SG11201900068PA - Single crystal silicon plate-shaped body and production method therefor - Google Patents

Single crystal silicon plate-shaped body and production method therefor

Info

Publication number
SG11201900068PA
SG11201900068PA SG11201900068PA SG11201900068PA SG11201900068PA SG 11201900068P A SG11201900068P A SG 11201900068PA SG 11201900068P A SG11201900068P A SG 11201900068PA SG 11201900068P A SG11201900068P A SG 11201900068PA SG 11201900068P A SG11201900068P A SG 11201900068PA
Authority
SG
Singapore
Prior art keywords
single crystal
crystal silicon
shaped body
silicon plate
ppma
Prior art date
Application number
SG11201900068PA
Inventor
Isao Masada
Shoji Tachibana
Original Assignee
Tokuyama Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tokuyama Corp filed Critical Tokuyama Corp
Publication of SG11201900068PA publication Critical patent/SG11201900068PA/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B15/00Single-crystal growth by pulling from a melt, e.g. Czochralski method
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/02Silicon
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B15/00Single-crystal growth by pulling from a melt, e.g. Czochralski method
    • C30B15/20Controlling or regulating
    • C30B15/206Controlling or regulating the thermal history of growing the ingot
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/02Elements
    • C30B29/06Silicon
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/60Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape characterised by shape
    • C30B29/64Flat crystals, e.g. plates, strips or discs
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L31/00Semiconductor devices sensitive to infrared radiation, light, electromagnetic radiation of shorter wavelength or corpuscular radiation and specially adapted either for the conversion of the energy of such radiation into electrical energy or for the control of electrical energy by such radiation; Processes or apparatus specially adapted for the manufacture or treatment thereof or of parts thereof; Details thereof
    • H01L31/18Processes or apparatus specially adapted for the manufacture or treatment of these devices or of parts thereof
    • H01L31/1804Processes or apparatus specially adapted for the manufacture or treatment of these devices or of parts thereof comprising only elements of Group IV of the Periodic Table

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Inorganic Chemistry (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)

Abstract

SINGLE CRYSTAL SILICON PLATE-SHAPED BODY AND PRODUCTION METHOD THEREFOR An object of the invention is to develop a single crystal silicon that becomes such a high-performance device as a solar cell or a power device in which decrease in lifetime is suppressed even if heating treatment from 800°C to 1100°C performed in a device production process is applied in a single crystal silicon plate-shaped body having a high oxygen concentration. Provided is a single crystal silicon plate-shaped body as cut out from an upper portion of a straight body portion of a CZ method single crystal silicon ingot in which an interstitial oxygen concentration in a crystal is 25 ppma to 45 ppma and a substitutional carbon concentration is 0.5 ppma or less in a radial center, wherein in the radial center, oxygen precipitates are not observed in a bulk in an image of 200,000 times by means of a transmission electron microscope, and after heating the single crystal silicon plate-shaped body at 950°C for 60 minutes, oxygen precipitates are observed in an image of the 200,000 times, and a shape of the oxygen precipitates is observed in a polyhedral structure in an image of 2,000,000 times. (Fig.1)
SG11201900068PA 2016-07-06 2017-06-30 Single crystal silicon plate-shaped body and production method therefor SG11201900068PA (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2016134375 2016-07-06
PCT/JP2017/024235 WO2018008561A1 (en) 2016-07-06 2017-06-30 Single crystal silicon plate-shaped body and production method therefor

Publications (1)

Publication Number Publication Date
SG11201900068PA true SG11201900068PA (en) 2019-02-27

Family

ID=60912812

Family Applications (1)

Application Number Title Priority Date Filing Date
SG11201900068PA SG11201900068PA (en) 2016-07-06 2017-06-30 Single crystal silicon plate-shaped body and production method therefor

Country Status (8)

Country Link
US (1) US10975496B2 (en)
JP (1) JP6484762B2 (en)
KR (1) KR102032535B1 (en)
CN (1) CN109477240B (en)
DE (1) DE112017003436T5 (en)
SG (1) SG11201900068PA (en)
TW (1) TWI732898B (en)
WO (1) WO2018008561A1 (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6645545B1 (en) * 2018-09-03 2020-02-14 株式会社Sumco Method for evaluating carbon concentration of silicon sample, method for evaluating silicon wafer manufacturing process, method for manufacturing silicon wafer, and method for manufacturing silicon single crystal ingot
JP6979007B2 (en) 2018-12-17 2021-12-08 グローバルウェーハズ・ジャパン株式会社 Ultra-low oxygen concentration measurement method for silicon wafers
CN114667370A (en) 2019-08-09 2022-06-24 尖端设备技术公司 Producing tapes or wafers having regions of low oxygen concentration
CN115148858B (en) * 2022-08-01 2024-06-11 安徽华晟新能源科技有限公司 Passivation method of silicon solar cell

