TW201440155A - Endpoint detection device and method of plasma treatment process - Google Patents

Endpoint detection device and method of plasma treatment process Download PDF

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TW201440155A
TW201440155A TW103102877A TW103102877A TW201440155A TW 201440155 A TW201440155 A TW 201440155A TW 103102877 A TW103102877 A TW 103102877A TW 103102877 A TW103102877 A TW 103102877A TW 201440155 A TW201440155 A TW 201440155A
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optical signal
signal strength
value
plasma processing
instantaneous
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TWI556340B (en
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Pian Yang
zhi-lin Huang
chao-hui Xi
Han Cao
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Advanced Micro Fab Equip Inc
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Abstract

The invention discloses an endpoint detection method of a plasma treatment process. The plasma treatment process comprises a plurality of periodical plasma treatment steps. The endpoint detection device includes collecting real-time optical signal strength with a specific wavelength in the plasma treatment process at regular intervals to obtain a plurality of real-time optical signal strength sampling values and establishing a real-time optical signal strength spectral line with periodicity; defining a flat area inside every period of the real-time optical signal strength spectral line; extracting an optical signal strength characteristic value in every flat area; establishing an optical signal strength characteristic spectral line according to the optical signal strength characteristic values; and determining an endpoint of the plasma treatment process according to the optical signal strength characteristic spectral line. The invention also provides an endpoint detection device of the plasma treatment process. The endpoint detection device and the endpoint detection method of the plasma treatment process can effectively improve the accuracy of the endpoint detection of a plasma periodical disturbance process.

Description

等離子體處理工藝的終點檢測裝置及方法 End point detecting device and method for plasma processing process

本發明涉及半導體製造技術領域,特別涉及一種等離子體處理工藝的終點檢測裝置及方法。 The present invention relates to the field of semiconductor manufacturing technology, and in particular, to an end point detecting device and method for a plasma processing process.

近年來,隨著半導體製造工藝的發展,對元件的集成度和性能要求越來越高,等離子體技術(Plasma Technology)在半導體製造領域中正起著舉足輕重的作用。等離子體技術通過使工藝氣體激發形成的等離子體被應用在許多半導體工藝中,如沉積工藝(如化學氣相沉積)、蝕刻工藝(如幹法蝕刻)等。對等離子體處理工藝來說,其準確度直接關係到元件的特徵尺寸。隨著半導體器件特徵尺寸縮小,以及半導體製造過程中所用的等離子體處理工藝步驟的數量和複雜性的迅速增加,對等離子體處理工藝控制的要求變得更加嚴格,這就需要採用即時監控的手段來控制工藝過程的關鍵階段。 In recent years, with the development of semiconductor manufacturing processes, the integration and performance requirements of components are becoming higher and higher, and Plasma Technology plays an important role in the field of semiconductor manufacturing. Plasma technology is applied to many semiconductor processes by plasma generated by excitation of process gases, such as deposition processes (such as chemical vapor deposition), etching processes (such as dry etching), and the like. For plasma processing, its accuracy is directly related to the feature size of the component. As the feature size of semiconductor devices shrinks and the number and complexity of plasma processing steps used in semiconductor manufacturing processes increase rapidly, the requirements for plasma processing process control become more stringent, requiring real-time monitoring To control the critical stages of the process.

以等離子體蝕刻工藝為例,在等離子體蝕刻過程中,一個關鍵的問題是當被蝕刻的介質層被蝕刻掉之後,應當及時停止等離子體蝕刻,以避免下層介質層受到等離子體的蝕刻而損傷,從而造成器件的失效。因此,精確判定等離子體蝕刻工藝終點(endpoint)以避免因蝕刻不足或蝕刻過度導致元器件失效就變得日益重要。現有技術中,通常採用光學發射光譜法(optical emission spectroscopy,OES)進行等離子體蝕刻終點檢測。OES技術主要是基於線上光譜檢測設備對等離子體發射出的光譜進行即時檢測,由於蝕刻到不同物質層光譜會出現明顯的變化,特別當到達是蝕刻終點時,因蝕刻的材料發生轉換,氣相的組成及被蝕刻薄膜都會發生化學變化,這種變化通過OES光譜信號的強度變化表現出來。因此,通過連續監測等離子體發射,就能夠用OES終點檢測方法來檢測出此變化並利用它來 確定薄膜被完全清除的時間。例如,當OES信號下降至預定閾值水準之下時,就利用這種轉變來觸發“終點”。因此,通過檢測蝕刻過程中蝕刻到不同層的物質時,反應物或生成物的發射譜線強度值,以此就能夠判斷蝕刻終點。例如美國專利US5565114公開了一種等離子體工藝中通過OES技術檢測終點的方法,通過先計算等離子體發光頻譜強度的總和平均值,然後計算總和平均值的差或是比值以決定蝕刻是否達到終端點。由此可知,通過OES技術能夠很好地實現了制程穩定的單一蝕刻步驟處理或有限分離蝕刻步驟的處理。 Taking the plasma etching process as an example, in the plasma etching process, a key problem is that after the etched dielectric layer is etched away, the plasma etching should be stopped in time to prevent the underlying dielectric layer from being damaged by plasma etching. , causing the device to fail. Therefore, it is increasingly important to accurately determine the end point of the plasma etch process to avoid component failure due to insufficient or excessive etch. In the prior art, plasma etch end point detection is usually performed by optical emission spectroscopy (OES). The OES technology is based on the on-line spectrum detection equipment to detect the spectrum emitted by the plasma in real time. Due to the etch to different material layers, the spectrum will change significantly, especially when the arrival is the end point of the etching, due to the conversion of the etched material, the gas phase Both the composition and the film being etched undergo chemical changes that are manifested by changes in the intensity of the OES spectral signal. Therefore, by continuously monitoring the plasma emission, the OES endpoint detection method can be used to detect this change and use it to Determine when the film is completely removed. For example, when the OES signal falls below a predetermined threshold level, this transition is utilized to trigger an "end point." Therefore, by detecting the emission line intensity value of the reactant or product when etching a substance to a different layer in the etching process, the etching end point can be judged. For example, U.S. Patent No. 5,565,114 discloses a method of detecting an end point by OES technique in a plasma process by first calculating the sum of the sums of the intensity spectra of the plasma light, and then calculating the difference or ratio of the mean values to determine whether the etching reaches the termination point. It can be seen that the process of the single etching step process or the limited separation etching step of the process stability can be well realized by the OES technology.

如今,對晶片進行深反應離子蝕刻以形成高深寬比結構(如矽通孔技術)正越來越受到廣泛的重視和研究,深反應離子蝕刻通常採用博世工藝(Bosch process)進行。而博世工藝是通過使等離子蝕刻工序和等離子沉積工序週期性地反復進行而對半導體晶片在垂直方向較深地進行蝕刻的工藝。博世工藝主要包括以下步驟:(1)蝕刻步驟,通常用含有SF6的混合氣體進行化學反應離子蝕刻;(2)聚合物沉積鈍化步驟,通常用含有C4H8的混合氣體在孔洞內側面形成氟碳聚合物層,以使下一個週期的蝕刻步驟中化學反應離子蝕刻時,SF6氣體不會對側壁的聚合物進行蝕刻或者蝕刻速率非常慢;蝕刻步驟和沉積步驟交替循環進行,直到深孔蝕刻完成。由於博世工藝採用交替重複進行各向同性蝕刻和聚合物沉積工藝,而其中蝕刻和沉積步驟所使用的等離子體條件(如工藝氣體類型、壓力、RF功率等)並不相同,因此在進行博世工藝過程中蝕刻步驟和沉積步驟的等離子體發射光譜就會顯著不同。如圖1所示,將常規的OES技術應用於具有快速且週期性的等離子體擾動特性的博世工藝會導致週期性的終點軌跡,容易發生誤判等離子體發射強度的改變,因此其無法準確檢測終點。 Nowadays, deep reactive ion etching of wafers to form high aspect ratio structures (such as germanium via technology) is gaining more and more attention and research. Deep reactive ion etching is usually carried out by the Bosch process. The Bosch process is a process in which the semiconductor wafer is etched deep in the vertical direction by periodically repeating the plasma etching process and the plasma deposition process. The Bosch process mainly includes the following steps: (1) an etching step, usually a chemical reaction ion etching using a mixed gas containing SF 6 ; (2) a polymer deposition passivation step, usually using a mixed gas containing C 4 H 8 in the inner side of the hole Forming the fluorocarbon polymer layer so that the chemical reaction ion etching in the etching process of the next cycle, the SF 6 gas does not etch the polymer of the sidewall or the etching rate is very slow; the etching step and the deposition step are alternately cycled until Deep hole etching is completed. Since the Bosch process uses alternating repeating isotropic etching and polymer deposition processes, and the plasma conditions (such as process gas type, pressure, RF power, etc.) used in the etching and deposition steps are not the same, the Bosch process is performed. The plasma emission spectra of the etching step and the deposition step in the process are significantly different. As shown in Figure 1, the application of conventional OES technology to Bosch processes with fast and periodic plasma disturbance characteristics leads to periodic end-point trajectories, which are prone to misjudgment of plasma emission intensity changes, so that it is impossible to accurately detect the end point. .

