SU410020A1 - - Google Patents

Info

Publication number

SU410020A1

SU410020A1 SU1778670A SU1778670A SU410020A1 SU 410020 A1 SU410020 A1 SU 410020A1 SU 1778670 A SU1778670 A SU 1778670A SU 1778670 A SU1778670 A SU 1778670A SU 410020 A1 SU410020 A1 SU 410020A1

Authority

SU

USSR - Soviet Union

Prior art keywords

iolifluoro

target product

mol

alkaline metal

polyfluoro

Prior art date

1972-04-27

Links

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• 238000000034 method Methods 0.000 claims description 6
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 4
• -1 alkylene glycol Chemical compound 0.000 claims description 4
• LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 4
• WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 3
• 239000003960 organic solvent Substances 0.000 claims description 3
• 238000010438 heat treatment Methods 0.000 claims description 2
• IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims description 2
• 229910000041 hydrogen chloride Inorganic materials 0.000 claims description 2
• 238000004519 manufacturing process Methods 0.000 claims description 2
• 239000002184 metal Substances 0.000 claims 2
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 1
• YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims 1
• 229910052731 fluorine Inorganic materials 0.000 claims 1
• 239000011737 fluorine Substances 0.000 claims 1
• RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 11
• ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 9
• SBZXBUIDTXKZTM-UHFFFAOYSA-N diglyme Chemical compound COCCOCCOC SBZXBUIDTXKZTM-UHFFFAOYSA-N 0.000 description 4
• 150000001875 compounds Chemical class 0.000 description 2
• UBIJTWDKTYCPMQ-UHFFFAOYSA-N hexachlorophosphazene Chemical compound ClP1(Cl)=NP(Cl)(Cl)=NP(Cl)(Cl)=N1 UBIJTWDKTYCPMQ-UHFFFAOYSA-N 0.000 description 2
• 239000000178 monomer Substances 0.000 description 2
• 229920000642 polymer Polymers 0.000 description 2
• 238000002360 preparation method Methods 0.000 description 2
• 239000000047 product Substances 0.000 description 2
• 239000011541 reaction mixture Substances 0.000 description 2
• 239000000243 solution Substances 0.000 description 2
• 238000001228 spectrum Methods 0.000 description 2
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
• RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
• DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
• 239000007983 Tris buffer Substances 0.000 description 1
• 150000001298 alcohols Chemical class 0.000 description 1
• 229910052783 alkali metal Inorganic materials 0.000 description 1
• 238000009835 boiling Methods 0.000 description 1
• 239000007795 chemical reaction product Substances 0.000 description 1
• 238000001816 cooling Methods 0.000 description 1
• 238000002955 isolation Methods 0.000 description 1
• 239000000203 mixture Substances 0.000 description 1
• 150000004812 organic fluorine compounds Chemical class 0.000 description 1
• 239000002244 precipitate Substances 0.000 description 1
• 229910052708 sodium Inorganic materials 0.000 description 1
• 239000011734 sodium Substances 0.000 description 1
• 239000002904 solvent Substances 0.000 description 1
• 150000003512 tertiary amines Chemical class 0.000 description 1