RU2508301C1 - Получение лигнина из лигноцеллюлозной биомассы - Google Patents

Получение лигнина из лигноцеллюлозной биомассы Download PDF

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Publication number
RU2508301C1
RU2508301C1 RU2012154207/05A RU2012154207A RU2508301C1 RU 2508301 C1 RU2508301 C1 RU 2508301C1 RU 2012154207/05 A RU2012154207/05 A RU 2012154207/05A RU 2012154207 A RU2012154207 A RU 2012154207A RU 2508301 C1 RU2508301 C1 RU 2508301C1
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Russia
Prior art keywords
pressure
lignin
temperature
specified
soluble
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RU2012154207/05A
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English (en)
Russian (ru)
Inventor
Кришнан В. ИЙЕР
Мишель А. СИМАРД
Киран КАДАМ
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Ренмэтикс, Инк.
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    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
    • C04B24/16—Sulfur-containing compounds
    • C04B24/18—Lignin sulfonic acid or derivatives thereof, e.g. sulfite lye
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07G—COMPOUNDS OF UNKNOWN CONSTITUTION
    • C07G1/00—Low-molecular-weight derivatives of lignin
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
    • C08H6/00—Macromolecular compounds derived from lignin, e.g. tannins, humic acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
    • C08H8/00—Macromolecular compounds derived from lignocellulosic materials
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L97/00—Compositions of lignin-containing materials
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C11/00—Regeneration of pulp liquors or effluent waste waters
    • D21C11/0007—Recovery of by-products, i.e. compounds other than those necessary for pulping, for multiple uses or not otherwise provided for
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1011—Biomass
    • C10G2300/1014—Biomass of vegetal origin
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/10—Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Ceramic Engineering (AREA)
  • Structural Engineering (AREA)
  • Processing Of Solid Wastes (AREA)
  • Paper (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Compounds Of Unknown Constitution (AREA)
  • Dry Formation Of Fiberboard And The Like (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
RU2012154207/05A 2011-05-04 2012-05-04 Получение лигнина из лигноцеллюлозной биомассы RU2508301C1 (ru)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201161482425P 2011-05-04 2011-05-04
US61/482,425 2011-05-04
PCT/US2012/036566 WO2012151509A2 (en) 2011-05-04 2012-05-04 Lignin production from lignocellulosic biomass

Publications (1)

Publication Number Publication Date
RU2508301C1 true RU2508301C1 (ru) 2014-02-27

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RU2012154207/05A RU2508301C1 (ru) 2011-05-04 2012-05-04 Получение лигнина из лигноцеллюлозной биомассы

Country Status (13)

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US (2) US8317928B1 (https=)
EP (1) EP2705074B1 (https=)
JP (1) JP5905570B2 (https=)
KR (1) KR101425765B1 (https=)
CN (1) CN103502320B (https=)
AU (1) AU2012250560B2 (https=)
BR (1) BR112013028146A2 (https=)
CA (1) CA2834856C (https=)
PH (1) PH12013502197A1 (https=)
RU (1) RU2508301C1 (https=)
SG (1) SG194704A1 (https=)
WO (1) WO2012151509A2 (https=)
ZA (1) ZA201309031B (https=)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10253057B2 (en) 2014-11-12 2019-04-09 Renmatix, Inc. Method of coalescing a substance
RU2710376C2 (ru) * 2015-05-29 2019-12-26 ЮПМ-Кюммене Корпорейшн Способ и устройство для промывки сырого лигнина, содержащая растворимые углеводы фракция, твердая фракция и их применение
RU2717097C2 (ru) * 2015-05-29 2020-03-18 ЮПМ-Кюммене Корпорейшн Способ и устройство для образования фракции лигнина, лигниновая композиция и ее применение

