SG11201406509YA - Purification of bio-based acrylic acid to crude and glacial acrylic acid - Google Patents

Purification of bio-based acrylic acid to crude and glacial acrylic acid

Info

Publication number
SG11201406509YA
SG11201406509YA SG11201406509YA SG11201406509YA SG11201406509YA SG 11201406509Y A SG11201406509Y A SG 11201406509YA SG 11201406509Y A SG11201406509Y A SG 11201406509YA SG 11201406509Y A SG11201406509Y A SG 11201406509YA SG 11201406509Y A SG11201406509Y A SG 11201406509YA
Authority
SG
Singapore
Prior art keywords
acrylic acid
bio
crude
purification
glacial
Prior art date
Application number
SG11201406509YA
Other languages
English (en)
Inventor
Jane Ellen Godlewski
Janette Villalobos Lingoes
Juan Esteban Velasquez
Dimitris Ioannis Collias
Original Assignee
Procter & Gamble
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US13/760,505 external-priority patent/US20130274518A1/en
Application filed by Procter & Gamble filed Critical Procter & Gamble
Publication of SG11201406509YA publication Critical patent/SG11201406509YA/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/48Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14Phosphorus; Compounds thereof
    • B01J27/16Phosphorus; Compounds thereof containing oxygen, i.e. acids, anhydrides and their derivates with N, S, B or halogens without carriers or on carriers based on C, Si, Al or Zr; also salts of Si, Al and Zr
    • B01J27/18Phosphorus; Compounds thereof containing oxygen, i.e. acids, anhydrides and their derivates with N, S, B or halogens without carriers or on carriers based on C, Si, Al or Zr; also salts of Si, Al and Zr with metals other than Al or Zr
    • B01J27/1802Salts or mixtures of anhydrides with compounds of other metals than V, Nb, Ta, Cr, Mo, W, Mn, Tc, Re, e.g. phosphates, thiophosphates
    • B01J27/1806Salts or mixtures of anhydrides with compounds of other metals than V, Nb, Ta, Cr, Mo, W, Mn, Tc, Re, e.g. phosphates, thiophosphates with alkaline or alkaline earth metals
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/347Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups
    • C07C51/377Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups by splitting-off hydrogen or functional groups; by hydrogenolysis of functional groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C07C51/46Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation by azeotropic distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/47Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/02Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C57/03Monocarboxylic acids
    • C07C57/04Acrylic acid; Methacrylic acid

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
SG11201406509YA 2012-04-11 2013-04-11 Purification of bio-based acrylic acid to crude and glacial acrylic acid SG11201406509YA (en)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US201261623054P 2012-04-11 2012-04-11
US13/760,505 US20130274518A1 (en) 2012-04-11 2013-02-06 Purification Of Bio Based Acrylic Acid To Crude And Glacial Acrylic Acid
US13/838,823 US20130274520A1 (en) 2012-04-11 2013-03-15 Purification Of Bio Based Acrylic Acid To Crude And Glacial Acrylic Acid
US13/835,187 US9926256B2 (en) 2012-04-11 2013-03-15 Catalytic conversion of lactic acid to acrylic acid
PCT/US2013/036158 WO2013155292A2 (en) 2012-04-11 2013-04-11 Purification of bio-based acrylic acid to crude and glacial acrylic acid

Publications (1)

Publication Number Publication Date
SG11201406509YA true SG11201406509YA (en) 2014-11-27

Family

ID=49325676

Family Applications (2)

Application Number Title Priority Date Filing Date
SG11201406509YA SG11201406509YA (en) 2012-04-11 2013-04-11 Purification of bio-based acrylic acid to crude and glacial acrylic acid
SG10201703949YA SG10201703949YA (en) 2012-04-11 2013-04-11 Purification of bio-based acrylic acid to crude and glacial acrylic acid

Family Applications After (1)

