SU482040A3 - Способ получени сложного метилового эфира (3-оксо-2-пропилциклопентил)-уксусной кислоты - Google Patents
Способ получени сложного метилового эфира (3-оксо-2-пропилциклопентил)-уксусной кислотыInfo
- Publication number
- SU482040A3 SU482040A3 SU1871017A SU1871017A SU482040A3 SU 482040 A3 SU482040 A3 SU 482040A3 SU 1871017 A SU1871017 A SU 1871017A SU 1871017 A SU1871017 A SU 1871017A SU 482040 A3 SU482040 A3 SU 482040A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- oxo
- acetic acid
- propylcyclopentyl
- methyl ester
- preparing
- Prior art date
Links
- 238000000034 method Methods 0.000 title description 7
- XIWMHTMGRGPLQO-UHFFFAOYSA-N methyl 2-(3-oxo-2-propylcyclopentyl)acetate Chemical compound CCCC1C(CC(=O)OC)CCC1=O XIWMHTMGRGPLQO-UHFFFAOYSA-N 0.000 title 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 9
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
- 229910052782 aluminium Inorganic materials 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 3
- -1 aluminum alcohols Chemical class 0.000 description 3
- 239000003054 catalyst Substances 0.000 description 3
- 238000005984 hydrogenation reaction Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 2
- WQDUMFSSJAZKTM-UHFFFAOYSA-N Sodium methoxide Chemical compound [Na+].[O-]C WQDUMFSSJAZKTM-UHFFFAOYSA-N 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 239000003208 petroleum Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- DYLIWHYUXAJDOJ-OWOJBTEDSA-N (e)-4-(6-aminopurin-9-yl)but-2-en-1-ol Chemical compound NC1=NC=NC2=C1N=CN2C\C=C\CO DYLIWHYUXAJDOJ-OWOJBTEDSA-N 0.000 description 1
- ZGCCZYRRIHZFCM-UHFFFAOYSA-N 2-(3-oxo-2-propylcyclopentyl)acetic acid Chemical compound CCCC1C(CC(O)=O)CCC1=O ZGCCZYRRIHZFCM-UHFFFAOYSA-N 0.000 description 1
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000009903 catalytic hydrogenation reaction Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 238000002329 infrared spectrum Methods 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 150000004702 methyl esters Chemical class 0.000 description 1
- NRQNMMBQPIGPTB-UHFFFAOYSA-N methylaluminum Chemical compound [CH3].[Al] NRQNMMBQPIGPTB-UHFFFAOYSA-N 0.000 description 1
- 125000000250 methylamino group Chemical group [H]N(*)C([H])([H])[H] 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000005809 transesterification reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/003—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing less than six carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fats And Perfumes (AREA)
- Cosmetics (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR727201510A FR2173652B1 (enExample) | 1972-01-18 | 1972-01-18 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU482040A3 true SU482040A3 (ru) | 1975-08-25 |
Family
ID=9092031
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1971534A SU484680A3 (ru) | 1972-01-18 | 1973-01-17 | Способ получени сложного метилового эфира (3-кето-2-пропилцикло-пентил)-уксусной кислоты |
| SU1871017A SU482040A3 (ru) | 1972-01-18 | 1973-01-17 | Способ получени сложного метилового эфира (3-оксо-2-пропилциклопентил)-уксусной кислоты |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1971534A SU484680A3 (ru) | 1972-01-18 | 1973-01-17 | Способ получени сложного метилового эфира (3-кето-2-пропилцикло-пентил)-уксусной кислоты |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US3970682A (enExample) |
| AR (1) | AR195995A1 (enExample) |