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9359651B2 (en) 2010-01-19 2016-06-07 Renmatix, Inc. Production of fermentable sugars and lignin from biomass using supercritical fluids
KR20130119935A (ko) 2010-11-01 2013-11-01 리엑 퓰 에이비 고온압축수 처리에 의한 바이오매스 피드스탁의 조절 전환을 위한 공정
US8663800B2 (en) 2011-05-04 2014-03-04 Renmatix, Inc. Lignin production from lignocellulosic biomass
US8801859B2 (en) 2011-05-04 2014-08-12 Renmatix, Inc. Self-cleaning apparatus and method for thick slurry pressure control
CN103917666A (zh) * 2011-11-08 2014-07-09 雷克燃料公司 生物质在低pH下的液化
US8759498B2 (en) 2011-12-30 2014-06-24 Renmatix, Inc. Compositions comprising lignin
FI20125362L (fi) * 2012-03-29 2013-09-30 Upm Kymmene Corp Ligniini sekä menetelmä ja järjestelmä ligniinin käsittelemiseksi
BR112014025714A8 (pt) * 2012-04-30 2018-02-06 Renmatix Inc Processo que envolve a liquefação de uma calda de biomassa por meio de tratamento em água comprimida quente (hcw)
US9222040B2 (en) * 2012-06-07 2015-12-29 General Electric Company System and method for slurry handling
US10018416B2 (en) 2012-12-04 2018-07-10 General Electric Company System and method for removal of liquid from a solids flow
SE538224C2 (sv) * 2013-01-25 2016-04-05 Ren Fuel K2B Ab Kompositioner av biomassamaterial för raffinering
EP2970595B1 (en) 2013-03-15 2018-07-11 Renmatix Inc. High purity lignin, lignin compositions, and higher structured lignin
US9255187B2 (en) * 2013-03-15 2016-02-09 Synergy Horizon Limited Method for production of dry hydrolytic lignin
KR101479676B1 (ko) 2013-05-23 2015-01-08 씨제이제일제당 주식회사 저분자 리그닌 유도체의 제조방법
US9784121B2 (en) 2013-12-11 2017-10-10 General Electric Company System and method for continuous solids slurry depressurization
US9702372B2 (en) 2013-12-11 2017-07-11 General Electric Company System and method for continuous solids slurry depressurization
KR20170066408A (ko) 2014-09-26 2017-06-14 렌매틱스, 인코포레이티드. Ii형 셀룰로스를 포함하는 접착제 조성물
EP3186296A4 (en) 2014-09-26 2018-05-23 Renmatix, Inc. Methods for preparing and collecting polyaromatic compounds, and products comprising polyaromatic compounds
GB2546243B (en) * 2015-12-23 2018-07-11 Aerothermal Green Energy Ltd Biomass, thermal pressure hydrolysis and anaerobic digestion
BR112019017106A2 (pt) 2017-02-16 2020-04-28 Sweetwater Energy, Inc. formação de zona de alta pressão para pré-tratamento
CA3073072A1 (en) * 2017-09-07 2019-03-14 Renmatix, Inc. Antioxidant stabilizer in polymers
AU2020412611A1 (en) 2019-12-22 2022-07-14 Apalta Patents OÜ Methods of making specialized lignin and lignin products from biomass

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1086046A1 (ru) * 1982-07-12 1984-04-15 Ленинградская Ордена Ленина Лесотехническая Академия Им.С.М.Кирова Способ делигнификации древесины
JP2006255676A (ja) * 2005-03-18 2006-09-28 Kri Inc リグニン物質分離方法
WO2007009463A2 (en) * 2005-07-19 2007-01-25 Holm Christensen Biosystemer Aps Method and apparatus for conversion of cellulosic material to ethanol
RU2338769C1 (ru) * 2007-05-22 2008-11-20 Институт физической химии и электрохимии им. А.Н. Фрумкина Российской академии наук Способ переработки растительного сырья
EA012161B1 (ru) * 2004-09-24 2009-08-28 Камби Биоэтанол Апс Способ обработки биомассы и органических отходов с целью образования желаемых биологических продуктов
US20100043782A1 (en) * 2008-07-16 2010-02-25 Srinivas Kilambi Solvo-thermal fractionation of biomass

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2156159A (en) 1938-05-17 1939-04-25 Northwood Chemical Company Process of making lignin
US2994633A (en) 1958-08-21 1961-08-01 Crossett Company Process for separating lignin solids from used neutral sulfite pulping liquors
US2997466A (en) 1958-11-04 1961-08-22 West Virginia Pulp & Paper Co Decantation of lignin
DE2737118A1 (de) 1977-08-17 1979-03-01 Projektierung Chem Verfahrenst Verfahren zur gewinnung von zuckern, gegebenenfalls cellulose und gegebenenfalls lignin aus lignocellulosischen pflanzlichen rohstoffen
CA1100266A (en) 1977-08-31 1981-05-05 Laszlo Paszner Organosolv delignification and saccharification process for lignocellulosic plant materials
US4470851A (en) 1981-03-26 1984-09-11 Laszlo Paszner High efficiency organosolv saccharification process
DE3428661A1 (de) 1983-08-09 1985-03-07 Krupp Industrietechnik GmbH Werk Buckau Wolf, 4048 Grevenbroich Verfahren zur hydrolyse von lignocellulosehaltiger biomasse
CA1198703A (en) 1984-08-02 1985-12-31 Edward A. De Long Method of producing level off d p microcrystalline cellulose and glucose from lignocellulosic material
US4764596A (en) 1985-11-05 1988-08-16 Repap Technologies Inc. Recovery of lignin
CA1284637C (en) 1987-08-24 1991-06-04 George S. Faass Biomass fractionation process
US5041192A (en) * 1988-09-16 1991-08-20 University Of South Florida Supercritical delignification of wood
US6180845B1 (en) * 1999-10-07 2001-01-30 Board Of Supervisors Of Louisiana State University And Agricultural And Mechanical College Transforming biomass to hydrocarbon mixtures in near-critical or supercritical water
JP2006288676A (ja) * 2005-04-11 2006-10-26 Takahiko Katayama 飲料入り容器の陳列方法
WO2007120210A2 (en) 2005-11-23 2007-10-25 Natureworks Llc Process for fractionating lignocellulosic biomass into liquid and solid products
ATE497058T1 (de) * 2006-03-29 2011-02-15 Virginia Tech Intell Prop Celluloselösungsmittelbasierte fraktionierung von lignocellulose unter mässigen reaktionsbedingungen und eduktrückführung
CN101522760A (zh) * 2006-08-07 2009-09-02 艾米塞莱克斯能源公司 从生物质中回收全纤维素和近天然木质素的方法
US8613781B2 (en) 2007-08-08 2013-12-24 Harrison R. Cooper Lignin dewatering process
CA2730766C (en) * 2008-07-16 2016-11-01 Sriya Innovations, Inc. Method of extraction of furfural and glucose from biomass using one or more supercritical fluids
JP5339341B2 (ja) * 2008-08-13 2013-11-13 宜章 大木 亜臨界状態による木材の繊維を線維固形分としての分離方法
JP5410060B2 (ja) * 2008-10-02 2014-02-05 株式会社Ｋｒｉ イオン液体によるリグノセルロース系バイオマスのセルロースとリグニンの分離化方法
KR101657100B1 (ko) * 2008-10-29 2016-09-19 삼성전자주식회사 리그노셀룰로오스계 바이오매스의 분별방법 및 분별장치
SI2421911T1 (sl) 2009-04-23 2014-10-30 Greenfield Ethanol Inc. Ločevanje reaktivne celuloze od lignocelulozne biomase z visoko vsebnostjo lignina
CN102575422B (zh) * 2009-07-13 2016-08-03 贝塔可再生资源公司 木质素的高温分离方法
CN101974161B (zh) * 2010-09-30 2012-10-31 中国科学院西双版纳热带植物园 一种溶解和快速水解木质纤维素生物质的方法及其设备和应用