為解決上述技術問題,美國專利US7101805公開了一種在交替循環蝕刻處理或分時多工處理期間確立終點的方法。其利用公知的光發射光譜測定技術(OES技術)檢測等離子體發射強度的變化,並利用包絡跟隨器演算法從等離子體發射強度的複雜波形中提取幅度資訊。其中包絡線跟隨器演算法採用多個峰值檢測演算法,按照循環方式依次重定。也即是說,該專利中是利用發射峰值來形成包絡線,之後根據包絡線軌跡確 定終點產生的時間,構建終點對策。然而,在實際操作中,由於峰值一般是由該工藝步驟開始的時候RF射頻源射出而產生的,其本身也是等離子體最不穩定的區域,因此容易發生偏差,以其形成的包絡線對終點檢測一般不敏感。此外,資料的採集頻率一般是固定的,但在實際採樣過程中由於等離子體功率、氣體以及終端檢測的採樣時間的同步性在每個週期都會有不同,很可能會發生延時,從而造成採集點的位置會和最大值不重合。如果延時的時間不同,則在不同的採樣時間可能會採集到峰值左邊的資料點,峰值或峰值右邊的資料點,由於在峰值兩側的資料值相對的變化量非常大,從而使得形成的包絡線抖動非常大。因此採用峰值所形成的包絡線來進行終點檢測的話準確性不佳,特別是當蝕刻面積較小時,根本無法用來進行終點檢測。 In order to solve the above technical problems, U.S. Patent No. 7,101,805 discloses a method of establishing an end point during an alternate cycle etching process or a time division multiplexing process. It uses known light emission spectrometry (OES) to detect changes in plasma emission intensity, and uses an envelope follower algorithm to extract amplitude information from complex waveforms of plasma emission intensity. The envelope follower algorithm uses multiple peak detection algorithms and is sequentially reset according to the cyclic method. That is to say, in this patent, the emission peak is used to form the envelope, and then according to the envelope trajectory. The time at which the endpoint is generated is constructed to determine the endpoint. However, in practice, since the peak is generally generated by the RF source being emitted at the beginning of the process step, it is also the most unstable region of the plasma, so it is prone to deviation, and the envelope-to-end point formed by it Detection is generally not sensitive. In addition, the data acquisition frequency is generally fixed, but in the actual sampling process, the synchronization of the plasma power, gas and sampling time of the terminal detection will be different in each cycle, and it is likely that a delay will occur, resulting in a collection point. The position will not coincide with the maximum value. If the delay time is different, the data point to the left of the peak may be collected at different sampling times, and the data point to the right of the peak or peak value, because the relative value of the data values on both sides of the peak is relatively large, so that the envelope formed Line jitter is very large. Therefore, the accuracy of the end point detection using the envelope formed by the peak is not good, especially when the etching area is small, it cannot be used for the end point detection.

因此,如何實現一種準確性高,靈活性大的終點檢測方法,以準確找到具有交替循環步驟的等離子體處理工藝的終點,成為應用等離子體技術的半導體製造工藝中的難點問題。 Therefore, how to realize an endpoint detection method with high accuracy and flexibility to accurately find the end point of the plasma treatment process with alternating cycle steps becomes a difficult problem in the semiconductor manufacturing process using plasma technology.

本發明的主要目的在於克服現有技術的缺陷,提供一種等離子體處理工藝的終點檢測裝置及方法,以提高利用OES方法進行交替循環等離子體處理工藝終點檢測的靈敏性和準確性。 The main object of the present invention is to overcome the deficiencies of the prior art and to provide an end point detecting device and method for a plasma processing process to improve the sensitivity and accuracy of the end point detection of the alternating cycle plasma processing process by the OES method.

為達成上述目的,本發明提供一種等離子體處理工藝的終點檢測方法,所述等離子體處理工藝包括多個週期性的等離子體處理步驟,所述終點檢測方法包括:以一定時間間隔採集所述等離子體處理工藝過程中特定波長的即時光信號強度以獲取多個即時光信號強度取樣值並建立具有週期性的即時光信號強度譜線,所述即時光信號強度與所述等離子體處理工藝的反應物組分濃度或產物組分濃度對應;在所述即時光信號強度譜線的每一個週期內定義一個平緩區,所述平緩區內具有至少一個所述即時光信號強度取樣值;在每一所述平緩區內的即時光信號強度取樣值中抽取一個作為光信號強度特徵值;根據所述光信號強度特徵值建立光信號強度特徵譜線;以及根據所述光信號強度特徵譜線確定所述等離子體處理工藝的終點。 In order to achieve the above object, the present invention provides an end point detecting method for a plasma processing process, the plasma processing process comprising a plurality of periodic plasma processing steps, the end point detecting method comprising: collecting the plasma at certain time intervals Instantaneous optical signal strength at a particular wavelength during the body processing process to obtain a plurality of instantaneous optical signal strength samples and to establish a periodic instantaneous optical signal intensity line, the instantaneous optical signal strength reacting with the plasma processing process a concentration of the component or a concentration of the product component; defining a gradual zone in each of the periods of the instantaneous optical signal intensity line, the gradual zone having at least one of the instantaneous optical signal intensity samples; Extracting, as an optical signal intensity characteristic value, an instantaneous optical signal strength sample value in the gradual region; establishing an optical signal strength characteristic line according to the optical signal strength characteristic value; and determining, according to the optical signal intensity characteristic line The end point of the plasma treatment process.

優選的,所述平緩區內具有至少兩個所述即時光信號強度取樣值。 Preferably, the gradual zone has at least two of the instant optical signal strength samples.

優選的,在所述即時光信號強度譜線的每一個週期內定義一個平緩區的步驟包括將一定時間段內所述即時光信號強度取樣值的變化量小於參考值的區域定義為所述平緩區,其中所述參考值的範圍為該週期內所述即時光信號強度取樣值的最大值的0.1%~10%。 Preferably, the step of defining a gradual region in each period of the instantaneous optical signal intensity line includes defining, as the gradual, a region in which the variation of the instantaneous optical signal strength sample value is less than a reference value in a certain period of time. a region, wherein the reference value ranges from 0.1% to 10% of a maximum value of the instantaneous optical signal strength sample value in the period.

優選的,在所述即時光信號強度譜線的每一個週期內定義一個平緩區的步驟包括將所述即時光信號強度取樣值在預定範圍內且在一定時間段內所述即時光信號強度取樣值的變化量小於參考值的區域定義為所述平緩區,其中所述參考值的範圍為該週期內所述即時光信號強度取樣值的最大值的0.1%~10%。 Preferably, the step of defining a gradual region in each period of the instantaneous optical signal intensity line comprises sampling the instantaneous optical signal strength sample value within a predetermined range and sampling the instantaneous optical signal intensity for a certain period of time A region in which the amount of change in value is less than the reference value is defined as the gradual region, wherein the reference value ranges from 0.1% to 10% of the maximum value of the instantaneous optical signal strength sample value in the period.

