SU159498A1 - - Google Patents

Info

Publication number

SU159498A1

SU159498A1 SU806968A SU806968A SU159498A1 SU 159498 A1 SU159498 A1 SU 159498A1 SU 806968 A SU806968 A SU 806968A SU 806968 A SU806968 A SU 806968A SU 159498 A1 SU159498 A1 SU 159498A1

Authority

SU

USSR - Soviet Union

Prior art keywords

nitrophenyl

nitropropylene

sulfuric acid

nitrate

propyl nitrate

Prior art date

Links

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• 238000000034 method Methods 0.000 description 5
• -1 1- (l-nitrophenyl) propyl Chemical group 0.000 description 4
• 229910002651 NO3 Inorganic materials 0.000 description 4
• QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
• 239000000047 product Substances 0.000 description 3
• GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 2
• DYUQAZSOFZSPHD-UHFFFAOYSA-N Phenylpropanol Chemical compound CCC(O)C1=CC=CC=C1 DYUQAZSOFZSPHD-UHFFFAOYSA-N 0.000 description 2
• 229910017604 nitric acid Inorganic materials 0.000 description 2
• 238000002360 preparation method Methods 0.000 description 2
• DBWBKROWASFCCD-UHFFFAOYSA-N 1-nitro-2-(2-nitroprop-1-enyl)benzene Chemical group [O-][N+](=O)C(C)=CC1=CC=CC=C1[N+]([O-])=O DBWBKROWASFCCD-UHFFFAOYSA-N 0.000 description 1
• NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 1
• VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
• IOVCWXUNBOPUCH-UHFFFAOYSA-M Nitrite anion Chemical compound [O-]N=O IOVCWXUNBOPUCH-UHFFFAOYSA-M 0.000 description 1
• RJIXBYBWNAFXMR-UHFFFAOYSA-N [N+](=O)([O-])C(=C(C)[N+](=O)[O-])C1=CC=CC=C1 Chemical group [N+](=O)([O-])C(=C(C)[N+](=O)[O-])C1=CC=CC=C1 RJIXBYBWNAFXMR-UHFFFAOYSA-N 0.000 description 1
• 150000001412 amines Chemical class 0.000 description 1
• QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
• 235000011114 ammonium hydroxide Nutrition 0.000 description 1
• 230000000844 anti-bacterial effect Effects 0.000 description 1
• 238000009835 boiling Methods 0.000 description 1
• 239000003245 coal Substances 0.000 description 1
• 238000009833 condensation Methods 0.000 description 1
• 230000005494 condensation Effects 0.000 description 1
• 239000013078 crystal Substances 0.000 description 1
• 238000010438 heat treatment Methods 0.000 description 1
• 238000004519 manufacturing process Methods 0.000 description 1
• 238000006396 nitration reaction Methods 0.000 description 1
• MCSAJNNLRCFZED-UHFFFAOYSA-N nitroethane Chemical compound CC[N+]([O-])=O MCSAJNNLRCFZED-UHFFFAOYSA-N 0.000 description 1
• 125000000636 p-nitrophenyl group Chemical group [H]C1=C([H])C(=C([H])C([H])=C1*)[N+]([O-])=O 0.000 description 1
• 239000002244 precipitate Substances 0.000 description 1
• JNTOKFNBDFMTIV-UHFFFAOYSA-N propyl nitrate Chemical compound CCCO[N+]([O-])=O JNTOKFNBDFMTIV-UHFFFAOYSA-N 0.000 description 1
• 239000011541 reaction mixture Substances 0.000 description 1
• 238000001953 recrystallisation Methods 0.000 description 1
• 238000003756 stirring Methods 0.000 description 1
• 239000000126 substance Substances 0.000 description 1
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1