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1086046A1 (ru) * 1982-07-12 1984-04-15 Ленинградская Ордена Ленина Лесотехническая Академия Им.С.М.Кирова Способ делигнификации древесины
EA012161B1 (ru) * 2004-09-24 2009-08-28 Камби Биоэтанол Апс Способ обработки биомассы и органических отходов с целью образования желаемых биологических продуктов
JP2006255676A (ja) * 2005-03-18 2006-09-28 Kri Inc リグニン物質分離方法
WO2007009463A2 (en) * 2005-07-19 2007-01-25 Holm Christensen Biosystemer Aps Method and apparatus for conversion of cellulosic material to ethanol
WO2007009463A3 (en) * 2005-07-19 2007-07-05 Holm Christensen Biosystemer A Method and apparatus for conversion of cellulosic material to ethanol
RU2338769C1 (ru) * 2007-05-22 2008-11-20 Институт физической химии и электрохимии им. А.Н. Фрумкина Российской академии наук Способ переработки растительного сырья
US20100043782A1 (en) * 2008-07-16 2010-02-25 Srinivas Kilambi Solvo-thermal fractionation of biomass

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10253057B2 (en) 2014-11-12 2019-04-09 Renmatix, Inc. Method of coalescing a substance
RU2686832C2 (ru) * 2014-11-12 2019-04-30 Ренмэтикс, Инк. Способ коалесценции вещества
US10633405B2 (en) 2014-11-12 2020-04-28 Renmatix, Inc. Method of coalescing a substance
RU2710376C2 (ru) * 2015-05-29 2019-12-26 ЮПМ-Кюммене Корпорейшн Способ и устройство для промывки сырого лигнина, содержащая растворимые углеводы фракция, твердая фракция и их применение
RU2717097C2 (ru) * 2015-05-29 2020-03-18 ЮПМ-Кюммене Корпорейшн Способ и устройство для образования фракции лигнина, лигниновая композиция и ее применение
US11078225B2 (en) 2015-05-29 2021-08-03 Upm-Kymmene Corporation Method and an apparatus for forming a lignin fraction, a lignin composition and its use
US11267837B2 (en) 2015-05-29 2022-03-08 Upm-Kymmene Corporation Method and an apparatus for washing a crude lignin, a soluble carbohydrate containing fraction, a solid fraction and their use
US12428440B2 (en) 2015-05-29 2025-09-30 Upm-Kymmene Corporation Method and an apparatus for forming a lignin fraction, a lignin composition and its use

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Publication number Publication date
US8317928B1 (en) 2012-11-27
US20120282467A1 (en) 2012-11-08
US20120282466A1 (en) 2012-11-08
AU2012250560B2 (en) 2015-11-19
JP2014513740A (ja) 2014-06-05
SG194704A1 (en) 2013-12-30
WO2012151509A3 (en) 2013-03-21
WO2012151509A2 (en) 2012-11-08
NZ616924A (en) 2015-10-30
CN103502320B (zh) 2016-03-30
AU2012250560A1 (en) 2013-11-07
KR20140027376A (ko) 2014-03-06
BR112013028146A2 (pt) 2017-04-25
KR101425765B1 (ko) 2014-08-01
JP5905570B2 (ja) 2016-04-20
EP2705074B1 (en) 2017-11-01
PH12013502197A1 (en) 2014-01-13
CA2834856C (en) 2020-04-07
CA2834856A1 (en) 2012-11-08
EP2705074A2 (en) 2014-03-12
ZA201309031B (en) 2015-03-25
EP2705074A4 (en) 2014-12-03
CN103502320A (zh) 2014-01-08
US8404051B2 (en) 2013-03-26

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