優選的,在每一所述平緩區的即時光信號強度中內抽取一個光信號強度特徵值的步驟包括:判斷所述平緩區內即時光信號強度取樣值的個數;當所述即時光信號強度取樣值的個數為2N-1時,抽取第N個即時光信號強度取樣值作為所述光信號強度特徵值;當所述即時光信號強度取樣值的個數為2N時,抽取第N個或第N+1個即時光信號強度取樣值作為所述光信號強度特徵值,其中N為大於1的正整數。 Preferably, the step of extracting an optical signal strength characteristic value in the instantaneous optical signal strength of each of the gradual regions comprises: determining a number of instantaneous optical signal strength sampling values in the gradual region; and when the instant optical signal When the number of the intensity sampling values is 2N-1, the Nth instantaneous optical signal strength sample value is extracted as the optical signal strength characteristic value; when the number of the instant optical signal strength sampling values is 2N, the Nth is extracted. Or N+1th instantaneous optical signal strength sample values as the optical signal strength characteristic values, where N is a positive integer greater than one.

優選的,根據所述光信號強度特徵譜線確定所述等離子體處理工藝的終點的步驟包括:根據所述光信號強度特徵譜線確定特徵值拐點;以及根據所述特徵值拐點確定所述等離子體處理工藝的終點。 Preferably, the step of determining an end point of the plasma processing process according to the optical signal intensity characteristic line comprises: determining a feature value inflection point according to the optical signal intensity characteristic line; and determining the plasma according to the characteristic value inflection point The end point of the body treatment process.

優選的,每一所述等離子體處理步驟包括一個蝕刻步驟和一個沉積步驟。 Preferably, each of said plasma processing steps includes an etching step and a deposition step.

本發明還提供了一種等離子體處理工藝的終點檢測裝置,其中所述等離子體處理工藝包括多個週期性的等離子體處理步驟,該終點檢測裝置包括:信號採集模組,用於以一定時間間隔採集所述等離子體處理工藝過程中的即時光信號強度以獲取多個即時光信號強度取樣值並建立具有週期性的即時光信號強度譜線,所述即時光信號強度與所述等離子體處理工藝的反應物組分濃度或產物組分濃度對應;平緩區定義模組,與所述信號採集模組相連,用於在所述即時光信號強度譜線的每一個週期內定義 一個平緩區,所述平緩區內具有至少一個所述即時光信號強度取樣值;特徵值抽取模組,與所述平緩區定義模組,用於在每一所述平緩區的即時光信號強度取樣值中內抽取一個作為光信號強度特徵值;特徵譜線建立模組,與所述特徵值抽取模組相連,用於根據所述光信號強度特徵值建立光信號強度特徵譜線;以及終點確定模組,與所述特徵值譜建立模組相連,用於根據所述光信號強度特徵譜線確定所述等離子體處理工藝的終點。 The present invention also provides an end point detecting device for a plasma processing process, wherein the plasma processing process includes a plurality of periodic plasma processing steps, the end point detecting device comprising: a signal acquisition module for using a time interval Acquiring the instantaneous optical signal intensity during the plasma processing process to obtain a plurality of instantaneous optical signal intensity sampling values and establishing a periodic instantaneous optical signal intensity spectral line, the instantaneous optical signal strength and the plasma processing process Corresponding to a component concentration or a product component concentration; a gradual zone defining module coupled to the signal acquisition module for defining each cycle of the instantaneous optical signal intensity line a gradual zone having at least one of the instant optical signal strength samples; the eigenvalue extraction module, and the gradual zone definition module for instantaneous optical signal strength in each of the gradual zones Extracting one of the sampled values as an optical signal intensity characteristic value; a characteristic line establishing module connected to the characteristic value extracting module for establishing an optical signal intensity characteristic line according to the optical signal intensity characteristic value; and an end point The determining module is connected to the characteristic value spectrum establishing module for determining an end point of the plasma processing process according to the optical signal intensity characteristic line.

優選的,所述平緩區內具有至少兩個所述即時光信號強度取樣值。 Preferably, the gradual zone has at least two of the instant optical signal strength samples.

優選的,所述平緩區定義模組根據所述即時光信號強度的變化,將一定時間段內所述即時光信號強度取樣值的變化量小於參考值的區域定義為所述平緩區,其中所述參考值的範圍為該週期內所述即時光信號強度取樣值的最大值的0.1%~10%。 Preferably, the grading area defining module defines, according to the change of the instantaneous optical signal strength, an area in which the variation of the instantaneous optical signal strength sampling value is less than a reference value in a certain period of time as the gradual area, where The reference value ranges from 0.1% to 10% of the maximum value of the instantaneous optical signal strength sample value in the period.

優選的,所述平緩區定義模組根據所述即時光信號強度及所述即時光信號強度的變化,將所述即時光信號強度取樣值在預定範圍內且在一定時間段內所述即時光信號強度取樣值的變化量小於參考值的區域定義為所述平緩區,其中所述參考值的範圍為該週期內所述即時光信號強度取樣值的最大值的0.1%~10%。 Preferably, the tempering zone definition module sets the instantaneous optical signal strength sample value within a predetermined range according to the change of the instantaneous optical signal strength and the instantaneous optical signal strength, and the instant light is within a certain time period. A region in which the amount of change in the signal strength sample value is smaller than the reference value is defined as the gradation region, wherein the reference value ranges from 0.1% to 10% of the maximum value of the instantaneous light signal intensity sample value in the period.

優選的,所述特徵值抽取模組包括判斷子模組和抽取子模組,所述判斷子模組用於判斷所述平緩區內即時光信號強度取樣值的個數;所述抽取子模組與所述判斷子模組相連,當所述即時光信號強度取樣值的個數為2N-1時,抽取第N個即時光信號強度取樣值作為所述光信號強度特徵值;當所述即時光信號強度取樣值的個數為2N時,抽取第N個或第N+1個即時光信號強度取樣值作為所述光信號強度特徵值,其中N為大於1的正整數。 Preferably, the feature value extraction module includes a determination sub-module and an extraction sub-module, and the determination sub-module is configured to determine the number of instantaneous optical signal strength sampling values in the gradual area; the extraction sub-module The group is connected to the determining sub-module, and when the number of the instantaneous optical signal strength sampling values is 2N-1, extracting the Nth instantaneous optical signal strength sampling value as the optical signal strength characteristic value; When the number of the instantaneous optical signal strength sample values is 2N, the Nth or N+1th instantaneous optical signal strength sample value is extracted as the optical signal strength characteristic value, where N is a positive integer greater than 1.

優選的,所述終點確定模組還包括特徵值拐點搜索子模組以及終點確定子模組,所述特徵值拐點搜索子模組根據所述光信號強度特徵譜線確定特徵值拐點;所述終點確定子模組與所述特徵值拐點搜索子模組相連,根據所述特徵值拐點確定所述等離子體處理工藝的終點。 Preferably, the endpoint determining module further includes a feature value inflection point search submodule and an end point determining submodule, and the feature value inflection point search submodule determines a feature value inflection point according to the optical signal intensity characteristic line; The endpoint determining sub-module is coupled to the feature value inflection point search sub-module, and determining an end point of the plasma processing process according to the feature value inflection point.

優選的,每一所述等離子體處理步驟包括一個蝕刻步驟和一 個沉積步驟。 Preferably, each of the plasma processing steps includes an etching step and a a deposition step.

