SU665773A3 - Insecticide composition - Google Patents
Insecticide compositionInfo
- Publication number
- SU665773A3 SU665773A3 SU772525402A SU2525402A SU665773A3 SU 665773 A3 SU665773 A3 SU 665773A3 SU 772525402 A SU772525402 A SU 772525402A SU 2525402 A SU2525402 A SU 2525402A SU 665773 A3 SU665773 A3 SU 665773A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- dimethyl
- solvent
- active
- active substance
- emulsifier
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/18—One oxygen or sulfur atom
- C07D231/20—One oxygen atom attached in position 3 or 5
- C07D231/22—One oxygen atom attached in position 3 or 5 with aryl radicals attached to ring nitrogen atoms
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/10—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
- A01N47/18—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing a —O—CO—N< group, or a thio analogue thereof, directly attached to a heterocyclic or cycloaliphatic ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/18—One oxygen or sulfur atom
- C07D231/20—One oxygen atom attached in position 3 or 5
Description
(54) ИНСЕКТИЦИДНОЕ СРЕДСТВО(54) INSECTICIDE MEANS
Ё Присутствии растворител или разбавител .In the presence of a solvent or diluent.
Таким образом, получают следующие соединени общей формулы I, представленные в табл. 1.Thus, the following compounds of general formula I are obtained, presented in Table. one.
Таблица 1Table 1
Действующие начали, kOHueHTpaiiHH их Длительность оценки и результаты видны из табл. 2.The active ones began, kOHueHTpaiiHH their Duration of assessment and the results are visible from the table. 2
Таблица 2table 2
Опыт с MyzusExperience with Myzus
Формы применени средств - обычные; растворы, эмульсии, порошки, суспензии. Их приготавливают методами общими при изготовлении препаративных форм пестицидов .Forms of application are common; solutions, emulsions, powders, suspensions. They are prepared by methods common in the manufacture of preparative forms of pesticides.
Пример 1. Опыт с тлей (контактное действие).Example 1. Experience with aphids (contact action).
Растворитель: 3 вес. ч. ацетона.Solvent: 3 wt. including acetone.
Эмульгатор: 1 вес. ч. алкиларилполигликолевого эфира.Emulsifier: 1 weight. including alkylaryl polyglycol ether.
Дл получени препарата действующего начала 1 вес. ч. его смешивают с указанным количеством растворител и эмульгатора и разбавл ют концентрат водой до желаемой концентрации.In order to obtain an active drug, start 1 wt. it is mixed with the indicated amount of solvent and emulsifier and the concentrate is diluted with water to the desired concentration.
Препаратом действующего начала обры:згивают до образовани капель растени капусты (Brassica oleracea), сильно пораженные тлей (Myzus persicae).The preparation of the current beginning of the crop: zgivayut before the formation of cabbage plants (Brassica oleracea), strongly affected by aphids (Myzus persicae).
По истечении указанного времени определ ют степень умерщвлени . При этом 100% обозначает, что вс тл умерщвлена, 0% -ни одна тл не yмepu влeнa.After a specified time, the degree of killing is determined. At the same time, 100% means that all the animals have been euthanized, 0% - or only one person has not died.
Пример 2. Опыт с личинками листо &да.Example 2. Experiment with larvae of leaf & yes.
Растворитель: 3 вес. ч. ацетона.Solvent: 3 wt. including acetone.
Эмульгатор: 1 вес. ч. алкиларилпоЛиМйколевого эфира.Emulsifier: 1 weight. including alkylaryl ethers.
Дл получений препарата действующего начала 1 вес. ч. его смешивают с указанным количеством растворител и эмульгатора и разбавл ют концентрат водой до желаемой концентрации.To obtain the drug active start 1 wt. it is mixed with the indicated amount of solvent and emulsifier and the concentrate is diluted with water to the desired concentration.
Препаратом действующего начала обрызгивают до образовани капель листь каиусты н сажают на них личинки хренового листоеда (Phaeilon cochlearial).The drug of the beginning of the beginning is sprayed before the formation of kajusta leaves and the larvae of the crap leaves (Phaeilon cochlearial) are planted on them.
По истечении указанного времени определ ют степень умерщвлени . При этом 100% означает, что все личинки умерщвлень1 , 0%-ни одна личинка не умерщвлена .After a specified time, the degree of killing is determined. At the same time, 100% means that all larvae are killed, 0% - and one larva is not killed.
Действующие начала, концентрации их, длительность оценки и результаты видны из табл. 3.The active principles, their concentrations, the duration of the assessment and the results are visible from the table. 3
Таблица 3 Опыт с Phaedch - личинками.Table 3 Experience with Phaedch - larvae.
