SU519420A1 - Способ получени замещенных монои диамидов фосфористой кислоты - Google Patents
Способ получени замещенных монои диамидов фосфористой кислотыInfo
- Publication number
- SU519420A1 SU519420A1 SU1876010A SU1876010A SU519420A1 SU 519420 A1 SU519420 A1 SU 519420A1 SU 1876010 A SU1876010 A SU 1876010A SU 1876010 A SU1876010 A SU 1876010A SU 519420 A1 SU519420 A1 SU 519420A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- phosphorous
- anhydride
- obtaining
- phosphorous acid
- substituted
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 10
- 229910019142 PO4 Inorganic materials 0.000 title 1
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 title 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 title 1
- 239000010452 phosphate Substances 0.000 title 1
- VSAISIQCTGDGPU-UHFFFAOYSA-N phosphorus trioxide Inorganic materials O1P(O2)OP3OP1OP2O3 VSAISIQCTGDGPU-UHFFFAOYSA-N 0.000 claims description 8
- ISIJQEHRDSCQIU-UHFFFAOYSA-N tert-butyl 2,7-diazaspiro[4.5]decane-7-carboxylate Chemical compound C1N(C(=O)OC(C)(C)C)CCCC11CNCC1 ISIJQEHRDSCQIU-UHFFFAOYSA-N 0.000 claims description 6
- 238000000926 separation method Methods 0.000 claims description 4
- 150000001412 amines Chemical class 0.000 claims description 3
- 125000002723 alicyclic group Chemical group 0.000 claims 1
- 125000001931 aliphatic group Chemical group 0.000 claims 1
- 125000003118 aryl group Chemical group 0.000 claims 1
- 150000001470 diamides Chemical class 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 150000003018 phosphorus compounds Chemical class 0.000 claims 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 15
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 14
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 10
- 229910052698 phosphorus Inorganic materials 0.000 description 7
- 239000011574 phosphorus Substances 0.000 description 7
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 6
- 239000002244 precipitate Substances 0.000 description 6
- NQRYJNQNLNOLGT-UHFFFAOYSA-N Piperidine Chemical compound C1CCNCC1 NQRYJNQNLNOLGT-UHFFFAOYSA-N 0.000 description 4
- -1 alicyclic amines Chemical class 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- 239000013078 crystal Substances 0.000 description 4
- 239000000706 filtrate Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- NJBCRXCAPCODGX-UHFFFAOYSA-N 2-methyl-n-(2-methylpropyl)propan-1-amine Chemical compound CC(C)CNCC(C)C NJBCRXCAPCODGX-UHFFFAOYSA-N 0.000 description 3
- 238000004821 distillation Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 150000003863 ammonium salts Chemical class 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- SXADIBFZNXBEGI-UHFFFAOYSA-N phosphoramidous acid Chemical class NP(O)O SXADIBFZNXBEGI-UHFFFAOYSA-N 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- GKSKQDMOTNGGJV-UHFFFAOYSA-N C(C(C)C)N(P(O)O)CC(C)C Chemical compound C(C(C)C)N(P(O)O)CC(C)C GKSKQDMOTNGGJV-UHFFFAOYSA-N 0.000 description 1
- FOFIJPWHKQRVKT-UHFFFAOYSA-N C(C(C)C)NCC(C)C.C(C(C)C)NCC(C)C Chemical compound C(C(C)C)NCC(C)C.C(C(C)C)NCC(C)C FOFIJPWHKQRVKT-UHFFFAOYSA-N 0.000 description 1
- QBTKBZPWDYEFBL-UHFFFAOYSA-N P(O)(N1CCCCC1)N1CCCCC1 Chemical compound P(O)(N1CCCCC1)N1CCCCC1 QBTKBZPWDYEFBL-UHFFFAOYSA-N 0.000 description 1
- YQKSAIGZJMBURP-UHFFFAOYSA-N P(O)(O)O.NCCCC Chemical compound P(O)(O)O.NCCCC YQKSAIGZJMBURP-UHFFFAOYSA-N 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- HQABUPZFAYXKJW-UHFFFAOYSA-N butan-1-amine Chemical compound CCCCN HQABUPZFAYXKJW-UHFFFAOYSA-N 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- RLMOMHNXIWBGTF-UHFFFAOYSA-N diaminophosphinoamine Chemical class NP(N)N RLMOMHNXIWBGTF-UHFFFAOYSA-N 0.000 description 1
- ZLRAAUUPULJGTL-UHFFFAOYSA-N diaminophosphinous acid Chemical class NP(N)O ZLRAAUUPULJGTL-UHFFFAOYSA-N 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000001640 fractional crystallisation Methods 0.000 description 1
- 239000005457 ice water Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- GEQBPMNDDHGGPJ-UHFFFAOYSA-N tri(piperidin-1-yl)phosphane Chemical compound C1CCCCN1P(N1CCCCC1)N1CCCCC1 GEQBPMNDDHGGPJ-UHFFFAOYSA-N 0.000 description 1
- WUHCJANXMTUWBY-UHFFFAOYSA-N trihydroxy-bis(2-methylpropyl)-$l^{5}-phosphane Chemical compound CC(C)CP(O)(O)(O)CC(C)C WUHCJANXMTUWBY-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/22—Amides of acids of phosphorus
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DD16061272A DD100475A1 (forum.php) | 1972-01-31 | 1972-01-31 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU519420A1 true SU519420A1 (ru) | 1976-06-30 |
Family
ID=5485203
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1876010A SU519420A1 (ru) | 1972-01-31 | 1973-01-29 | Способ получени замещенных монои диамидов фосфористой кислоты |
Country Status (4)
| Country | Link |
|---|---|
| DD (1) | DD100475A1 (forum.php) |
| DE (1) | DE2300549A1 (forum.php) |
| NL (1) | NL7300793A (forum.php) |
| SU (1) | SU519420A1 (forum.php) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2417229C2 (ru) * | 2005-11-08 | 2011-04-27 | Басф Се | Способ выделения кислот из химических реакционных смесей с помощью неполярных аминов |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2017528451A (ja) * | 2014-08-19 | 2017-09-28 | ストライトマルク・ホールディング・アーゲー | 複素環式水素ホスフィンオキシドの合成のための方法 |
-
1972
- 1972-01-31 DD DD16061272A patent/DD100475A1/xx unknown
-
1973
- 1973-01-08 DE DE19732300549 patent/DE2300549A1/de active Pending
- 1973-01-19 NL NL7300793A patent/NL7300793A/xx unknown
- 1973-01-29 SU SU1876010A patent/SU519420A1/ru active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2417229C2 (ru) * | 2005-11-08 | 2011-04-27 | Басф Се | Способ выделения кислот из химических реакционных смесей с помощью неполярных аминов |
| RU2417229C9 (ru) * | 2005-11-08 | 2012-05-10 | Басф Се | Способ выделения кислот из химических реакционных смесей с помощью неполярных аминов |
Also Published As
| Publication number | Publication date |
|---|---|
| NL7300793A (forum.php) | 1973-08-02 |
| DD100475A1 (forum.php) | 1973-09-20 |
| DE2300549A1 (de) | 1973-08-09 |
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