本發明的有益效果在於利用圖形識別的方法,通過在即時光信號強度譜線中定義平緩區並在平緩區中抽取光信號強度特徵值來形成平滑的光信號強度-時間特徵譜線,不僅能夠解決因等離子體快速且週期性擾動而造成的終點判定誤判的問題,還能有效改善現有技術中採用最大值形成包絡線對終點判定不敏感及易發生包絡線抖動而造成終點檢測不準確的缺陷。此外,在本發明中,即使光信號強度特徵值抽取時發生延時仍然能保證形成的包絡線光滑,從而有效提高終點檢測能力和檢測靈活性。 The invention has the beneficial effects of using a pattern recognition method to form a smooth optical signal intensity-time characteristic line by defining a gradual area in the instantaneous optical signal intensity line and extracting the optical signal intensity characteristic value in the gradual area. Solving the problem of misjudgment of the endpoint judgment caused by the rapid and periodic disturbance of the plasma, and effectively improving the defect that the maximum value forming envelope is insensitive to the endpoint determination and the envelope jitter is easy to occur, resulting in inaccurate endpoint detection in the prior art. . In addition, in the present invention, even if a delay occurs in the extraction of the optical signal intensity characteristic value, the formed envelope is ensured to be smooth, thereby effectively improving the end point detection capability and the detection flexibility.

201、202、203、204、205‧‧‧步驟 Steps 201, 202, 203, 204, 205‧‧

701‧‧‧信號採集模組 701‧‧‧Signal acquisition module

702‧‧‧平緩區定義模組 702‧‧‧ Flat Zone Definition Module

703‧‧‧特徵值抽取模組 703‧‧‧Characteristic value extraction module

704‧‧‧特徵譜線建立模組 704‧‧‧Characteristic line building module

705‧‧‧終點確定模組 705‧‧‧ Endpoint Determination Module

圖1所示為現有的博世工藝中所獲得的OES光信號強度隨工藝時間變化的示意圖。 Figure 1 is a schematic diagram showing the OES optical signal intensity obtained in the prior Bosch process as a function of process time.

圖2是所示為本發明實施例的一種等離子體處理工藝的終點檢測方法的步驟流程圖。 2 is a flow chart showing the steps of an end point detecting method of a plasma processing process according to an embodiment of the present invention.

圖3是所示為本發明實施例的等離子體處理工藝中即時光信號強度譜線的示意圖。 3 is a schematic view showing an instantaneous light signal intensity spectrum line in a plasma processing process according to an embodiment of the present invention.

圖4所示為現有技術採用峰值形成的包絡線與本發明的等離子體處理工藝中反應物的光信號強度特徵譜線的對比示意圖。 FIG. 4 is a schematic diagram showing the comparison of the optical signal intensity characteristic lines of the reactants in the prior art using the peak formed envelope and the plasma processing process of the present invention.

圖5所示為當等離子體處理工藝的蝕刻面積為晶片面積時蝕刻產物的光信號強度特徵譜線的示意圖。 Figure 5 is a schematic illustration of the optical signal intensity characteristic line of the etched product when the etched area of the plasma processing process is the wafer area.

圖6所示為當等離子體處理工藝的蝕刻面積為晶片面積的5%時蝕刻產物的光信號強度特徵譜線的示意圖。 Figure 6 is a schematic illustration of the optical signal intensity characteristic line of the etched product when the etched area of the plasma processing process is 5% of the wafer area.

圖7所示為本發明實施例的一種等離子體處理工藝的終點檢測裝置的方塊圖。 FIG. 7 is a block diagram showing an end point detecting device of a plasma processing process according to an embodiment of the present invention.

為使本發明的內容更加清楚易懂,以下結合說明書附圖,對本發明的內容作進一步說明。當然本發明並不局限於該具體實施例,本領域內的技術人員所熟知的一般替換也涵蓋在本發明的保護範圍內。 In order to make the content of the present invention clearer and easier to understand, the contents of the present invention will be further described below in conjunction with the accompanying drawings. Of course, the invention is not limited to the specific embodiment, and general replacements well known to those skilled in the art are also encompassed within the scope of the invention.

由背景技術可知,在具有週期性處理步驟的等離子體處理工藝中,抽取峰值形成包絡線來檢測等離子體工藝終點的方法並不能準確檢測到終點。為此,本發明提出一種優化的等離子體處理工藝終點檢測方法,來解決現有技術的缺陷。 It is known from the background art that in a plasma processing process having a periodic processing step, the method of extracting the peak forming envelope to detect the end point of the plasma process does not accurately detect the end point. To this end, the present invention proposes an optimized plasma processing process endpoint detection method to address the deficiencies of the prior art.

請參考圖2,其示出了本發明的一種等離子體處理工藝的終點檢測方法,等離子體處理工藝包括多個週期性的等離子體處理步驟。具體可以包括以下步驟:步驟201,以一定時間間隔採集等離子體處理工藝過程中特定波長的的即時光信號強度以獲取多個即時光信號強度取樣值並建立具有週期性的即時光信號強度譜線;其中即時光信號強度與等離子體處理工藝的反應物組分濃度或產物組分濃度對應,本領域技術人員可以根據晶片的類型和工藝氣體的類型,選擇相應的特定波長的即時光信號,並獲取特定波長的即時光信號強度。 Please refer to FIG. 2, which illustrates an end point detecting method of a plasma processing process of the present invention, the plasma processing process including a plurality of periodic plasma processing steps. Specifically, the method may include the following steps: Step 201: Acquire real-time optical signal intensity of a specific wavelength during a plasma processing process at a certain time interval to obtain a plurality of instantaneous optical signal strength sampling values and establish a periodic optical signal intensity line with periodicity Where the instantaneous light signal intensity corresponds to the reactant component concentration or the product component concentration of the plasma treatment process, those skilled in the art can select an appropriate specific wavelength of the instantaneous light signal according to the type of the wafer and the type of the process gas, and Get instant optical signal strength at a specific wavelength.

步驟202,在所述即時光信號強度譜線的每一個週期內定義一個平緩區,所述平緩區內具有至少一個所述即時光信號強度取樣值。 Step 202: Define a gradual zone in each period of the instant optical signal intensity line, the gradual zone having at least one of the instant optical signal strength samples.

步驟203,在每一所述平緩區的即時光信號強度取樣值中內抽取一個作為光信號強度特徵值。 Step 203: Extract one of the instantaneous optical signal strength sample values in each of the gradual regions as an optical signal strength feature value.

步驟204,根據所述光信號強度特徵值建立光信號強度特徵譜線。 Step 204: Establish an optical signal intensity characteristic line according to the optical signal strength characteristic value.

步驟205,根據所述光信號強度特徵譜線確定所述等離子體處理工藝的終點。 Step 205: Determine an end point of the plasma processing process according to the optical signal intensity characteristic line.

請參照圖3,示出了本發明實施例的等離子體處理工藝中等離子體的光信號強度隨時間變化的示意圖,也即是特定波長的即時光信號強度譜線的示意圖。本發明的等離子體處理工藝包括多個週期性的等離子體處理步驟,而每個等離子體處理步驟可包括多個不同步驟。在本實施例中,每個等離子體處理步驟均包括一個蝕刻步驟和一個沉積步驟,等離子體處理工藝為博世工藝,通過使等離子蝕刻步驟和等離子沉積步驟週期性交替反復進行而進行蝕刻。當然在其他實施例中,每個等離子體處理步驟也可包括蝕刻步驟,沉積步驟,過渡步驟或清洗步驟等,本發明並不限於 此。 Referring to FIG. 3, there is shown a schematic diagram of the optical signal intensity variation of plasma in a plasma processing process according to an embodiment of the present invention, that is, a schematic diagram of an instantaneous optical signal intensity spectrum of a specific wavelength. The plasma processing process of the present invention includes a plurality of periodic plasma processing steps, and each plasma processing step can include a plurality of different steps. In the present embodiment, each of the plasma processing steps includes an etching step and a deposition step, and the plasma processing is a Bosch process, and etching is performed by periodically alternately repeating the plasma etching step and the plasma deposition step. Of course, in other embodiments, each plasma processing step may also include an etching step, a deposition step, a transition step or a cleaning step, etc., and the invention is not limited thereto. this.