Пример 3. Опыт с предельной концентрацией (системное действие через корни).Example 3. Experience with limiting concentration (systemic action through the roots).
Подопытные насекомые. Myzus persieae.Experimental insects. Myzus persieae.
Растворитель: 3 вес. ч ацетона.Solvent: 3 wt. h acetone.
Эмульгатор: 1 вес. ч. алкиларилполигликолевого эфира.Emulsifier: 1 weight. including alkylaryl polyglycol ether.
Дл получени препарата действующего начала 1 вес. ч. его смешивают с указанным количеством растворител и эмульгатора и разбавл ют концентрат водой до желаемой концентрации.In order to obtain an active drug, start 1 wt. it is mixed with the indicated amount of solvent and emulsifier and the concentrate is diluted with water to the desired concentration.
Препарат действующего начала тщательно смешивают е землей. При этом решающим вл етс только количество действующего начала на объемную единицу земли, которое выражают в част х на млн. или мг/л. Обработанную землю засыпают в горшки и сажают в них капусту (Brassicu oleraceu). Действующее начало воспринимаетс растени ми из земли и передаетс в листь .The preparation of the active principle is thoroughly mixed with earth. In this case, the decisive factor is only the amount of active principle per volumetric unit of earth, which is expressed in parts per million or mg / l. The cultivated land is poured into pots and planted in cabbage (Brassicu oleraceu). The active principle is perceived by plants from the ground and transmitted to the leaves.
Дл дбказаГельства систбммб1 о действи через корни по истечении 7 дней иа листь Сажают указанных подопытных насекомых. По истечении дальнейших 2 дней осуществл ют оценкупутем подсчета или определени мертвых насекомых. Из числа умерщвленных насекомых вывод т системное действие действующего начала. Она составл ет 100%, если все насекомые умерщвлены, и 0% -если осталось в живых столько же насекомых, сколько при необработанном контроле.For sbstbmmb1 action through the roots after 7 days, these insect insects are planted. After a further 2 days, an evaluation is made of the counting or determination of dead insects. From the number of dead insects, a systemic action of the active principle is derived. It is 100% if all insects are euthanized, and 0% if as many insects are alive as with the untreated control.
Действующие иачала и результаты опыта .Existing and the results of the experiment.
1515
СтепеньPower
умерщвлени приkilling at
концентрацииconcentration
Действующее началоActive principle
действующегоacting
начала 20 частейstart 20 pieces
на млн.per million
2525
С-0-С-11(,СНз);C-0-C-11 (, CH3);
30thirty
9 7 5 4 2 6 1 39 7 5 4 2 6 1 3
100 100 100 100 100 100 100 100100 100 100 100 100 100 100 100
Пример 4. Опыт с паразитирующими личинками мух.Example 4. Experience with parasitic larvae of flies.
Растворитель: 35 вес. ч. этнленполнгликольмонометрилового эфира.Solvent: 35 wt. including ethnlen-complete glycol monomethyl ether.
Эмульгатор: 35 вес. ч. ноннлфенолролигликолевого эфира.Emulsifier: 35 wt. including nonnofenololiglycol ether.
Дл получени препарата действующего начала 30 вес. ч. соответствующего активного вещества смешивают с указанным количеством растворител , содержащего указанное количество эмульгатора и полученный таким образом концентрат разбавл ют водой до желаемой концентрации.To obtain a drug of the current beginning, 30 wt. the part of the corresponding active substance is mixed with the indicated amount of solvent containing the indicated amount of emulsifier and the concentrate thus obtained is diluted with water to the desired concentration.
Приблизительно 20 личинок мух (Lucillia cuprina) сажают в пробирку, в которой находитс приблизительно 2 см конины. На эту конину нанесены 0,5 мл препарата действующего начала. По истечении 24 определ ют степень умерщвлени . При этом 100% означает, что все личинки умерщвлены , а 0% -ни одна личинка не умерщвлена .Approximately 20 fly larvae (Lucillia cuprina) are planted in a test tube containing approximately 2 cm of horse meat. On this horse meat 0.5 ml of the active ingredient is applied. After 24, the killing degree is determined. At the same time, 100% means that all the larvae are euthanized, and 0% - and one larva is not killed.
Таким образом, предложенные соединени обладают хорошей инсектицидной активностью .Thus, the proposed compounds have good insecticidal activity.
