SU242896A1 - - Google Patents
Info
- Publication number
- SU242896A1 SU242896A1 SU1218517A SU1218517A SU242896A1 SU 242896 A1 SU242896 A1 SU 242896A1 SU 1218517 A SU1218517 A SU 1218517A SU 1218517 A SU1218517 A SU 1218517A SU 242896 A1 SU242896 A1 SU 242896A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- methyl
- phenol
- ethyl
- product
- butyl alcohol
- Prior art date
Links
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- -1 methyl ethyl Chemical group 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000002329 infrared spectrum Methods 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- HMNKTRSOROOSPP-UHFFFAOYSA-N 3-Ethylphenol Chemical compound CCC1=CC=CC(O)=C1 HMNKTRSOROOSPP-UHFFFAOYSA-N 0.000 description 1
- VJOWMORERYNYON-UHFFFAOYSA-N 5-ethenyl-2-methylpyridine Chemical compound CC1=CC=C(C=C)C=N1 VJOWMORERYNYON-UHFFFAOYSA-N 0.000 description 1
- 229910021634 Rhenium(III) chloride Inorganic materials 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000005804 alkylation reaction Methods 0.000 description 1
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 1
- PASDCCFISLVPSO-UHFFFAOYSA-N benzoyl chloride Chemical compound ClC(=O)C1=CC=CC=C1 PASDCCFISLVPSO-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000000994 depressogenic effect Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 1
- 235000019341 magnesium sulphate Nutrition 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 125000001424 substituent group Chemical group 0.000 description 1
- LOIHSHVELSAXQN-UHFFFAOYSA-K trirhenium nonachloride Chemical compound Cl[Re](Cl)Cl LOIHSHVELSAXQN-UHFFFAOYSA-K 0.000 description 1
- 229940117958 vinyl acetate Drugs 0.000 description 1
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU242896A1 true SU242896A1 (enExample) |
Family
ID=
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CA2658652C (en) | Novel process for the synthesis of (e)-stilbene derivatives which makes it possible to obtain resveratrol and piceatannol | |
| KR20110100311A (ko) | 치환된 페닐렌 방향족 디에스테르의 제조 | |
| US4218567A (en) | Process for aromatic ethers | |
| CN115636731A (zh) | 一种2,4-二枯基苯酚的合成方法 | |
| SU242896A1 (enExample) | ||
| JP5827694B2 (ja) | アルジトールアセタールの製造方法 | |
| US2769833A (en) | Production of phenoxy acid esters through the potassium phenolate | |
| KR101707237B1 (ko) | 치환된 1,4-퀴논 메티드의 제조 방법 | |
| CN119191929A (zh) | 一种联枯及其制备方法与应用 | |
| Haworth et al. | 311. The constituents of guaiacum resin. Part II. Synthesis of dl-guaiaretic acid dimethyl ether | |
| CN116283504A (zh) | 一种2,4-二枯基酚的合成方法 | |
| JP2594826B2 (ja) | ｐ−またはｍ−ヒドロキシフェネチルアルコールの製造法 | |
| CN102627626A (zh) | 一种2,3-二醛基噻吩的制备方法 | |
| KR100293646B1 (ko) | 해당알독심의탈수반응을통하여오르토-하이드록시치환된방향족니트릴을제조하는방법 | |
| KR100201518B1 (ko) | 2-알킬-4-아실-6-3급-부틸페놀 화합물의 제조방법 | |
| CN110845331A (zh) | 一种苯甲酸高碳醇酯的制备方法 | |
| RU2423343C2 (ru) | Способ получения высокочистого, свободного от галогенов о-фталальдегида | |
| RU2807280C1 (ru) | Ресурсосберегающий способ получения фенилацетилена | |
| GB1561464A (en) | Oxidation of alkaryl compounds | |
| CN109678687B (zh) | 一种邻羟基苯乙酮类化合物的高效制备方法 | |
| CN110862318B (zh) | 一种叔丁基取代羟基苯甲酸酯的制备方法 | |
| CN113754527B (zh) | 一种醚菌酯中间体的合成方法 | |
| WO1998011039A1 (fr) | Procede de chloromethylation d'hydrocarbures aromatiques | |
| SU238534A1 (ru) | Способ получения 4-алкокси-3-метил-2-хлор-1- толилбутанов | |
| WO1998005630A1 (en) | Process for the preparation of organic nitriles |