SU1761750A1 - 1-hexyl-4-isonitroso-3-methyl-2-pyrazoline-5-on as an extraction reagent of zinc, cadmium or nickel - Google Patents

1-hexyl-4-isonitroso-3-methyl-2-pyrazoline-5-on as an extraction reagent of zinc, cadmium or nickel Download PDF

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Publication number
SU1761750A1
SU1761750A1 SU904853273A SU4853273A SU1761750A1 SU 1761750 A1 SU1761750 A1 SU 1761750A1 SU 904853273 A SU904853273 A SU 904853273A SU 4853273 A SU4853273 A SU 4853273A SU 1761750 A1 SU1761750 A1 SU 1761750A1
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SU
USSR - Soviet Union
Prior art keywords
hexyl
methyl
nickel
isonitroso
cadmium
Prior art date
Application number
SU904853273A
Other languages
Russian (ru)
Inventor
Петр Тимофеевич Павлов
Андрей Евгеньевич Леснов
Борис Иосифович Петров
Оксана Юрьевна Галкина
Original Assignee
Пермский государственный университет им.А.М.Горького
Институт органической химии Уральского отделения АН СССР
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Application filed by Пермский государственный университет им.А.М.Горького, Институт органической химии Уральского отделения АН СССР filed Critical Пермский государственный университет им.А.М.Горького
Priority to SU904853273A priority Critical patent/SU1761750A1/en
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Publication of SU1761750A1 publication Critical patent/SU1761750A1/en

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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

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  • Nitrogen Condensed Heterocyclic Rings (AREA)

Abstract

Использование: в качестве экстракционного реагента цинка, кадми  или никел . Сущность изобретени : продукт - 1-гексил- 4-изонитрозо-3-метил-2-пиразолин-5-он, БФСюН1 №02, выход 93,5%, т.пл.85-87°С. Реагент 1 - 1-гексил-4-изонитрозо-3-метил- 2-пиразолин-5-он. Реагент 2 - нитрит натри . Услови  реакции: в смеси метанола и 15%-ной HCI. 1 табл., 3 ил.Use: as an extraction reagent zinc, cadmium or nickel. The essence of the invention: the product is 1-hexyl-4-isonitroso-3-methyl-2-pyrazolin-5-one, BFSN1 No. 02, yield 93.5%, mp 85-87 ° C. Reagent 1 - 1-hexyl-4-isonitroso-3-methyl-2-pyrazolin-5-one. Reagent 2 is sodium nitrite. Reaction conditions: in a mixture of methanol and 15% HCI. 1 tab., 3 Il.

Description

KCd т / KCd t /

80 I80 I

1one

77

8989

фие. 1fie. one

РЯрав.Riarav.

20 -о20th

five. 2five. 2

рМрав.mrav.

/ pMpcrfa./ pMpcrfa.

Claims (1)

Формула изобретения 1-Гексил-4-изонитрозо-3-метил-2-пиразолин-5-он формулы C6H13 как экстракционный реагент цинка, кадмия или никеля.The claims 1-Hexyl-4-isonitrozo-3-methyl-2-pyrazolin-5-one of the formula C 6 H 13 as an extraction reagent of zinc, cadmium or nickel. Влияние концентрации реагентов на экстракцию 0,01 М никеля из 0,5 М раствора аммиакаThe effect of the concentration of reagents on the extraction of 0.01 M Nickel from 0.5 M ammonia solution Концентрация реагента, М Reagent concentration, M RNi, % RNi,% Соединение I Compound I Соединение II Compound II 0,005 0.005 24 24 16 16 0,01 0.01 46 46 36 36 0,015 0.015 68 68 57 57 0,0175 0.0175 78 78 65 65
фиг. /FIG. / Фиг. 2FIG. 2
SU904853273A 1990-07-18 1990-07-18 1-hexyl-4-isonitroso-3-methyl-2-pyrazoline-5-on as an extraction reagent of zinc, cadmium or nickel SU1761750A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU904853273A SU1761750A1 (en) 1990-07-18 1990-07-18 1-hexyl-4-isonitroso-3-methyl-2-pyrazoline-5-on as an extraction reagent of zinc, cadmium or nickel

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU904853273A SU1761750A1 (en) 1990-07-18 1990-07-18 1-hexyl-4-isonitroso-3-methyl-2-pyrazoline-5-on as an extraction reagent of zinc, cadmium or nickel

Publications (1)

Publication Number Publication Date
SU1761750A1 true SU1761750A1 (en) 1992-09-15

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
SU904853273A SU1761750A1 (en) 1990-07-18 1990-07-18 1-hexyl-4-isonitroso-3-methyl-2-pyrazoline-5-on as an extraction reagent of zinc, cadmium or nickel

Country Status (1)

Country Link
SU (1) SU1761750A1 (en)

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
РЖ Хим., 1979, 17В 220. *

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