SU352894A1 - - Google Patents
Info
- Publication number
- SU352894A1 SU352894A1 SU1600110A SU1600110A SU352894A1 SU 352894 A1 SU352894 A1 SU 352894A1 SU 1600110 A SU1600110 A SU 1600110A SU 1600110 A SU1600110 A SU 1600110A SU 352894 A1 SU352894 A1 SU 352894A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- phenol
- methadioxane
- yield
- reaction
- target product
- Prior art date
Links
- 238000000034 method Methods 0.000 claims description 10
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 9
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 125000002877 alkyl aryl group Chemical group 0.000 claims 2
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims 1
- 125000001475 halogen functional group Chemical group 0.000 claims 1
- -1 hydroxyphenylethyl Chemical group 0.000 claims 1
- 229910000077 silane Inorganic materials 0.000 claims 1
- 239000000047 product Substances 0.000 description 9
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 5
- 239000003054 catalyst Substances 0.000 description 4
- 230000002378 acidificating effect Effects 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 description 2
- IJOOHPMOJXWVHK-UHFFFAOYSA-N chlorotrimethylsilane Chemical compound C[Si](C)(C)Cl IJOOHPMOJXWVHK-UHFFFAOYSA-N 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 239000012429 reaction media Substances 0.000 description 2
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical compound CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 description 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- 229930185605 Bisphenol Natural products 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 1
- VSCMNSZBNLOXNR-UHFFFAOYSA-N bromo(triphenyl)silane Chemical compound C=1C=CC=CC=1[Si](C=1C=CC=CC=1)(Br)C1=CC=CC=C1 VSCMNSZBNLOXNR-UHFFFAOYSA-N 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- QABCGOSYZHCPGN-UHFFFAOYSA-N chloro(dimethyl)silicon Chemical compound C[Si](C)Cl QABCGOSYZHCPGN-UHFFFAOYSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000005051 trimethylchlorosilane Substances 0.000 description 1
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU352894A1 true SU352894A1 (enrdf_load_stackoverflow) |
Family
ID=
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR20200070127A (ko) | 트리아세톤 아민을 제조하는 개선된 방법 | |
| EP0447074A2 (en) | Catalytic isocyanate trimerization and urethane formation | |
| US2462433A (en) | Preparation of organic thiocyanates and isothiocyanates | |
| EP3935041B1 (en) | Integrated methods and systems for producing amide and nitrile compounds | |
| SU352894A1 (enrdf_load_stackoverflow) | ||
| JPS58164549A (ja) | アリ−ルヒドロキシルアミンの製造方法 | |
| US3393241A (en) | Preparation of nitrodiarylamines | |
| US4080392A (en) | Process for the production of aromatic trifluoromethyl compounds of the benzene series | |
| JPS625418B2 (enrdf_load_stackoverflow) | ||
| US3839387A (en) | Process for preparing n-trimethyl-silylacetamide | |
| SU560529A3 (ru) | Способ получени амидов карбоновых кислот | |
| US2817681A (en) | Arylacetic acids | |
| JPS635060A (ja) | ４−ニトロジフエニルアミンの製造方法 | |
| JPS59222449A (ja) | ジフエニルアミン及びアニリンの製法 | |
| US2561787A (en) | Production of nitriles | |
| SU1093243A3 (ru) | Способ получени бензоилцианида | |
| JP3864997B2 (ja) | ２，４−オキサゾリジンジオン類の製造方法 | |
| JPH0313229B2 (enrdf_load_stackoverflow) | ||
| JP4576667B2 (ja) | ３，９−ビス（２−ヒドロキシ−１，１−ジメチルエチル）−２，４，８，１０−テトラオキサスピロ［５．５］ウンデカンの製造方法 | |
| SU627134A1 (ru) | Способ получени тетрафурфурилоксисилана | |
| Abbasov et al. | SOME PROPERTIES OF ACYLATION REACTION OF PARA-(1-(CYCLOHEX-3-EN-1-YL) ETHYL) PEHOL WITH ACETIC ACID | |
| SU867297A3 (ru) | Способ получени бензоилцианида | |
| SU309522A1 (ru) | СПОСОБ ПОЛУЧЕНИЯ АЛКИЛ-ИЛИ ЦИКЛОАЛКИЛ- ХЛОРИДОВ или БРОМИДОВ ОЛОВА | |
| JPS6334854B2 (enrdf_load_stackoverflow) | ||
| SU370221A1 (ru) | СПОСОБ ПОЛУЧЕНИЯ а,со-ДИГИДРОКСИПОЛИДИОРГАНО- |