SU375295A1 - - Google Patents

Info

Publication number

SU375295A1

SU375295A1 SU1696156A SU1696156A SU375295A1 SU 375295 A1 SU375295 A1 SU 375295A1 SU 1696156 A SU1696156 A SU 1696156A SU 1696156 A SU1696156 A SU 1696156A SU 375295 A1 SU375295 A1 SU 375295A1

Authority

SU

USSR - Soviet Union

Prior art keywords

germanium

yield

mixture

alkyl halides

reaction

Prior art date

1971-08-30

Links

• Espacenet
• Global Dossier
• Discuss

• 229910052732 germanium Inorganic materials 0.000 description 11
• 238000000034 method Methods 0.000 description 9
• 239000000203 mixture Substances 0.000 description 7
• -1 germanium alkyl halides Chemical class 0.000 description 6
• 239000000047 product Substances 0.000 description 5
• GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 description 4
• HDVLQIDIYKIVRE-UHFFFAOYSA-N tetrabutylgermane Chemical compound CCCC[Ge](CCCC)(CCCC)CCCC HDVLQIDIYKIVRE-UHFFFAOYSA-N 0.000 description 4
• 238000006243 chemical reaction Methods 0.000 description 3
• 230000015572 biosynthetic process Effects 0.000 description 2
• 238000004519 manufacturing process Methods 0.000 description 2
• 238000002360 preparation method Methods 0.000 description 2
• 239000011541 reaction mixture Substances 0.000 description 2
• 238000000926 separation method Methods 0.000 description 2
• 238000003786 synthesis reaction Methods 0.000 description 2
• CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 description 1
• 239000004215 Carbon black (E152) Substances 0.000 description 1
• 229910005742 Ge—C Inorganic materials 0.000 description 1
• 125000000217 alkyl group Chemical group 0.000 description 1
• 239000003708 ampul Substances 0.000 description 1
• JTCNNBSUKPHDMI-UHFFFAOYSA-N bromo(tributyl)germane Chemical compound CCCC[Ge](Br)(CCCC)CCCC JTCNNBSUKPHDMI-UHFFFAOYSA-N 0.000 description 1
• BDMFYHHLDXQFQD-UHFFFAOYSA-N butyl(trichloro)germane Chemical compound CCCC[Ge](Cl)(Cl)Cl BDMFYHHLDXQFQD-UHFFFAOYSA-N 0.000 description 1
• 239000006227 byproduct Substances 0.000 description 1
• 239000003054 catalyst Substances 0.000 description 1
• 239000007795 chemical reaction product Substances 0.000 description 1
• 230000006378 damage Effects 0.000 description 1
• 238000000605 extraction Methods 0.000 description 1
• 150000004820 halides Chemical class 0.000 description 1
• 229910052736 halogen Inorganic materials 0.000 description 1
• 150000002367 halogens Chemical group 0.000 description 1
• 238000010438 heat treatment Methods 0.000 description 1
• 229930195733 hydrocarbon Natural products 0.000 description 1
• 238000002955 isolation Methods 0.000 description 1
• 125000000082 organogermanium group Chemical group 0.000 description 1
• 125000002524 organometallic group Chemical group 0.000 description 1
• 239000002994 raw material Substances 0.000 description 1
• 238000001577 simple distillation Methods 0.000 description 1
• IEXRMSFAVATTJX-UHFFFAOYSA-N tetrachlorogermane Chemical compound Cl[Ge](Cl)(Cl)Cl IEXRMSFAVATTJX-UHFFFAOYSA-N 0.000 description 1
• 238000005979 thermal decomposition reaction Methods 0.000 description 1
• QPESFDZECLNXAL-UHFFFAOYSA-N tribromo(butyl)germane Chemical compound CCCC[Ge](Br)(Br)Br QPESFDZECLNXAL-UHFFFAOYSA-N 0.000 description 1
• MWNSUONCJRRKFE-UHFFFAOYSA-N tributyl(chloro)germane Chemical compound CCCC[Ge](Cl)(CCCC)CCCC MWNSUONCJRRKFE-UHFFFAOYSA-N 0.000 description 1