本發明的技術原理為首先以一定時間間隔採集即時光信號強度從而獲得多個即時光信號強度取樣值並根據這些即時光信號強度取樣值建立即時光信號強度譜線,如圖3所示,在本實施例中,採集的時間間隔為200ms,圖3中各個點即為即時光信號強度取樣值。由於等離子體處理工藝具有週期性的多個處理步驟,採集的即時光信號強度取樣值所形成的譜線也相應具有週期性,從圖3中可以看出,即時光信號強度譜線的週期性非常均勻。之後在光信號強度譜線的每一個週期內定義出一個平緩區,平緩區內具有至少一個即時光信號強度取樣值,如工藝時間為165秒時刻所採集的光信號強度取樣值的波動較小,則視其為處於平緩區。本發明可採用不同方法定義平緩區,如在週期開始後通過時間延遲,或根據光信號強度取樣值的變化趨勢等。當平緩區中只有一個即時光信號強度取樣值時,容易發生抖動,為了改善這一抖動現象,平緩區中可至少具有兩個即時光信號強度取樣值,以提供更多的選擇性和準確性。在本實施例中,是依據即時光信號強度取樣值的變化,將一定時間段內(如3個採集時間間隔),即時光信號強度取樣值的變化量小於參考值的部分定義為平緩區,如圖3中第159.4至159.8秒所對應的譜線區域。當然,在其他實施例中,即時光信號強度譜線的一個週期內可能會具有多個光信號強度取樣值變化平緩,即即時光信號強度取樣值的變化符合要求的區域,此時可進一步限定即時光信號強度取樣值的大小,將光信號強度取樣值在預定範圍內且在一定時間段內光信號強度取樣值的變化量小於參考值的區域定義為平緩區。較佳的,上述參考值的取值範圍為該週期中即時光信號強度取樣值的最大值的0.1%~10%,其中可以將該週期中的即時光信號強度譜線最高點的取樣值作為該週期即時光信號強度取樣值的最大值。接著,抽取每一平緩區即時光信號強度取樣值的一個作為光信號強度特徵值,再由這些特徵值來形成光信號強度特徵譜線。由於抽取的光信號強度特徵值均位於平緩區內,較為穩定,不易發生偏差,由其所形成的特徵譜線對終點檢測更為敏感。 The technical principle of the present invention is to first acquire the instantaneous optical signal intensity at a certain time interval to obtain a plurality of instantaneous optical signal strength sampling values and establish an instantaneous optical signal intensity spectral line according to the instantaneous optical signal strength sampling values, as shown in FIG. In this embodiment, the time interval of the acquisition is 200 ms, and each point in FIG. 3 is the instantaneous optical signal strength sample value. Since the plasma processing process has a plurality of periodic processing steps, the spectral lines formed by the acquired instantaneous optical signal intensity sampling values are also periodically periodic. As can be seen from FIG. 3, the periodicity of the instantaneous optical signal intensity spectral lines Very uniform. Then, a gradual zone is defined in each period of the optical signal intensity line, and at least one instantaneous optical signal intensity sample value is included in the gradual zone, and the fluctuation of the sampled value of the optical signal intensity collected at the time of the process time of 165 seconds is small. , it is considered to be in a gentle zone. The present invention can employ different methods to define a gradual zone, such as a time delay after the start of the cycle, or a trend of the sampled value according to the intensity of the optical signal. When there is only one instantaneous optical signal strength sample value in the gradual zone, jitter is easy to occur. In order to improve this jitter phenomenon, at least two instantaneous optical signal strength samples may be included in the gradual zone to provide more selectivity and accuracy. . In this embodiment, according to the change of the sampling value of the instantaneous optical signal strength, a portion in which the variation of the instantaneous optical signal strength sampling value is smaller than the reference value is defined as a gradual region within a certain period of time (eg, three acquisition time intervals). The area of the line corresponding to the 159.4th to 159.8th seconds in Figure 3. Certainly, in other embodiments, a period of the instantaneous optical signal strength spectrum may have a plurality of optical signal intensity sample values that are gentle, that is, a change in the instantaneous optical signal strength sample value meets the required region, and may be further limited. The size of the instantaneous optical signal strength sample value is defined as a gradual region in which the optical signal strength sample value is within a predetermined range and the amount of change of the optical signal strength sample value is less than the reference value within a certain period of time. Preferably, the reference value ranges from 0.1% to 10% of the maximum value of the instantaneous optical signal strength sample value in the period, wherein the sampled value of the highest point of the instantaneous optical signal intensity line in the period can be used as the sampling value The maximum value of the instantaneous optical signal strength sample value for this period. Then, one of the instantaneous optical signal intensity samples of each gradual zone is extracted as an optical signal strength eigenvalue, and the eigenvalues are used to form an optical signal strength characteristic line. Since the extracted optical signal intensity characteristic values are all located in the gradual region, they are relatively stable and are not easy to be deviated, and the characteristic lines formed by them are more sensitive to the end point detection.

接下來根據所形成的特徵值譜線確定等離子體處理工藝。圖 4為現有技術採用峰值形成的包絡線1與本發明的等離子體處理工藝中反應物的光信號強度特徵譜線2的對比示意圖。如圖4所示,對於採用峰值來形成包絡線1,由於峰值的穩定性較差,對終點的靈敏度較低,基本無法用來判定終點。通過本發明的即時光信號強度特徵值來形成的譜線2能夠很清楚地找到特徵值發生變化點即特徵值拐點,在接近特徵值拐點時,反應物的特徵譜線2迅速上升。因此根據特徵譜線能夠確定出特徵值拐點,而根據特徵值拐點即可進一步獲得等離子體處理工藝的終點。 Next, the plasma processing process is determined based on the formed feature value lines. Figure 4 is a schematic diagram comparing the optical signal intensity characteristic line 2 of the reactants in the prior art using the peak formed envelope 1 and the plasma treatment process of the present invention. As shown in FIG. 4, for the use of the peak to form the envelope 1, since the stability of the peak is poor, the sensitivity to the end point is low, and it is basically impossible to determine the end point. The spectral line 2 formed by the instantaneous light signal intensity characteristic value of the present invention can clearly find the characteristic value inflection point, that is, the characteristic value inflection point, and the characteristic line 2 of the reactant rapidly rises as it approaches the inflection point of the characteristic value. Therefore, the inflection point of the feature value can be determined according to the characteristic line, and the end point of the plasma processing process can be further obtained according to the inflection point of the feature value.