Application Number Title Priority Date Filing Date
SG10201703949YA SG10201703949YA (en) 2012-04-11 2013-04-11 Purification of bio-based acrylic acid to crude and glacial acrylic acid

Country Status (12)

Country Link
US (2) US20130274520A1 (enExample)
EP (1) EP2836475B1 (enExample)
JP (2) JP2015517999A (enExample)
AU (1) AU2013245853B2 (enExample)
BR (1) BR112014025188B1 (enExample)
CA (1) CA2870314C (enExample)
IN (1) IN2014DN08551A (enExample)
MX (1) MX380544B (enExample)
MY (1) MY164790A (enExample)
RU (1) RU2599640C2 (enExample)
SG (2) SG11201406509YA (enExample)
WO (1) WO2013155292A2 (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA3002289C (en) 2013-10-16 2021-11-30 The Procter & Gamble Company Method for producing bio-based acrylic acid and its derivatives from lactic acid and derivatives therefore using mixed phosphate catalyst and the process thereof
WO2016026761A1 (en) * 2014-08-18 2016-02-25 Basf Se Process for preparing acrylic acid by dehydration of 3-hydroxypropionic acid
EP3012244A1 (en) 2014-10-24 2016-04-27 Sulzer Chemtech AG Process and apparatus for purification of acrylic acid
EP3341124B1 (en) * 2015-08-28 2025-11-05 The Procter & Gamble Company Catalytic dehydration of hydroxypropionic acid and its derivatives
CA3050698C (en) 2015-08-28 2021-09-14 Juan Esteban Velasquez Catalysts for the dehydration of hydroxypropionic acid and its derivatives
DE102016114555A1 (de) 2016-08-05 2018-02-08 Thyssenkrupp Ag Prozess zur Herstellung von Acrylsäure aus einer wässrigen 3-Hydroxypropanol-Lösung
US9890102B1 (en) 2016-11-03 2018-02-13 The Procter & Gamble Company Method of making acrylic acid from hydroxypropionic acid
JP7618792B2 (ja) * 2020-10-16 2025-01-21 エルジー・ケム・リミテッド 乳酸気化方法、乳酸気化装置、およびアクリル酸の製造方法
KR102721330B1 (ko) * 2020-12-03 2024-10-23 주식회사 엘지화학 아크릴산 제조방법
FR3125064B1 (fr) 2021-07-09 2024-07-12 Snf Sa Procédé biologique d’obtention de monomères comprenant une insaturation éthylénique par bioconversion d’un composé biosourcé comprenant au moins une fonction nitrile

