濕之植物多醣體萃取物,其中該初步多醣體溶液以離心分離技術及過濾技術自該萃取溶液取得。 The plant polysaccharide extract for moisturizing according to claim 1, wherein the preliminary polysaccharide solution is obtained from the extraction solution by a centrifugal separation technique and a filtration technique. 依申請專利範圍第1項所述之用於保濕之植物多醣體萃取物,其中該初步多醣體溶液以冷凍乾燥法製成該多醣體萃取物。 The plant polysaccharide extract for moisturizing according to claim 1, wherein the preliminary polysaccharide solution is freeze-dried to prepare the polysaccharide extract. 依申請專利範圍第1項所述之用於保濕之植物多醣體萃取物,其中該多醣體萃取物為一多醣體粉末。 The plant polysaccharide extract for moisturizing according to claim 1, wherein the polysaccharide extract is a polysaccharide powder. 一種植物多醣體萃取物之用途,其中該植物多醣體萃取物取自芸香科植物種子或芸香科植物種皮,且其用於皮膚保濕。 A use of a plant polysaccharide extract, wherein the plant polysaccharide extract is taken from a Rutaceae plant or a Rutaceae plant seed coat, and is used for skin moisturization. 依申請專利範圍第9項所述之植物多醣體萃取物之用途,其中該植物多醣體萃取物添加於一化妝品或一保養品。 The use of the plant polysaccharide extract according to claim 9, wherein the plant polysaccharide extract is added to a cosmetic or a skin care product.
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日本資生堂,「資生堂發現"柚子種子萃取物"有抑制皮膚老化效果—可修復造成皮膚老化的基底膜損傷,促進表皮透明質酸產生」,2006/12/26,資生堂(中國)官方網站,http://translate.googleusercontent.com/translate_c?anno=2&depth=1&h1=zh-TW&rur1=translate.google.com&s1=zh-CN&t1=zh-TW&u=http://www.shiseid... *

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