進一步的,為了更好地在平緩區抽取出適當的即時光強度特徵值,在即時光信號譜線每個週期的平緩區內,抽取其中即時光信號強度取樣值的中間位置的資料點作為光信號強度特徵值。詳細而言,首先判斷平緩區內即時光信號強度取樣值的個數,當即時光信號強度取樣值的個數為奇數時,抽取中間的即時光信號強度取樣值作為光信號強度特徵值;當即時光信號強度取樣值的個數為偶數時,抽取中間的兩個即時光信號強度取樣值之一作為光信號強度特徵值。這樣做是因為即時光信號強度取樣值抽取時可能會有抽取延時且每次延時的時間不一致的情況發生,如果平緩區具有多個即時光信號強度取樣值而抽取的是平緩區邊緣的光信號強度取樣值資料點,很容易因延時而使得平緩區以外的光信號強度取樣值被抽取,而在該區域光信號強度取樣值變化很大,因此以其形成的特徵譜線就會有較多鋸齒,如果這些鋸齒的強度變化與特徵值拐點的強度變化接近,則易發生特徵值拐點誤判甚而最終會影響到終點判定。而在本發明的檢測方法中,抽取平緩區中間的即時光信號強度取樣值作為光信號強度特徵值,即使因延遲發生提前抽取或延遲抽取的情況,所抽取的光信號強度特徵值還是在平緩區內,所以形成的特徵譜線依然很光滑,如此一來,就能夠很容易地找到發生變化的光信號強度特徵值拐點,尤其是在蝕刻面積比較小信號強度變化微弱時,仍然能夠有效判斷,從而提高終點檢測的能力。圖5和圖6所示分別為博世工藝蝕刻面積與晶片面積相同時,以及蝕刻面積為晶片面積的5%時蝕刻產物的光信號強度特徵譜線的示意圖。由圖中可以看出,在接近特徵值拐點時,蝕刻產物所對應的特徵譜線有明顯下降,說明蝕刻產物的濃度降低。即使圖6中蝕刻面積減小到一定程度,特徵譜 線的變化較為微弱時,仍然能夠找出特徵值拐點。 Further, in order to extract the appropriate instantaneous light intensity characteristic value in the gradual area, the data point of the intermediate position of the instantaneous optical signal intensity sampling value is extracted as light in the gradual area of each period of the instant optical signal line. Signal strength eigenvalue. In detail, firstly, the number of samples of the instantaneous optical signal intensity in the gradual area is determined. When the number of the instantaneous optical signal intensity samples is an odd number, the intermediate instantaneous optical signal intensity sample value is extracted as the optical signal strength characteristic value; When the number of signal strength samples is an even number, one of the two instantaneous optical signal intensity samples in the middle is extracted as the optical signal strength characteristic value. This is because the instantaneous optical signal strength sampling value extraction may have a decimation delay and the time of each delay is inconsistent. If the flat region has multiple instantaneous optical signal strength sampling values, the optical signal at the edge of the gradual region is extracted. The intensity sampling value data point is easy to extract the optical signal intensity sampling value outside the gradual area due to the delay, and the optical signal intensity sampling value varies greatly in this area, so the characteristic line formed by it will be more Sawtooth, if the intensity change of these serrations is close to the intensity change of the inflection point of the feature value, the eigenvalue inflection point misjudgment may easily occur and eventually affect the end point judgment. In the detection method of the present invention, the instantaneous optical signal strength sample value in the middle of the tempering zone is extracted as the optical signal strength eigenvalue, and even if the delay occurs in advance extraction or delayed extraction, the extracted optical signal strength eigenvalue is still gentle. In the area, the characteristic line formed is still very smooth, so that it is easy to find the inflection point of the characteristic value of the optical signal intensity that changes, especially when the etching area is small and the signal intensity changes are weak, it can still be effectively judged. , thereby improving the ability of endpoint detection. 5 and 6 are schematic diagrams showing the optical signal intensity characteristic lines of the etching product when the etching area of the Bosch process is the same as the wafer area, and the etching area is 5% of the wafer area, respectively. As can be seen from the figure, when the inflection point of the characteristic value is approached, the characteristic line corresponding to the etching product is significantly decreased, indicating that the concentration of the etching product is lowered. Even if the etching area in Figure 6 is reduced to a certain extent, the characteristic spectrum When the change of the line is weak, the inflection point of the feature value can still be found.

需要注意的是,在形成光信號強度特徵譜線後,可採用各種方式來判斷特徵值拐點,如閾值交叉檢測或導數處理,具體可以參考現有的等離子體蝕刻工藝的蝕刻終點判斷方式,其為本領域技術人員所熟知,在這裏不作贅述。 It should be noted that after the optical signal intensity characteristic line is formed, various methods can be used to determine the inflection point of the feature value, such as threshold crossing detection or derivative processing. For details, reference may be made to the etching end point judgment mode of the existing plasma etching process, which is Those skilled in the art are well known and will not be described herein.

根據光信號強度的特徵值拐點即可確定等離子體處理工藝終點所在,一般而言,該終點可為即時光強度譜線中,特徵值拐點所在的週期中最後一個即時光信號強度取樣值採集的時間點,也即是該等離子體處理步驟結束時的時間點,本發明並不限於此。 According to the inflection point of the characteristic value of the optical signal strength, the end point of the plasma processing process can be determined. Generally, the end point can be the instantaneous light signal intensity sampling value in the period of the inversion point of the characteristic value in the instantaneous light intensity spectrum. The time point, that is, the time point at the end of the plasma processing step, the present invention is not limited thereto.

綜上所述,通過本發明的等離子體處理工藝的終點檢測方法,不僅能夠解決對於等離子體快速且週期性擾動的工藝終點判定誤判的問題,還能有效提高終點檢測的靈活性。 In summary, the end point detection method of the plasma processing process of the present invention can not only solve the problem of misjudgment of the process end point determination for rapid and periodic disturbance of the plasma, but also effectively improve the flexibility of the end point detection.

接下來,請參照圖7,其示出了本發明一種等離子體處理工藝的終點檢測裝置實施例,該終點檢測裝置包括:信號採集模組701,用於以一定時間間隔採集等離子體處理工藝過程中特定波長的即時光信號強度以獲取多個即時光信號強度取樣值並建立具有週期性的即時光信號強度譜線。 Next, please refer to FIG. 7, which illustrates an embodiment of an end point detecting device for a plasma processing process of the present invention. The end point detecting device includes a signal collecting module 701 for collecting a plasma processing process at intervals of time. The instantaneous optical signal strength of a particular wavelength is obtained to obtain a plurality of instantaneous optical signal strength samples and to establish a periodic optical signal intensity line with periodicity.

平緩區定義模組702,與信號採集模組701相連,用於在所述即時光信號強度譜線的每一個週期內定義一個平緩區,每一個平緩區具有至少一個即時光信號強度取樣值;其中平緩區定義模組702可根據所述即時光信號強度取樣值的變化,將一定時間段內所述即時光信號強度取樣值的變化量小於參考值的區域定義為所述平緩區;或根據所述即時光信號強度取樣值大小及所述即時光信號強度取樣值的變化,將所述即時光信號強度取樣值在預定範圍內且在一定時間段內所述即時光信號強度取樣值相對時間的變化量小於參考值的區域定義為所述平緩區。其中參考值的範圍為該週期內所述即時光信號強度取樣值的最大值的0.1%~10%。 The grading area defining module 702 is connected to the signal collecting module 701, and is configured to define a gradual area in each period of the instant optical signal intensity spectrum line, each tempering area having at least one instantaneous optical signal strength sampling value; The ambiguous area definition module 702 may define, according to the change of the instantaneous optical signal strength sampling value, an area in which the change amount of the instantaneous optical signal strength sampling value is less than a reference value in a certain period of time as the gradual area; or The instantaneous optical signal strength sample value and the instantaneous optical signal strength sample value change, the instantaneous optical signal strength sample value is within a predetermined range and the instantaneous optical signal strength sample value relative time is within a certain period of time The area where the amount of change is smaller than the reference value is defined as the gentle area. The reference value ranges from 0.1% to 10% of the maximum value of the instantaneous optical signal strength sample value in the period.

特徵值抽取模組703,與平緩區定義模組702相連,用於在每一平緩區內的即時光信號強度取樣值中抽取一個作為光信號強度特徵值。較佳的,特徵值抽取模組703還包括判斷子模組和抽取子模組,判斷 子模組用於判斷平緩區內即時光信號強度取樣值的個數;抽取子模組與判斷子模組相連,當即時光信號強度取樣值的個數為2N-1時,抽取第N個即時光信號強度取樣值作為光信號強度特徵值;當即時光信號強度取樣值的個數為2N時,抽取第N或第N+1個即時光信號強度取樣值作為光信號強度特徵值,其中N為大於1的正整數。 The feature value extraction module 703 is connected to the gradation area definition module 702 for extracting one of the instantaneous optical signal strength sample values in each gradation area as the optical signal strength feature value. Preferably, the feature value extraction module 703 further includes a judgment sub-module and an extraction sub-module, and determines The sub-module is used for judging the number of instantaneous optical signal strength sampling values in the gradual area; the extraction sub-module is connected to the judging sub-module, and when the number of the instant optical signal strength sampling values is 2N-1, the Nth instant is extracted. The optical signal strength sample value is used as the optical signal strength characteristic value; when the instantaneous optical signal strength sample value is 2N, the Nth or N+1th instant optical signal intensity sample value is extracted as the optical signal strength characteristic value, where N is A positive integer greater than one.