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US4427884A (en) 1982-01-25 1984-01-24 The Research Foundation Of State University Of New York Method for detecting and quantifying carbon isotopes
US4973841A (en) 1990-02-02 1990-11-27 Genus, Inc. Precision ultra-sensitive trace detector for carbon-14 when it is at concentration close to that present in recent organic materials
US5438194A (en) 1993-07-30 1995-08-01 High Voltage Engineering Europa B.V. Ultra-sensitive molecular identifier
FR2736912B1 (fr) 1995-07-18 1997-08-22 Atochem Elf Sa Procede de purification de l'acide acrylique obtenu par oxydation catalytique du propylene
DE19600955A1 (de) * 1996-01-12 1997-07-17 Basf Ag Verfahren zur Herstellung von Acrylsäure und deren Ester
US5661299A (en) 1996-06-25 1997-08-26 High Voltage Engineering Europa B.V. Miniature AMS detector for ultrasensitive detection of individual carbon-14 and tritium atoms
DE19829477A1 (de) 1998-07-01 2000-01-05 Basf Ag Verfahren zur Reinigung von Acrylsäure oder Methacrylsäure durch Kristallisation und Destillation
DE19832962A1 (de) * 1998-07-22 2000-01-27 Basf Ag Reinigung von Acrylsäure durch Kristallisation mittels Vakuumverdampfung
EP1272453B1 (de) * 2000-04-11 2005-11-09 Basf Aktiengesellschaft Verfahren zur reinigung einer rohacrylsäureschmelze
JP4074194B2 (ja) * 2001-01-12 2008-04-09 ストックハウゼン ゲーエムベーハー (メタ)アクリル酸の精製方法及びその製造装置
DE10138150A1 (de) 2001-08-03 2003-02-13 Basf Ag Verfahren zur Herstellung wasserabsorbierender Harze
US20030146081A1 (en) * 2002-01-08 2003-08-07 Salvador Aldrett Acrylic acid recovery utilizing ethyl acrylate and selected co-solvents
EP1732874A1 (en) * 2004-04-02 2006-12-20 Ciba Speciality Chemicals Water Treatments Limited Preparation of acrylic acid derivatives from alpha or beta-hydroxy carboxylic acids
FR2897058B1 (fr) * 2006-02-07 2008-04-18 Arkema Sa Procede de preparation d'acroleine
DE102006039203B4 (de) * 2006-08-22 2014-06-18 Evonik Degussa Gmbh Verfahren zur Herstellung von durch Kristallisation gereinigter Acrylsäure aus Hydroxypropionsäure sowie Vorrichtung dazu
JP5489726B2 (ja) * 2007-01-26 2014-05-14 ビーエーエスエフ ソシエタス・ヨーロピア アクリル酸の製造方法
WO2008090190A1 (de) * 2007-01-26 2008-07-31 Basf Se Verfahren zur herstellung von acrylsäure
JP4822559B2 (ja) * 2007-09-19 2011-11-24 ローム アンド ハース カンパニー (メタ)アクリル酸生成物流からのプロピオン酸の選択的減少のための改良された方法
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CN102414159B (zh) * 2009-05-15 2014-02-26 株式会社日本触媒 制备(甲基)丙烯酸的方法
FR2948365B1 (fr) * 2009-07-22 2011-09-09 Arkema France Procede de fabrication d'acide acrylique bio-ressource a partir de glycerol
WO2011052178A1 (ja) * 2009-10-29 2011-05-05 株式会社サンギ 不飽和カルボン酸および/またはその誘導体の合成方法
JP2011225533A (ja) * 2010-03-31 2011-11-10 Nippon Shokubai Co Ltd アクリル酸およびその重合体の製造方法
WO2012033845A2 (en) * 2010-09-07 2012-03-15 Myriant Corporation Catalytic dehydration of lactic acid and lactic acid esters
JP5654615B2 (ja) * 2010-12-28 2015-01-14 株式会社日本触媒 アクリル酸および/またはそのエステルおよびその重合体の製法
US9714208B2 (en) * 2012-04-11 2017-07-25 The Procter & Gamble Company Catalysts conversion of hydroxypropionic acid or its derivatives to acrylic acid or its derivatives

Also Published As

Publication number Publication date
MY164790A (en) 2018-01-30
SG10201703949YA (en) 2017-06-29
AU2013245853B2 (en) 2016-06-02
BR112014025188B1 (pt) 2020-02-04
WO2013155292A4 (en) 2014-01-23
MX380544B (es) 2025-03-12
EP2836475A2 (en) 2015-02-18
WO2013155292A2 (en) 2013-10-17
CN104220410A (zh) 2014-12-17
CA2870314A1 (en) 2013-10-17
EP2836475B1 (en) 2021-05-26
CA2870314C (en) 2018-01-02
RU2014139950A (ru) 2016-04-20
RU2599640C2 (ru) 2016-10-10
US20150329462A1 (en) 2015-11-19
AU2013245853A1 (en) 2014-10-30
US20130274520A1 (en) 2013-10-17
MX2014012303A (es) 2014-11-10
JP2017101046A (ja) 2017-06-08
JP2015517999A (ja) 2015-06-25
WO2013155292A3 (en) 2013-12-05
IN2014DN08551A (enExample) 2015-05-15

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