Family Cites Families (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH03133121A (en) * 1989-10-19 1991-06-06 Showa Denko Kk Silicon substrate for semiconductor device and manufacture thereof
JPH0789789A (en) * 1993-09-20 1995-04-04 Fujitsu Ltd Si crystal, method for growing crystal and device therefor
US5593494A (en) * 1995-03-14 1997-01-14 Memc Electronic Materials, Inc. Precision controlled precipitation of oxygen in silicon
JP3006669B2 (en) 1995-06-20 2000-02-07 信越半導体株式会社 Method and apparatus for producing silicon single crystal having uniform crystal defects
JPH09190954A (en) 1996-01-10 1997-07-22 Sumitomo Sitix Corp Semiconductor substrate and its manufacture
EP0948037B1 (en) * 1996-07-29 2006-11-02 Sumco Corporation Method for manufacturing a silicon epitaxial wafer
US6503594B2 (en) 1997-02-13 2003-01-07 Samsung Electronics Co., Ltd. Silicon wafers having controlled distribution of defects and slip
JPH1143393A (en) * 1997-07-23 1999-02-16 Nippon Steel Corp Silicon single crystal wafer and its production
JP4112654B2 (en) 1997-09-19 2008-07-02 シルトロニック・ジャパン株式会社 Method for manufacturing silicon wafer
EP1090166B1 (en) * 1998-06-26 2002-03-27 MEMC Electronic Materials, Inc. Process for growth of defect free silicon crystals of arbitrarily large diameters
TW505710B (en) * 1998-11-20 2002-10-11 Komatsu Denshi Kinzoku Kk Production method for silicon single crystal and production device for single crystal ingot, and heat treating method for silicon single crystal wafer
DE60041309D1 (en) * 1999-03-16 2009-02-26 Shinetsu Handotai Kk METHOD OF MANUFACTURING SILICON WAFER AND SILICON WAFER
JP2002043318A (en) * 2000-07-28 2002-02-08 Shin Etsu Handotai Co Ltd Method for manufacturing silicon single crystal wafer
JP2002184779A (en) * 2000-12-13 2002-06-28 Shin Etsu Handotai Co Ltd Annealed wafer and method of manufacturing the same
WO2002059400A2 (en) * 2001-01-26 2002-08-01 Memc Electronic Materials, Inc. Low defect density silicon substantially free of oxidation induced stacking faults having a vacancy-dominated core
US7201800B2 (en) * 2001-12-21 2007-04-10 Memc Electronic Materials, Inc. Process for making silicon wafers with stabilized oxygen precipitate nucleation centers
KR100745308B1 (en) 2001-12-21 2007-08-01 엠이엠씨 일렉트로닉 머티리얼즈 인코포레이티드 Ideal oxygen precipitating silicon wafers with nitrogen/carbon stabilized oxygen precipitate nucleation centers and process for making the same
KR100745309B1 (en) * 2002-04-10 2007-08-01 엠이엠씨 일렉트로닉 머티리얼즈 인코포레이티드 Process for controlling denuded zone depth in an ideal oxygen precipitating silicon wafer
KR100573473B1 (en) 2004-05-10 2006-04-24 주식회사 실트론 Silicon wafer and method of fabricating the same
WO2006003812A1 (en) * 2004-06-30 2006-01-12 Sumitomo Mitsubishi Silicon Corporation Process for producing silicon wafer and silicon wafer produced by the process
CN1269186C (en) * 2004-11-22 2006-08-09 浙江大学 Carbon doped silicon sheet with internal impurity absorbing function and production thereof
EP1909315A4 (en) * 2005-07-27 2008-11-26 Sumco Corp Silicon wafer and process for producing the same
JP2007194232A (en) * 2006-01-17 2007-08-02 Shin Etsu Handotai Co Ltd Process for producing silicon single crystal wafer
JP5151777B2 (en) * 2008-07-30 2013-02-27 株式会社Sumco Method for manufacturing silicon epitaxial wafer and silicon epitaxial wafer
KR20100036155A (en) * 2008-09-29 2010-04-07 매그나칩 반도체 유한회사 Silicon wafer and fabrication method thereof
JP5088338B2 (en) * 2009-03-10 2012-12-05 信越半導体株式会社 Method of pulling silicon single crystal
JP2011228459A (en) 2010-04-19 2011-11-10 Sumco Corp Silicon wafer and method of manufacturing the same
JP5984448B2 (en) * 2012-03-26 2016-09-06 グローバルウェーハズ・ジャパン株式会社 Silicon wafer
JP5885305B2 (en) * 2013-08-07 2016-03-15 グローバルウェーハズ・ジャパン株式会社 Silicon wafer and manufacturing method thereof
CN104726931A (en) * 2015-03-30 2015-06-24 江苏盎华光伏工程技术研究中心有限公司 Single crystal furnace with annealing device and control method for single crystal furnace

Also Published As

Publication number Publication date
DE112017003436T5 (en) 2019-03-21
TWI732898B (en) 2021-07-11
JPWO2018008561A1 (en) 2018-11-29
TW201816201A (en) 2018-05-01
JP6484762B2 (en) 2019-03-13
CN109477240A (en) 2019-03-15
KR102032535B1 (en) 2019-10-15
US10975496B2 (en) 2021-04-13
CN109477240B (en) 2019-12-27
US20190161888A1 (en) 2019-05-30
WO2018008561A1 (en) 2018-01-11
KR20190007502A (en) 2019-01-22

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