特徵譜線建立模組704,與特徵值抽取模組703相連,用於根據光信號強度特徵值建立光信號強度特徵譜線。 The characteristic line establishing module 704 is connected to the feature value extracting module 703 for establishing an optical signal intensity characteristic line according to the optical signal intensity characteristic value.

終點確定模組705,與特徵譜線建立模組704相連,根據光信號強度特徵譜線確定等離子體處理工藝終點。 The endpoint determination module 705 is coupled to the feature line setup module 704 to determine the end of the plasma processing process based on the optical signal intensity profile.

在本發明的一較佳實施例中,終點確定模組705還可以包括特徵值拐點搜索子模組以及終點確定子模組,特徵值拐點搜索子模組根據光信號強度特徵譜線確定特徵值發生變化的特徵值拐點;終點確定子模組與特徵值拐點搜索子模組相連,根據特徵值拐點確定等離子體處理工藝的終點。 In a preferred embodiment of the present invention, the endpoint determining module 705 may further include a feature value inflection point search submodule and an end point determining submodule, and the feature value inflection point search submodule determines the feature value according to the optical signal intensity characteristic line. The changed feature value inflection point; the end point determining sub-module is connected to the feature value inflection point search sub-module, and the end point of the plasma processing process is determined according to the feature value inflection point.

圖7所示的終點檢測裝置可以通過軟體,固件,硬體或其組合來實現,在此不作限制。由於終點檢測裝置對應前述的終點檢測方法,因此描述較為簡略,未詳盡之處可參見本說明書前述相應部分的描述。 The endpoint detecting device shown in FIG. 7 can be implemented by software, firmware, hardware, or a combination thereof, and is not limited herein. Since the end point detecting device corresponds to the aforementioned end point detecting method, the description is relatively simple, and the details of the corresponding parts in the foregoing description of the present specification can be referred to.

綜上所述,本發明充分利用了圖形識別方法,通過在採集的即時光信號強度譜線中定義出平緩區並從中抽取特徵值來形成特徵譜線,從而形成平滑的光信號強度-時間曲線,提高了在等離子體週期性擾動的工藝中進行終點檢測的準確性。進一步的,本發明通過在平緩區中間時刻抽取特徵值,有效改善了因信號強度採集延時而導致的特徵值抽取不准的問題,具有較高的靈活性和實用性。 In summary, the present invention makes full use of the pattern recognition method, and forms a characteristic line by defining a gradual area in the acquired instantaneous optical signal intensity line and extracting the feature value therefrom, thereby forming a smooth optical signal intensity-time curve. Improves the accuracy of endpoint detection in plasma periodic disturbances. Further, the present invention effectively improves the problem of inaccurate extraction of the feature values due to the signal strength acquisition delay by extracting the feature values in the middle of the gradual zone, and has high flexibility and practicability.

雖然本發明已以較佳實施例揭示如上,然所述諸多實施例僅為了便於說明而舉例而已,並非用以限定本發明,本領域的技術人員在不脫離本發明精神和範圍的前提下可作若干的更動與潤飾,本發明所主張的保護範圍應以權利要求書所述為准。 The present invention has been described in terms of the preferred embodiments of the present invention, and the present invention is intended to be illustrative only, and is not intended to limit the scope of the invention. In the case of a number of changes and refinements, the scope of protection claimed in the present invention shall be as defined in the claims.

201、202、203、204、205‧‧‧步驟 Steps 201, 202, 203, 204, 205‧‧

Claims (14)

