SU598865A1 - Method of obtaining 13-ketodicyclo-(10,3,0)-1/12-pentadecine - Google Patents

Method of obtaining 13-ketodicyclo-(10,3,0)-1/12-pentadecine

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Publication number
SU598865A1
SU598865A1 SU762418030A SU2418030A SU598865A1 SU 598865 A1 SU598865 A1 SU 598865A1 SU 762418030 A SU762418030 A SU 762418030A SU 2418030 A SU2418030 A SU 2418030A SU 598865 A1 SU598865 A1 SU 598865A1
Authority
SU
USSR - Soviet Union
Prior art keywords
obtaining
ketodicyclo
pentadecine
ketobicyclo
calculated
Prior art date
Application number
SU762418030A
Other languages
Russian (ru)
Inventor
Леонид Иванович Захаркин
Валентина Васильевна Гусева
Александр Петрович Пряянишников
Original Assignee
Ордена Ленина Институт Элементроорганических Соединений Ан Ссср
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Ордена Ленина Институт Элементроорганических Соединений Ан Ссср filed Critical Ордена Ленина Институт Элементроорганических Соединений Ан Ссср
Priority to SU762418030A priority Critical patent/SU598865A1/en
Application granted granted Critical
Publication of SU598865A1 publication Critical patent/SU598865A1/en

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Description

(54) СПОСОБ ПОЛУЧЕНИЯ 13-КЕТОБИЦИКЛО Ю ,3,О -1 (12)-ПЕНТАДЕЦЕНА(54) METHOD OF OBTAINING 13-KETOBICYCLO U, 3, O -1 (12) -PENTADESEN

Найдено, %: С 82,07; Н 10,.35.Found,%: C 82.07; H 10, .35.

S5 .4°S5 .4 °

Вычислено,%: С 81,81; Н 11,0 Элементарный анализ 2,4-ДФГ. Найдено,%: N 14,00,Calculated,%: C 81.81; H 11.0 Elemental analysis of 2,4-DFG. Found,%: N 14.00,

Cai .в 4Cai .in 4

Вычислено,%: N14,00Calculated,%: N14.00

Пример2, 20 г циклододеценилсукцинангидрида , 80 мл декана и 40 Мл полифосфорной кислоты быстро нагревают до 180°С. Реакционную cxiedb продолжают нагревать в течение 2 час. Далее массу обрабатывают, как в примере 1, и получают 7,5 г 13-кетобицикло- Ю,3,(12)-пентаДецена, выход 45%.Example 2, 20 g of cyclododecenylsuccinic anhydride, 80 ml of decane and 40 ml of polyphosphoric acid are rapidly heated to 180 ° C. The reaction cxiedb continue to heat for 2 hours. Next, the mass is treated as in Example 1, and 7.5 g of 13-ketobicyclo-U, 3, (12) -pentaDetsen are obtained, yield 45%.

Claims (1)

1. Патент Швейцарии 519456, кл. С 07 С, 49/54, 1972.1. Swiss patent 519456, cl. C 07 C, 49/54, 1972.
SU762418030A 1976-11-05 1976-11-05 Method of obtaining 13-ketodicyclo-(10,3,0)-1/12-pentadecine SU598865A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU762418030A SU598865A1 (en) 1976-11-05 1976-11-05 Method of obtaining 13-ketodicyclo-(10,3,0)-1/12-pentadecine

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU762418030A SU598865A1 (en) 1976-11-05 1976-11-05 Method of obtaining 13-ketodicyclo-(10,3,0)-1/12-pentadecine

Publications (1)

Publication Number Publication Date
SU598865A1 true SU598865A1 (en) 1978-03-25

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ID=20682074

Family Applications (1)

Application Number Title Priority Date Filing Date
SU762418030A SU598865A1 (en) 1976-11-05 1976-11-05 Method of obtaining 13-ketodicyclo-(10,3,0)-1/12-pentadecine

Country Status (1)

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SU (1) SU598865A1 (en)

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