SU388498A1 - Method of obtaining lithium metatantalate monocrystals - Google Patents

Method of obtaining lithium metatantalate monocrystals

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Publication number
SU388498A1
SU388498A1 SU701481624A SU1481624A SU388498A1 SU 388498 A1 SU388498 A1 SU 388498A1 SU 701481624 A SU701481624 A SU 701481624A SU 1481624 A SU1481624 A SU 1481624A SU 388498 A1 SU388498 A1 SU 388498A1
Authority
SU
USSR - Soviet Union
Prior art keywords
monocrystals
obtaining lithium
temperature
metatantalate
lithium metatantalate
Prior art date
Application number
SU701481624A
Other languages
Russian (ru)
Inventor
Н.Б. Ангерт
В.М. Гармаш
В.П. Клюев
Ю.М. Колбацков
Original Assignee
Angert N B
Garmash V M
Klyuev V P
Kolbatskov Yu M
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Angert N B, Garmash V M, Klyuev V P, Kolbatskov Yu M filed Critical Angert N B
Priority to SU701481624A priority Critical patent/SU388498A1/en
Application granted granted Critical
Publication of SU388498A1 publication Critical patent/SU388498A1/en

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Description

(54) СПСХХШ ПОЛУЧЕНИЯ МОНОДОМЕННЫХ КРИСТАЛЛОВ МЕТАТАЩ-АЛАТА ЛИТИЯ Предлагаемый способ относитс  s технологии получени  моаодомениьгх мощж|ш гад ол сегветозпеЕ рвка метатантелата лвтв . Моиодомев{Ш1е К| ас7вк ы метатйвтадатв niJTSM нгу;д т iteposoe применена® юмвтишой j-;seit-if oaiuis ДЛЕ мо/  авет лйэерк го ., а также прако&вте руировазшн некот кАЯ схем в вьвзо «хш же. К|жсташав метата талата ЯЯТЕЯ в iстс щее врем  клрашпвают вэ расплава методом Чохральского. Получение монодомешшх . кристаллов, сегнетоэлектркков сводитс  к о-лжигу образцов с приложением электричесЕОГо ss- л  при опредаленной температуре - во близЁоЗ к точке . Известен способ получеш   монодомвв: ных кристаллов метатантапата лити  путем отжига образцов с ванесе шми ва поверхность, перпендикул рно оси Z , апект родами под посто нным электрическим полем при температуре, близкой к температуре Кю1ри, с последующим охлажденвем. Цель изобретени  - получение 9О5&-вс го «лхода годных кристаллов, ускоревве процесса в улучшение качества конечного продукта. Дл  этого провесе ведут 1фх температуре не более чем на 5 С ниже температуры в течввве 5О-7О кпш в напр  сев оств алектрвческого пол  Б (5 + О.О05Т) В/см дл  Т 62О°С. где Т - температура Кюри, а Т - TK и Е (5 О,5Т) В/см дл  Т,; 62О С, с послеоуюшим охлаждением со скоростью 6О-9О С/ч, снима  электрическое попе при температуре на BO-IOO C ниже температуры Кюри. Пример. Берут 374,0 г Та.О CXC.-i: т 78.5 г , О.С.Ч. Состав кс йпоакщ1И состветствует соотношению ионов JisiTfja к тантала в расплаве, равном 1. Смесь этих продуктов перемещввают в течение 24 ч в полиэтиленовом « суде и брикетируют под давлением 15О атм в таблет ш диаметром 48 мм. Тигель ппатино родиевый 56x3x53 с платиновым вкладышем 50х2х5О мм ус(54) ASCHSHSH OBTAINING OF MONODOMENIC LITHIUM METATASTAL-ALATE CRYSTALS The proposed method relates to the technology of obtaining myodomeny power amplifiers of metatantelate lvtv. Moyodomev {Ш1е К | assumptions of metatvatatv niJTSM ngu; d t iteposoe is applied® by jumbo j-; seit-if oaiuis DLE mo / avet lyerk go., as well as practice and integrate some of the schemes in the same way. To | zhashashav metat talata YAYATEYA at the present time, they melt the melt by the Czochralski method. Getting monodomeshhshh. crystals, ferroelectric solids is reduced to o-lying of samples with the application of electrical ssl at a certain temperature - close to the point. The known method is obtained from monodomas: metatanthapatite lithium crystals by annealing the samples with a vanesha surface, perpendicular to the Z axis, by means of a genera under a constant electric field at a temperature close to the Cu1ri temperature, followed by cooling. The purpose of the invention is to obtain a 9O5 & all of the suitable crystals, accelerating the process in improving the quality of the final product. For this sag, the 1fx temperature is not more than 5 ° C lower than the temperature in 5O-7O kpsh in the direction of sowing in the electric field B (5 + OO05T) V / cm for T 62O ° C. where T is the Curie temperature, and T is TK and E (5 O, 5T) V / cm for T; 62O C, with subsequent cooling at a rate of 6O-9O C / h, remove the electric bottom at a temperature at BO-IOO C below the Curie temperature. Example. Take 374.0 g of Ta.O. CXC.-i: t 78.5 g, O.C. The composition of the copolyacid corresponds to the ratio of JisiTfja ions to tantalum in the melt equal to 1. The mixture of these products is transferred for 24 hours in a polyethylene vessel and is briquetted under a pressure of 15O atm into a tablet with a diameter of 48 mm. Crucible patatino rhodium 56x3x53 with platinum liner 50x2x5O mm mustache

SU701481624A 1970-10-08 1970-10-08 Method of obtaining lithium metatantalate monocrystals SU388498A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU701481624A SU388498A1 (en) 1970-10-08 1970-10-08 Method of obtaining lithium metatantalate monocrystals

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU701481624A SU388498A1 (en) 1970-10-08 1970-10-08 Method of obtaining lithium metatantalate monocrystals

Publications (1)

Publication Number Publication Date
SU388498A1 true SU388498A1 (en) 1979-07-25

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Application Number Title Priority Date Filing Date
SU701481624A SU388498A1 (en) 1970-10-08 1970-10-08 Method of obtaining lithium metatantalate monocrystals

Country Status (1)

Country Link
SU (1) SU388498A1 (en)

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