SU126571A1 - A method of extracting rose oil with a solvent and apparatus for carrying out the method - Google Patents
A method of extracting rose oil with a solvent and apparatus for carrying out the methodInfo
- Publication number
- SU126571A1 SU126571A1 SU629858A SU629858A SU126571A1 SU 126571 A1 SU126571 A1 SU 126571A1 SU 629858 A SU629858 A SU 629858A SU 629858 A SU629858 A SU 629858A SU 126571 A1 SU126571 A1 SU 126571A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- solvent
- rose oil
- carrying
- extracting rose
- extracting
- Prior art date
Links
Landscapes
- Extraction Or Liquid Replacement (AREA)
- Fats And Perfumes (AREA)
Description
На предпри ти х эфиромасличной промышленности розовое масло из дистил циоиных вод выдел етс путем сорбции активированиым углем и последующего извлечеии из угл сериым эфиром; при этом тер етс значительное количество розового масла и серного эфира, а процесс извлечени розового масла, поглощенного углем, протекает медленно. .In plants of the essential oil industry, rose oil from distilled water is extracted by sorption with activated charcoal and subsequent extraction from coal with serum ether; significant amounts of rose oil and sulfuric ether are lost, and the process of extracting rose oil absorbed by coal proceeds slowly. .
Насто щее изобретение позвол ет интенсифицировать процесс экстрагировани розового масла растворите чем из гидродистилл та паровой фазы. Это достигаетс тем, что вод ной пар в смеси с розовым маслом подвергают тонкому диспергированию в растворителе.The present invention allows to intensify the process of extraction of rose oil, dissolve than from hydro-distillate vapor phase. This is achieved in that water vapor mixed with rose oil is finely dispersed in a solvent.
Дл осуществлени способа предлагаетс аппарат с применением холодильников, дефлегматора и водоотделител . Аппарат выполнен в виде насадочной колонны, в верхней расширенной части которой, наполн емой растворителем, установлен пароструйный эжектор дл диспергировани в растворитель паровой фазы из перегонного аппарата.To implement the method, an apparatus is proposed using refrigerators, a dephlegmator and a water separator. The apparatus is designed as a packed column, in the upper expanded part of which, filled with a solvent, a steam ejector is installed to disperse the vapor phase into the solvent from the distillation apparatus.
Дл экономии растворител в насадочной колонне установлен клапанный регул тор, сблокированный с поплавковым регул тором уровн мисцеллы в верхней части аппарата, с целью дополнительной подачи отработанного растворител в колонну.To save the solvent, a valve regulator is interlocked in the packed column with the float level regulator of the miscella level in the upper part of the apparatus in order to add additional spent solvent to the column.
Аппарат (см. чертеж) представл ет собой насадочную колонну /, верхн расширенна часть 2 которой, заполненна растворителем, служит дл диспергировани в растворитель паровой фазы, нагнетаемой пароструйным инжектором 3 из перегонного аппарата 4.The apparatus (see drawing) is a packed column /, the upper expanded part 2 of which, filled with solvent, serves to disperse the vapor phase into the solvent, which is injected with a steam jet injector 3 from the distillation unit 4.
Пар конденсируетс в мелко дисперсном состо нии и отдает скрытую теплоту испарени растворителю, который при этом нагреваетс до кипени и частично испар етс . Пары растворител , пройд холодильник 5, конденсируютс и поступают в сборник 6 дл вторичного использовани . .The vapor condenses in a finely dispersed state and gives up the latent heat of evaporation to the solvent, which at the same time heats up to a boiling point and partially evaporates. Solvent vapors that pass through cooler 5 condense and enter collection 6 for reuse. .
Мисцелла, отобранна с верхнего уровн экстрактора, пройд водоотделитель 7, поступает в выпарной аппарат 8, в котором вторично отобранна мисцелла идет на укрепление посредством вакуум-отгонки, а пары растворител , сконденсировавшиес в холодильнике 9, поступают вThe miscell, selected from the upper level of the extractor, has passed the water separator 7, enters the evaporator 8, in which the secondary selected miscella is strengthened by vacuum distillation, and the solvent vapor condensed in the refrigerator 9 enters
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU629858A SU126571A1 (en) | 1959-06-01 | 1959-06-01 | A method of extracting rose oil with a solvent and apparatus for carrying out the method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU629858A SU126571A1 (en) | 1959-06-01 | 1959-06-01 | A method of extracting rose oil with a solvent and apparatus for carrying out the method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU126571A1 true SU126571A1 (en) | 1959-11-30 |
Family
ID=48397853
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU629858A SU126571A1 (en) | 1959-06-01 | 1959-06-01 | A method of extracting rose oil with a solvent and apparatus for carrying out the method |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU126571A1 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU167702U1 (en) * | 2014-12-08 | 2017-01-10 | Общество с ограниченной ответственностью научно-производственная фирма "Уникальный импульс" | Laboratory device for the intensification of technological processes |
-
1959
- 1959-06-01 SU SU629858A patent/SU126571A1/en active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU167702U1 (en) * | 2014-12-08 | 2017-01-10 | Общество с ограниченной ответственностью научно-производственная фирма "Уникальный импульс" | Laboratory device for the intensification of technological processes |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| NO743735L (en) | ||
| US3230155A (en) | Production of pure methanol by thermo-compression distillation | |
| CN105779129A (en) | Method for preparing Artemisia apiacea volatile oil from Artemisia apiacea waste mother liquor, method for preparing byproduct and obtained byproduct | |
| SU126571A1 (en) | A method of extracting rose oil with a solvent and apparatus for carrying out the method | |
| GB776154A (en) | Improvements in and relating to the fractional distillation of mixtures of liquids | |
| US2048178A (en) | Process for dehydrating organic compounds | |
| US1870854A (en) | Process for separating mixtures of substances only partially miscible | |
| US2801265A (en) | Dehydration of volatile fatty acids through solvents | |
| SU62964A1 (en) | Method for extracting essential oils | |
| JPS5551401A (en) | Distilling apparatus | |
| US2623845A (en) | Distillation of wood carbonization | |
| CN208803044U (en) | A kind of device of vacuum distillation recycling aromatic oil | |
| SU87656A1 (en) | The method of extraction of 1-naphthylamine | |
| JPS54103403A (en) | Treatment of waste oil | |
| EA201892022A1 (en) | METHOD FOR DISCHARGING LIQUIDS IN THE ENVIRONMENTAL GAS ENVIRONMENT | |
| GB807609A (en) | Method of cleaning storage and transport tanks, especially ship's tanks, from oil, fat, wax and the like | |
| SU40811A1 (en) | The method of separation from the products of dry distillation of wood concentrated acetic acid and crude wood alcohol | |
| SU407155A1 (en) | METHOD OF OBTAINING COLD IN A BIAGENT EJECTOR INSTALLATION | |
| SU31939A1 (en) | Methyl ethyl ketone dehydration method | |
| GB703476A (en) | Method of separating higher boiling components from steam distillates | |
| ES464467A1 (en) | Process for distillation of miscellas from extraction of oleaginous seeds | |
| GB851935A (en) | Improvements in or relating to processes and plants for treating substances by vapour injection | |
| SU117913A1 (en) | The method of separation of the gas mixture by distillation | |
| SU68307A1 (en) | Method for continuous extraction of substances from their aqueous solutions | |
| US1398791A (en) | Process and apparatus for the manufacture of liquid sulfurous acid from dilute sulfurous-acid gas |