| AU (1) | AU446217B2 (enExample) |
| BE (1) | BE794233A (enExample) |
| BR (1) | BR7300334D0 (enExample) |
| CA (1) | CA992091A (enExample) |
| CH (1) | CH574243A5 (enExample) |
| ES (1) | ES410697A1 (enExample) |
| FR (1) | FR2173652B1 (enExample) |
| GB (1) | GB1347667A (enExample) |
| NL (1) | NL159362B (enExample) |
| SE (1) | SE389861B (enExample) |
| SU (2) | SU484680A3 (enExample) |
| ZA (1) | ZA728967B (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL179368C (nl) * | 1976-07-16 | 1986-09-01 | Roure Bertrand Dupont Sa | Werkwijze voor het bereiden van oxocyclopentyl- en oxocyclohexylverbindingen. |
| US4310701A (en) * | 1980-01-18 | 1982-01-12 | International Flavors & Fragrances Inc. | Process for the preparation of homologues of methyl dihydrojasmonate |
| US4537704A (en) * | 1983-12-21 | 1985-08-27 | International Flavors & Fragrances Inc. | Alkyl substituted and unsubstituted para-carboalkoxy cyclohexanones and organoleptic uses thereof |
| US4643903A (en) * | 1983-12-21 | 1987-02-17 | International Flavors & Fragrances Inc. | Alkyl substituted and unsubstituted para-carboalkoxy cyclohexanones and organoleptic uses thereof |
| US5235110A (en) * | 1989-05-23 | 1993-08-10 | Nippon Zeon Co., Ltd. | Fragrant composition |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH382731A (fr) * | 1960-02-25 | 1964-10-15 | Firmenich & Cie | Procédé pour la préparation de céto-esters alicycliques |
| CH490313A (fr) * | 1960-07-27 | 1970-05-15 | Demole Edouard | Procédé de préparation de cétoesters et utilisation des esters obtenus par ce procédé |
| NL289339A (enExample) * | 1962-02-23 | |||
| CH509247A (de) * | 1969-03-10 | 1971-06-30 | Givaudan & Cie Sa | Verfahren zur Herstellung von neuen Cycloalkenonestern |
-
0
- BE BE794233D patent/BE794233A/xx unknown
-
1972
- 1972-01-18 FR FR727201510A patent/FR2173652B1/fr not_active Expired
- 1972-12-18 CH CH1870772A patent/CH574243A5/xx not_active IP Right Cessation
- 1972-12-19 ZA ZA728967A patent/ZA728967B/xx unknown
- 1972-12-22 AU AU50469/72A patent/AU446217B2/en not_active Expired
-
1973
- 1973-01-11 US US05/322,748 patent/US3970682A/en not_active Expired - Lifetime
- 1973-01-16 AR AR246150A patent/AR195995A1/es active
- 1973-01-16 BR BR334/73A patent/BR7300334D0/pt unknown
- 1973-01-17 SU SU1971534A patent/SU484680A3/ru active
- 1973-01-17 SU SU1871017A patent/SU482040A3/ru active
- 1973-01-17 CA CA161,517A patent/CA992091A/en not_active Expired
- 1973-01-17 NL NL7300683.A patent/NL159362B/xx unknown
- 1973-01-17 GB GB246773A patent/GB1347667A/en not_active Expired
- 1973-01-17 ES ES410697A patent/ES410697A1/es not_active Expired
- 1973-01-17 SE SE7300658A patent/SE389861B/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| FR2173652A1 (enExample) | 1973-10-12 |
| GB1347667A (en) | 1974-02-27 |
| US3970682A (en) | 1976-07-20 |
| DE2301828B2 (de) | 1976-04-15 |
| CA992091A (en) | 1976-06-29 |
| CH574243A5 (enExample) | 1976-04-15 |
| ZA728967B (en) | 1973-09-26 |
| BR7300334D0 (pt) | 1974-01-08 |
| AU5046972A (en) | 1974-03-14 |
| SU484680A3 (ru) | 1975-09-15 |
| FR2173652B1 (enExample) | 1974-07-26 |
| AU446217B2 (en) | 1974-03-14 |
| AR195995A1 (es) | 1973-11-23 |
| SE389861B (sv) | 1976-11-22 |
| ES410697A1 (es) | 1976-04-01 |
| NL159362B (nl) | 1979-02-15 |
| BE794233A (fr) | 1973-07-18 |
| NL7300683A (enExample) | 1973-07-20 |
| DE2301828A1 (de) | 1973-07-19 |
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