SU490292A3 - Способ получени диалкоксифосфонометилгидантоинов - Google Patents
Способ получени диалкоксифосфонометилгидантоиновInfo
- Publication number
- SU490292A3 SU490292A3 SU1903202A SU1903202A SU490292A3 SU 490292 A3 SU490292 A3 SU 490292A3 SU 1903202 A SU1903202 A SU 1903202A SU 1903202 A SU1903202 A SU 1903202A SU 490292 A3 SU490292 A3 SU 490292A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- mol
- product
- temperature
- dimethylhydantoin
- dialkoxyphosphonomethylhydantoins
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000000047 product Substances 0.000 description 9
- 239000000203 mixture Substances 0.000 description 7
- NEHMKBQYUWJMIP-UHFFFAOYSA-N chloromethane Chemical compound ClC NEHMKBQYUWJMIP-UHFFFAOYSA-N 0.000 description 6
- 238000004821 distillation Methods 0.000 description 5
- BDZBKCUKTQZUTL-UHFFFAOYSA-N triethyl phosphite Chemical compound CCOP(OCC)OCC BDZBKCUKTQZUTL-UHFFFAOYSA-N 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- VFWCMGCRMGJXDK-UHFFFAOYSA-N 1-chlorobutane Chemical compound CCCCCl VFWCMGCRMGJXDK-UHFFFAOYSA-N 0.000 description 3
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
- 125000000217 alkyl group Chemical group 0.000 description 3
- 239000012043 crude product Substances 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N hexane Substances CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 229940050176 methyl chloride Drugs 0.000 description 3
- BBNYHDQRQXPHRX-UHFFFAOYSA-N 3-(chloromethyl)-5,5-dimethylimidazolidine-2,4-dione Chemical compound CC1(C)NC(=O)N(CCl)C1=O BBNYHDQRQXPHRX-UHFFFAOYSA-N 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 230000008030 elimination Effects 0.000 description 2
- 238000003379 elimination reaction Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 238000001953 recrystallisation Methods 0.000 description 2
- CYTQBVOFDCPGCX-UHFFFAOYSA-N trimethyl phosphite Chemical compound COP(OC)OC CYTQBVOFDCPGCX-UHFFFAOYSA-N 0.000 description 2
- -1 3-Di-n-butoxyphosphonomethyl-5, 5-dimethylhydantoin Chemical compound 0.000 description 1
- NIQFIROZARQJKP-UHFFFAOYSA-N 3-[bis(ethylperoxy)phosphorylmethyl]-5,5-dimethylimidazolidine-2,4-dione Chemical compound CCOOP(=O)(OOCC)CN1C(=O)NC(C)(C)C1=O NIQFIROZARQJKP-UHFFFAOYSA-N 0.000 description 1
- BADISKLZJQKRND-UHFFFAOYSA-N 3-[bis(methylperoxy)phosphorylmethyl]-5,5-dimethylimidazolidine-2,4-dione Chemical compound COOP(=O)(OOC)CN1C(=O)NC(C)(C)C1=O BADISKLZJQKRND-UHFFFAOYSA-N 0.000 description 1
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical group [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 125000002947 alkylene group Chemical group 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Chemical group BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 229910052794 bromium Chemical group 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 125000001309 chloro group Chemical group Cl* 0.000 description 1
- HRYZWHHZPQKTII-UHFFFAOYSA-N chloroethane Chemical compound CCCl HRYZWHHZPQKTII-UHFFFAOYSA-N 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 125000000753 cycloalkyl group Chemical group 0.000 description 1
- 229960003750 ethyl chloride Drugs 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 125000004970 halomethyl group Chemical group 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 125000001570 methylene group Chemical group [H]C([H])([*:1])[*:2] 0.000 description 1
- RGSFGYAAUTVSQA-UHFFFAOYSA-N pentamethylene Natural products C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 description 1
- 125000004817 pentamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/49—Phosphorus-containing compounds
- C08K5/51—Phosphorus bound to oxygen
- C08K5/53—Phosphorus bound to oxygen bound to oxygen and to carbon only
- C08K5/5317—Phosphonic compounds, e.g. R—P(:O)(OR')2
- C08K5/5333—Esters of phosphonic acids
- C08K5/5373—Esters of phosphonic acids containing heterocyclic rings not representing cyclic esters of phosphonic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/645—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having two nitrogen atoms as the only ring hetero atoms
- C07F9/6503—Five-membered rings
- C07F9/6506—Five-membered rings having the nitrogen atoms in positions 1 and 3
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/6558—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom containing at least two different or differently substituted hetero rings neither condensed among themselves nor condensed with a common carbocyclic ring or ring system
- C07F9/65583—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom containing at least two different or differently substituted hetero rings neither condensed among themselves nor condensed with a common carbocyclic ring or ring system each of the hetero rings containing nitrogen as ring hetero atom
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH489372 | 1972-04-04 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU490292A3 true SU490292A3 (ru) | 1975-10-30 |
Family
ID=4284357
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1903202A SU490292A3 (ru) | 1972-04-04 | 1973-04-04 | Способ получени диалкоксифосфонометилгидантоинов |
Country Status (13)
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3324127A (en) * | 1965-10-08 | 1967-06-06 | Standard Oil Co | Hydrouracil process |
-
1973
- 1973-03-30 NL NL7304490A patent/NL7304490A/xx unknown
- 1973-04-02 BR BR732355A patent/BR7302355D0/pt unknown
- 1973-04-02 DE DE2316382A patent/DE2316382A1/de active Pending
- 1973-04-02 DD DD169951A patent/DD106853A5/xx unknown
- 1973-04-03 IT IT22543/73A patent/IT981866B/it active
- 1973-04-03 GB GB1584773A patent/GB1424403A/en not_active Expired
- 1973-04-03 ZA ZA732272A patent/ZA732272B/xx unknown
- 1973-04-03 BE BE129568A patent/BE797688A/xx unknown
- 1973-04-03 JP JP48038203A patent/JPS497281A/ja active Pending
- 1973-04-03 FR FR7311925A patent/FR2179034B1/fr not_active Expired
- 1973-04-03 ES ES413278A patent/ES413278A1/es not_active Expired
- 1973-04-04 AU AU54112/73A patent/AU5411273A/en not_active Expired
- 1973-04-04 SU SU1903202A patent/SU490292A3/ru active
Also Published As
| Publication number | Publication date |
|---|---|
| BR7302355D0 (pt) | 1974-06-27 |
| DD106853A5 (enrdf_load_stackoverflow) | 1974-07-05 |
| DE2316382A1 (de) | 1973-10-25 |
| AU5411273A (en) | 1974-10-10 |
| NL7304490A (enrdf_load_stackoverflow) | 1973-10-08 |
| ZA732272B (en) | 1974-01-30 |
| BE797688A (fr) | 1973-10-03 |
| FR2179034A1 (enrdf_load_stackoverflow) | 1973-11-16 |
| IT981866B (it) | 1974-10-10 |
| ES413278A1 (es) | 1976-05-01 |
| JPS497281A (enrdf_load_stackoverflow) | 1974-01-22 |
| GB1424403A (en) | 1976-02-11 |
| FR2179034B1 (enrdf_load_stackoverflow) | 1975-12-26 |
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