Claims (2)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19762644588 DE2644588A1 (en) | 1976-10-02 | 1976-10-02 | Insecticidal O-pyrazolyl (N,N)-di:methyl-carbamate derivs. - prepd. from 3-substd.-5-hydroxy-pyrazole and di:methyl carbamic acid chloride |
Publications (1)
Publication Number | Publication Date |
---|---|
SU665773A3 true SU665773A3 (en) | 1979-05-30 |
Family
ID=5989532
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SU772525402A SU665773A3 (en) | 1976-10-02 | 1977-09-27 | Insecticide composition |
Country Status (8)
Country | Link |
---|---|
BE (1) | BE859239A (en) |
CS (1) | CS194187B2 (en) |
DE (1) | DE2644588A1 (en) |
ES (1) | ES462808A1 (en) |
HU (1) | HU177937B (en) |
PL (1) | PL107883B1 (en) |
SU (1) | SU665773A3 (en) |
ZA (1) | ZA775854B (en) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2721188A1 (en) * | 1977-05-11 | 1978-11-16 | Bayer Ag | Insecticidal O-pyrazolyl (N,N)-di:methyl-carbamate derivs. - prepd. from 3-substd.-5-hydroxy-pyrazole and di:methyl carbamic acid chloride |
DE2819932A1 (en) * | 1978-05-06 | 1979-11-15 | Bayer Ag | N, N-DIMETHYL-O-PYRAZOLYL-CARBAMINE ACID ESTER, METHOD FOR THE PRODUCTION THEREOF AND THEIR USE AS INSECTICIDES |
DE2839270A1 (en) * | 1978-09-09 | 1980-03-20 | Bayer Ag | N, N-DIMETHYL-O-PYRAZOLYL-CARBAMINIC ACID ESTER, METHOD FOR THE PRODUCTION THEREOF AND THEIR USE AS A PEST CONTROL |
DE2912494A1 (en) * | 1979-03-29 | 1980-10-09 | Bayer Ag | N, N-DIMETHYL-0-PYRAZOLYL-CARBAMINIC ACID ESTER, METHOD FOR THE PRODUCTION THEREOF AND THEIR USE AS A PEST CONTROL |
DE3002413A1 (en) * | 1980-01-24 | 1981-07-30 | Hoechst Ag, 6000 Frankfurt | N, N-DIALKYL-O- (PYRAZOL-5-YL) -CARBAMIC ACID ESTER, METHOD FOR THE PRODUCTION THEREOF AND THEIR USE AS INSECTICIDES |
DE3003019A1 (en) * | 1980-01-29 | 1981-07-30 | Bayer Ag, 5090 Leverkusen | N, N-DIMETHYL-O- (4,6-DIHYDRO-2H-THIENO (3,4-C) PYRAZOL-3-YL) -CARBAMINIC ACID ESTERS AND THEIR 5-OXIDES AND 5,5-DIOXIDES, METHOD FOR THEIR PROCESS PRODUCTION AND THEIR USE IN PEST CONTROL |
JPS6425764A (en) * | 1987-06-08 | 1989-01-27 | Monsanto Co | Substituted 3-(4-nitrophenoxy)pyrazole and herbicide |
US4964895A (en) * | 1987-06-08 | 1990-10-23 | Monsanto Company | Substituted 4-(4-nitrophenoxy) pyrazoles and their use as herbicides |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2420360A1 (en) * | 1974-04-26 | 1975-11-06 | Bayer Ag | N, N-DIMETHYL-0- SQUARE BRACKET ON 1-METHYL-3-N-METHYL-CARBAMINYL-METHYL-PYRAZOLE (5) YL SQUARE BRACKET ON CARBAMIC ACID ESTER, THE PROCESS FOR ITS MANUFACTURING AND USE AS A SIDE |
-
1976
- 1976-10-02 DE DE19762644588 patent/DE2644588A1/en active Granted
-
1977
- 1977-09-27 SU SU772525402A patent/SU665773A3/en active
- 1977-09-30 ZA ZA00775854A patent/ZA775854B/en unknown
- 1977-09-30 ES ES462808A patent/ES462808A1/en not_active Expired
- 1977-09-30 PL PL1977201169A patent/PL107883B1/en unknown
- 1977-09-30 CS CS776356A patent/CS194187B2/en unknown
- 1977-09-30 BE BE181337A patent/BE859239A/en unknown
- 1977-09-30 HU HU77BA3589A patent/HU177937B/en unknown
Also Published As
Publication number | Publication date |
---|---|
PL201169A1 (en) | 1978-05-08 |
HU177937B (en) | 1982-02-28 |
ZA775854B (en) | 1978-08-30 |
DE2644588C2 (en) | 1987-02-19 |
PL107883B1 (en) | 1980-03-31 |
ES462808A1 (en) | 1978-12-16 |
DE2644588A1 (en) | 1978-04-06 |
BE859239A (en) | 1978-03-30 |
CS194187B2 (en) | 1979-11-30 |
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