一種等離子體處理工藝的終點檢測方法,所述等離子體處理工藝包括多個週期性的等離子體處理步驟,所述終點檢測方法包括:以一定時間間隔採集所述等離子體處理工藝過程中特定波長的即時光信號強度以獲取多個即時光信號強度取樣值並建立具有週期性的即時光信號強度譜線,所述即時光信號強度與所述等離子體處理工藝的反應物組分濃度或產物組分濃度對應;在所述即時光信號強度譜線的每一個週期內定義一個平緩區,所述平緩區內具有至少一個所述即時光信號強度取樣值;在每一所述平緩區內的即時光信號強度取樣值中抽取一個作為光信號強度特徵值;根據所述光信號強度特徵值建立光信號強度特徵譜線;以及根據所述光信號強度特徵譜線確定所述等離子體處理工藝的終點。 An end point detecting method for a plasma processing process, the plasma processing process comprising a plurality of periodic plasma processing steps, the end point detecting method comprising: collecting a specific wavelength of the plasma processing process at intervals of time Instant optical signal strength to obtain a plurality of instantaneous optical signal strength samples and to establish a periodic instantaneous optical signal intensity line, the instantaneous optical signal strength and the reactant component concentration or product composition of the plasma processing process Corresponding to a concentration; defining a gradual zone in each period of the instant optical signal intensity line, the gradual zone having at least one of the instant optical signal strength samples; and instant light in each of the gradual zones Extracting one of the signal strength sample values as an optical signal strength characteristic value; establishing an optical signal strength characteristic line according to the optical signal strength characteristic value; and determining an end point of the plasma processing process according to the optical signal intensity characteristic line. 根據權利要求1所述的等離子體處理工藝的終點檢測方法,其中,所述平緩區內具有至少兩個所述即時光信號強度取樣值。 The endpoint detection method of a plasma processing process according to claim 1, wherein said gentle region has at least two of said instantaneous optical signal intensity samples. 根據權利要求2所述的等離子體處理工藝的終點檢測方法,其中,在所述即時光信號強度譜線的每一個週期內定義一個平緩區的步驟包括:將一定時間段內所述即時光信號強度取樣值的變化量小於參考值的區域定義為所述平緩區,其中所述參考值的範圍為該週期內所述即時光信號強度取樣值的最大值的0.1%~10%。 The endpoint detection method of a plasma processing process according to claim 2, wherein the step of defining a gradual region in each period of the instantaneous optical signal intensity line comprises: the instantaneous optical signal for a certain period of time A region in which the amount of change in the intensity sample value is smaller than the reference value is defined as the gradation region, wherein the reference value ranges from 0.1% to 10% of the maximum value of the instantaneous light signal intensity sample value in the period. 根據權利要求2所述的等離子體處理工藝的終點檢測方法,其中,在所述即時光信號強度譜線的每一個週期內定義一個平緩區的步驟包括:將 所述即時光信號強度取樣值在預定範圍內且在一定時間段內所述即時光信號強度取樣值的變化量小於參考值的區域定義為所述平緩區,其中所述參考值的範圍為該週期內所述即時光信號強度取樣值的最大值的0.1%~10%。 The endpoint detection method of a plasma processing process according to claim 2, wherein the step of defining a gradation region in each period of the instantaneous light signal intensity spectrum line comprises: The area where the instantaneous optical signal strength sample value is within a predetermined range and the amount of change of the instantaneous optical signal strength sample value is less than a reference value within a certain period of time is defined as the gradation area, wherein the reference value ranges from The maximum value of the instantaneous optical signal intensity sample value in the period is 0.1% to 10%. 根據權利要求1所述的等離子體處理工藝的終點檢測方法,其中,在每一所述平緩區內的即時光信號強度取樣值中抽取一個作為光信號強度特徵值的步驟包括:判斷所述平緩區內即時光信號強度取樣值的個數;當所述即時光信號強度取樣值的個數為2N-1時,抽取第N個即時光信號強度取樣值作為所述光信號強度特徵值;當所述即時光信號強度取樣值的個數為2N時,抽取第N個或第N+1個即時光信號強度取樣值作為所述光信號強度特徵值,其中N為大於1的正整數。 The method for detecting an end point of a plasma processing process according to claim 1, wherein the step of extracting one of the instantaneous optical signal strength samples in each of the gradual regions as the optical signal strength characteristic value comprises: determining the gradual The number of the instantaneous optical signal strength samples in the area; when the number of the instantaneous optical signal strength samples is 2N-1, extracting the Nth instantaneous optical signal strength sample value as the optical signal strength characteristic value; When the number of the instantaneous optical signal strength sample values is 2N, the Nth or N+1th instantaneous optical signal strength sample value is extracted as the optical signal strength characteristic value, where N is a positive integer greater than 1. 根據權利要求1所述的等離子體處理工藝的終點檢測方法,其中,根據所述光信號強度特徵譜線確定所述等離子體處理工藝的終點的步驟包括:根據所述光信號強度特徵譜線確定特徵值拐點;以及根據所述特徵值拐點確定所述等離子體處理工藝的終點。 The endpoint detection method of a plasma processing process according to claim 1, wherein the determining the end point of the plasma processing process according to the optical signal intensity characteristic line comprises: determining, according to the optical signal intensity characteristic line An inflection point of the feature value; and determining an end point of the plasma processing process based on the inflection point of the feature value. 根據權利要求1所述的等離子體處理工藝的終點檢測方法,其中,每一所述等離子體處理步驟包括一個蝕刻步驟和一個沉積步驟。 The endpoint detection method of a plasma processing process according to claim 1, wherein each of said plasma processing steps includes an etching step and a deposition step. 一種等離子體處理工藝的終點檢測裝置,所述等離子體處理工藝包括多個週期性的等離子體處理步驟,所述終點檢測裝置包括: 信號採集模組,用於以一定時間間隔採集所述等離子體處理工藝過程中特定波長的即時光信號強度以獲取多個即時光信號強度取樣值並建立具有週期性的即時光信號強度譜線,所述即時光信號強度與所述等離子體處理工藝的反應物組分濃度或產物組分濃度對應;平緩區定義模組,與所述信號採集模組相連,用於在所述即時光信號強度譜線的每一個週期內定義一個平緩區,所述平緩區內具有至少一個所述即時光信號強度取樣值;特徵值抽取模組,與所述平緩區定義模組,用於在每一所述平緩區的即時光信號強度取樣值中內抽取一個作為光信號強度特徵值;特徵譜線建立模組,與所述特徵值抽取模組相連,用於根據所述光信號強度特徵值建立光信號強度特徵譜線;以及終點確定模組,與所述特徵譜線建立模組相連,用於根據所述光信號強度特徵譜線確定所述等離子體處理工藝的終點。 An end point detecting device for a plasma processing process, the plasma processing process comprising a plurality of periodic plasma processing steps, the end point detecting device comprising: The signal acquisition module is configured to acquire the instantaneous optical signal intensity of the specific wavelength during the plasma processing process at a certain time interval to obtain a plurality of instantaneous optical signal intensity sampling values and establish a periodic optical signal intensity spectrum line. The instantaneous optical signal intensity corresponds to a concentration of a reactant component or a product component of the plasma processing process; a gradual zone defining module is coupled to the signal acquisition module for use in the instantaneous optical signal strength Defining a gradual zone in each cycle of the line, the gradual zone having at least one of the instant optical signal strength samples; a feature value extraction module, and the gradual zone definition module for each Extracting an instant optical signal strength sample value in the gradual region as an optical signal strength feature value; a feature line establishing module connected to the eigenvalue extraction module for establishing light according to the optical signal intensity characteristic value a signal strength characteristic line; and an end point determining module connected to the characteristic line establishing module for determining a characteristic line according to the optical signal intensity The end point of the plasma treatment process. 根據權利要求8所述的等離子體處理工藝的終點檢測裝置,其中,所述平緩區內具有至少兩個所述即時光信號強度取樣值。 The endpoint detection apparatus of a plasma processing process according to claim 8, wherein said gentle region has at least two of said instantaneous optical signal strength samples. 根據權利要求9所述的等離子體處理工藝的終點檢測裝置,其中,所述平緩區定義模組根據所述即時光信號強度取樣值的變化,將一定時間段內所述即時光信號強度取樣值的變化量小於參考值的區域定義為所述平緩區,其中所述參考值的範圍為該週期內所述即時光信號強度取樣值的最大值的0.1%~10%。 The end point detecting device of the plasma processing process according to claim 9, wherein the gradual area defining module samples the instantaneous optical signal intensity in a certain period of time according to the change of the instantaneous optical signal intensity sampling value. The area where the amount of change is less than the reference value is defined as the gradual area, wherein the reference value ranges from 0.1% to 10% of the maximum value of the instantaneous optical signal strength sample value in the period. 根據權利要求9所述的等離子體處理工藝的終點檢測裝置,其中,所述平緩區定義模組根據所述即時光信號的強度及所述即時光信號強度的 變化,將所述即時光信號強度取樣值在預定範圍內且在一定時間段內所述即時光信號強度取樣值的變化量小於參考值的區域定義為所述平緩區,其中所述參考值為該週期內所述即時光信號強度取樣值的最大值的0.1%~10%。 The end point detecting device of the plasma processing process according to claim 9, wherein the gradual area defining module is based on the intensity of the instant optical signal and the intensity of the instantaneous optical signal And changing, the region in which the instantaneous optical signal strength sample value is within a predetermined range and the amount of change in the instantaneous optical signal strength sample value is less than a reference value in a certain period of time is defined as the gradation region, wherein the reference value is The maximum value of the instantaneous optical signal intensity sample value in the period is 0.1% to 10%. 根據權利要求8所述的等離子體處理工藝的終點檢測方法,其中,所述特徵值抽取模組包括判斷子模組和抽取子模組,所述判斷子模組用於判斷所述平緩區內即時光信號強度取樣值的個數;所述抽取子模組與所述判斷子模組相連,當所述即時光信號取樣值的個數為2N-1時,抽取第N個即時光信號強度取樣值作為所述光信號強度特徵值;當所述即時光信號取樣值的個數為2N時,抽取第N個或第N+1個即時光信號強度取樣值作為所述光信號強度特徵值,其中N為大於1的正整數。 The method for detecting an endpoint of a plasma processing process according to claim 8, wherein the feature value extraction module comprises a determination sub-module and an extraction sub-module, and the determination sub-module is configured to determine the gradual region The number of the instantaneous optical signal strength samples; the extraction sub-module is connected to the determination sub-module, and when the number of the instantaneous optical signal samples is 2N-1, extracting the Nth instantaneous optical signal strength The sampled value is used as the characteristic value of the optical signal strength; when the number of samples of the instant optical signal is 2N, the Nth or N+1th instantaneous optical signal intensity sample value is extracted as the optical signal strength characteristic value. Where N is a positive integer greater than one. 根據權利要求8所述的等離子體處理工藝的終點檢測方法,其中,所述終點確定模組還包括特徵值拐點搜索子模組以及終點確定子模組,所述特徵值拐點搜索子模組根據所述光信號強度特徵譜線確定特徵值拐點;所述終點確定子模組與所述特徵值拐點搜索子模組相連,根據所述特徵值拐點確定所述等離子體處理工藝的終點。 The endpoint detection method of the plasma processing process of claim 8, wherein the endpoint determination module further comprises a feature value inflection point search sub-module and an end point determination sub-module, and the feature value inflection point search sub-module is The optical signal intensity characteristic line determines a feature value inflection point; the end point determination sub-module is connected to the feature value inflection point search sub-module, and an end point of the plasma processing process is determined according to the feature value inflection point. 根據權利要求8所述的等離子體處理工藝的終點檢測方法,其中,每一所述等離子體處理步驟包括一個蝕刻步驟和一個沉積步驟。 The endpoint detection method of a plasma processing process according to claim 8, wherein each of said plasma processing steps includes an etching step and a deposition step.
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