SU527132A3 - Способ получени ариловых эфиров хлоругольной кислоты или циклических карбонатов - Google Patents
Способ получени ариловых эфиров хлоругольной кислоты или циклических карбонатовInfo
- Publication number
- SU527132A3 SU527132A3 SU1802668A SU1802668A SU527132A3 SU 527132 A3 SU527132 A3 SU 527132A3 SU 1802668 A SU1802668 A SU 1802668A SU 1802668 A SU1802668 A SU 1802668A SU 527132 A3 SU527132 A3 SU 527132A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- phosgene
- reaction
- acid
- cyclic carbonates
- aryl esters
- Prior art date
Links
- 239000002253 acid Substances 0.000 title description 14
- 238000000034 method Methods 0.000 title description 7
- 150000005676 cyclic carbonates Chemical class 0.000 title description 2
- 150000007860 aryl ester derivatives Chemical class 0.000 title 1
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 description 23
- 238000006243 chemical reaction Methods 0.000 description 15
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 14
- 229910052757 nitrogen Inorganic materials 0.000 description 13
- -1 phenyl ester Chemical class 0.000 description 12
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 9
- 239000003054 catalyst Substances 0.000 description 8
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 7
- 238000004821 distillation Methods 0.000 description 7
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- 239000011541 reaction mixture Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 4
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- AVQQQNCBBIEMEU-UHFFFAOYSA-N 1,1,3,3-tetramethylurea Chemical compound CN(C)C(=O)N(C)C AVQQQNCBBIEMEU-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 150000001408 amides Chemical class 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- YCIMNLLNPGFGHC-UHFFFAOYSA-N catechol Chemical compound OC1=CC=CC=C1O YCIMNLLNPGFGHC-UHFFFAOYSA-N 0.000 description 1
- XTEGARKTQYYJKE-UHFFFAOYSA-N chloric acid Chemical compound OCl(=O)=O XTEGARKTQYYJKE-UHFFFAOYSA-N 0.000 description 1
- 229940005991 chloric acid Drugs 0.000 description 1
- 238000005660 chlorination reaction Methods 0.000 description 1
- 229940077239 chlorous acid Drugs 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 125000002993 cycloalkylene group Chemical group 0.000 description 1
- ROORDVPLFPIABK-UHFFFAOYSA-N diphenyl carbonate Chemical compound C=1C=CC=CC=1OC(=O)OC1=CC=CC=C1 ROORDVPLFPIABK-UHFFFAOYSA-N 0.000 description 1
- USIUVYZYUHIAEV-UHFFFAOYSA-N diphenyl ether Chemical compound C=1C=CC=CC=1OC1=CC=CC=C1 USIUVYZYUHIAEV-UHFFFAOYSA-N 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- SAVROPQJUYSBDD-UHFFFAOYSA-N formyl(dimethyl)azanium;chloride Chemical compound [Cl-].C[N+](C)=CO SAVROPQJUYSBDD-UHFFFAOYSA-N 0.000 description 1
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 1
- 239000012442 inert solvent Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 150000004780 naphthols Chemical class 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- LMBFAGIMSUYTBN-MPZNNTNKSA-N teixobactin Chemical compound C([C@H](C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H](CCC(N)=O)C(=O)N[C@H]([C@@H](C)CC)C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H]1C(N[C@@H](C)C(=O)N[C@@H](C[C@@H]2NC(=N)NC2)C(=O)N[C@H](C(=O)O[C@H]1C)[C@@H](C)CC)=O)NC)C1=CC=CC=C1 LMBFAGIMSUYTBN-MPZNNTNKSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/96—Esters of carbonic or haloformic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C68/00—Preparation of esters of carbonic or haloformic acids
- C07C68/02—Preparation of esters of carbonic or haloformic acids from phosgene or haloformates
