SU124450A1 - The method of separation of glucoalkaloids in the production of solysodin - Google Patents

The method of separation of glucoalkaloids in the production of solysodin

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Publication number
SU124450A1
SU124450A1 SU623022A SU623022A SU124450A1 SU 124450 A1 SU124450 A1 SU 124450A1 SU 623022 A SU623022 A SU 623022A SU 623022 A SU623022 A SU 623022A SU 124450 A1 SU124450 A1 SU 124450A1
Authority
SU
USSR - Soviet Union
Prior art keywords
glucoalkaloids
separation
production
solysodin
mass
Prior art date
Application number
SU623022A
Other languages
Russian (ru)
Inventor
З.В. Зейфман
З.Б. Кристалл
Г.А. Потков
А.И. Сильман
Original Assignee
З.В. Зейфман
З.Б. Кристалл
Г.А. Потков
А.И. Сильман
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by З.В. Зейфман, З.Б. Кристалл, Г.А. Потков, А.И. Сильман filed Critical З.В. Зейфман
Priority to SU623022A priority Critical patent/SU124450A1/en
Application granted granted Critical
Publication of SU124450A1 publication Critical patent/SU124450A1/en

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  • Medicines Containing Plant Substances (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Saccharide Compounds (AREA)

Description

Предлагаетс  отдел ть и высушивать глюкоалкалоиды птичьего паслена Solanum aviculare Forst, из водных экстрактов, содержащих 0,5% сухого остатка, сепарированием экстракта, что приводит к увеличению количества сухого остатка в отсепарированной массе. Сепарирование осуществл ют на сепараторах тонкослойной сепарации с пульсирующей центробежной выгрузкой сгущенной массы глюкоалкалоидов. Выход щую из сепаратора подвижную массу глюкоалкалопдов непрерывно подают на вальцовые сущилки с непрерывным отбором порощкообразных глюкоалкалоидов заданной влажности.It is proposed to separate and dry the glucoalkaloids of the bird nightshade Solanum aviculare Forst from aqueous extracts containing 0.5% of dry residue by separating the extract, which leads to an increase in the amount of dry residue in the separated mass. Separation is carried out on thin-layer separators with a pulsating centrifugal discharge of the thickened mass of glucoalkaloids. The moving mass of glucoalkalodes coming out of the separator is continuously fed to the roller molds with the continuous selection of powdered glucoalkaloids of a given humidity.

В дальнейшем полученный порошок обрабатывают органическими растворител ми дл  извлечени  соласодина.The resulting powder is subsequently treated with organic solvents to extract solasodine.

Предмет изобретени Subject invention

Способ отделени  глюкоалкалоидов в производстве соласодина от экстрактов паслена птичьего Solanum aviculare Forst, содержащих глюкоалкалоиды от 0,5% и выше, путем экстракции растительного материала слабыми растворами кислот с последующим подщелачиванием диффузионных соков и отделением .глюкоалкалоидов путем сепарировани , о тли чающийс  тем, что, в цел х увеличени  отсепарированного остатка глюкоалкалоидов в 10 раз, сепарирование коллоидальной взвеси осуществл ют на сепараторах тонкослойной сепарации непрерывного двйст-ВИЯ с пульсирующей центробежной выгрузкой сгущенной массь глюкбалкалоидов без остановки процесса сепарации с последующей непрерывней сущкой сгущенной массы глюкоалкалоидов на вальцевых сушилках до получени  порошка нужной влажности.The method of separating glucoalkaloids in the production of solasodine from the extracts of the nightshade of the avian Solanum aviculare Forst, containing glucoalkaloids from 0.5% and above, by extracting the plant material with weak acid solutions, followed by alkalinizing the diffusion juices and separating the glucoalkaloids by separation, according to the in order to increase the separated residue of glucoalkaloids by a factor of 10, the separation of the colloidal suspension is carried out on thin-layer separators of continuous dvist-VIV from a pulsating center. ntrobezhnoy discharging the thickened mass glyukbalkaloidov without stopping the separation process followed by continuous suschkoy thickened mass glyukoalkaloidov on Roller kilns to obtain the desired moisture content of the powder.

SU623022A 1959-03-23 1959-03-23 The method of separation of glucoalkaloids in the production of solysodin SU124450A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU623022A SU124450A1 (en) 1959-03-23 1959-03-23 The method of separation of glucoalkaloids in the production of solysodin

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU623022A SU124450A1 (en) 1959-03-23 1959-03-23 The method of separation of glucoalkaloids in the production of solysodin

Publications (1)

Publication Number Publication Date
SU124450A1 true SU124450A1 (en) 1959-11-30

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ID=48395913

Family Applications (1)

Application Number Title Priority Date Filing Date
SU623022A SU124450A1 (en) 1959-03-23 1959-03-23 The method of separation of glucoalkaloids in the production of solysodin

Country Status (1)

Country Link
SU (1) SU124450A1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6984725B2 (en) 2002-06-28 2006-01-10 Solbec Pharmaceuticals Ltd. Method for the separation of triglycoalkaloids

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6984725B2 (en) 2002-06-28 2006-01-10 Solbec Pharmaceuticals Ltd. Method for the separation of triglycoalkaloids

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