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
- C07D317/44—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 ortho- or peri-condensed with carbocyclic rings or ring systems
- C07D317/70—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 ortho- or peri-condensed with carbocyclic rings or ring systems condensed with ring systems containing two or more relevant rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D319/00—Heterocyclic compounds containing six-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D319/04—1,3-Dioxanes; Hydrogenated 1,3-dioxanes
- C07D319/08—1,3-Dioxanes; Hydrogenated 1,3-dioxanes condensed with carbocyclic rings or ring systems
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19712131555 DE2131555C3 (de) | 1971-06-25 | 1971-06-25 | Verfahren zur Herstellung von Chlorameisensäurephenylester |
| DE19722213408 DE2213408C2 (de) | 1972-03-20 | 1972-03-20 | Verfahren zur Herstellung von Chlorameisensäurearylestern |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU527132A3 true SU527132A3 (ru) | 1976-08-30 |
Family
ID=25761326
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1802668A SU527132A3 (ru) | 1971-06-25 | 1972-06-23 | Способ получени ариловых эфиров хлоругольной кислоты или циклических карбонатов |
Country Status (13)
| Country | Link |
|---|---|
| JP (1) | JPS5133897B1 (enExample) |
| AT (1) | AT332380B (enExample) |
| AU (1) | AU468132B2 (enExample) |
| BE (1) | BE785446A (enExample) |
| CA (1) | CA978979A (enExample) |
| CH (1) | CH586181A5 (enExample) |
| CS (1) | CS179385B2 (enExample) |
| DD (1) | DD97882A5 (enExample) |
| FR (1) | FR2143363B1 (enExample) |
| GB (1) | GB1400184A (enExample) |
| IT (1) | IT959950B (enExample) |
| NL (1) | NL7208416A (enExample) |
| SU (1) | SU527132A3 (enExample) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101741269B1 (ko) | 2009-06-26 | 2017-05-29 | 이데미쓰 고산 가부시키가이샤 | 비스클로로포메이트 화합물의 제조 방법, 저량체수 폴리카보네이트 올리고머, 및 비스클로로포메이트 화합물 함유 용액 |
| CN114920650B (zh) * | 2022-06-15 | 2024-06-18 | 江西亚太科技发展有限公司 | 一种用于分离4-硝基苯酚及4-硝基苯基氯甲酸酯的气相方法 |
-
1972
- 1972-06-20 NL NL7208416A patent/NL7208416A/xx active Search and Examination
- 1972-06-21 CS CS437672A patent/CS179385B2/cs unknown
- 1972-06-22 CH CH939172A patent/CH586181A5/xx not_active IP Right Cessation
- 1972-06-23 CA CA145,516A patent/CA978979A/en not_active Expired
- 1972-06-23 AU AU43817/72A patent/AU468132B2/en not_active Expired
- 1972-06-23 JP JP6246372A patent/JPS5133897B1/ja active Pending
- 1972-06-23 GB GB2959972A patent/GB1400184A/en not_active Expired
- 1972-06-23 AT AT540772A patent/AT332380B/de not_active IP Right Cessation
- 1972-06-23 FR FR7222734A patent/FR2143363B1/fr not_active Expired
- 1972-06-23 IT IT2615772A patent/IT959950B/it active
- 1972-06-23 SU SU1802668A patent/SU527132A3/ru active
- 1972-06-26 BE BE119178A patent/BE785446A/xx not_active IP Right Cessation
- 1972-06-26 DD DD16397272A patent/DD97882A5/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| AU468132B2 (en) | 1976-01-08 |
| CA978979A (en) | 1975-12-02 |
| GB1400184A (en) | 1975-07-16 |
| DD97882A5 (enExample) | 1973-05-20 |
| CH586181A5 (enExample) | 1977-03-31 |
| NL7208416A (enExample) | 1972-12-28 |
| FR2143363A1 (enExample) | 1973-02-02 |
| BE785446A (fr) | 1972-12-27 |
| FR2143363B1 (enExample) | 1977-12-23 |
| AT332380B (de) | 1976-09-27 |
| ATA540772A (de) | 1976-01-15 |
| JPS5133897B1 (enExample) | 1976-09-22 |
| CS179385B2 (en) | 1977-10-31 |
| AU4381772A (en) | 1974-01-03 |
| IT959950B (it) | 1973-11-10 |
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