RU2474569C2 - Способ отделения 1,3,3,3-тетрафторпропена от фтороводорода азеотропной дистилляцией - Google Patents

Способ отделения 1,3,3,3-тетрафторпропена от фтороводорода азеотропной дистилляцией Download PDF

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Publication number
RU2474569C2
RU2474569C2 RU2010138730/04A RU2010138730A RU2474569C2 RU 2474569 C2 RU2474569 C2 RU 2474569C2 RU 2010138730/04 A RU2010138730/04 A RU 2010138730/04A RU 2010138730 A RU2010138730 A RU 2010138730A RU 2474569 C2 RU2474569 C2 RU 2474569C2
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hfc
composition
stream
azeotropically
rich
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RU2010138730/04A
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RU2010138730A (ru
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Джеффри П. КНЭПП
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Е.И.Дюпон Де Немур Энд Компани
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C07C17/386—Separation; Purification; Stabilisation; Use of additives by distillation with auxiliary compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/19—Fluorine; Hydrogen fluoride
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00—Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Separation By Low-Temperature Treatments (AREA)
RU2010138730/04A 2008-02-21 2009-02-19 Способ отделения 1,3,3,3-тетрафторпропена от фтороводорода азеотропной дистилляцией RU2474569C2 (ru)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US3037108P 2008-02-21 2008-02-21
US61/030,371 2008-02-21
PCT/US2009/034492 WO2009105521A1 (en) 2008-02-21 2009-02-19 Processes for separation of 1,3,3,3-tetrafluoropropene from hydrogen fluoride by azeotropic distillation

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RU2010138730A RU2010138730A (ru) 2012-03-27
RU2474569C2 true RU2474569C2 (ru) 2013-02-10

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RU2010138730/04A RU2474569C2 (ru) 2008-02-21 2009-02-19 Способ отделения 1,3,3,3-тетрафторпропена от фтороводорода азеотропной дистилляцией

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US (1) US8658846B2 (https=)
EP (1) EP2247560B1 (https=)
JP (2) JP2011513228A (https=)
KR (5) KR102136117B1 (https=)
CN (1) CN101952229B (https=)
BR (1) BRPI0906015A2 (https=)
CA (1) CA2712616A1 (https=)
ES (1) ES2483995T3 (https=)
MX (1) MX2010009081A (https=)
RU (1) RU2474569C2 (https=)
WO (1) WO2009105521A1 (https=)

Families Citing this family (31)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102136117B1 (ko) 2008-02-21 2020-07-22 더 케무어스 컴퍼니 에프씨, 엘엘씨 공비 증류에 의한 플루오르화수소로부터의 1,3,3,3-테트라플루오로프로펜의 분리 방법
CN104164214B (zh) * 2008-05-07 2018-04-24 科慕埃弗西有限公司 可用作热传递组合物的组合物
CN105062427A (zh) 2009-12-22 2015-11-18 纳幕尔杜邦公司 包含2,3,3,3-四氟丙烯、1,1,2,3-四氯丙烯、2-氯-3,3,3-三氟丙烯、或2-氯-1,1,1,2-四氟丙烷的组合物
US8747691B2 (en) * 2010-05-06 2014-06-10 Honeywell International Inc. Azeotrope-like compositions of tetrafluoropropene and water
US8518293B2 (en) * 2010-09-03 2013-08-27 Honeywell International Inc. 1,3,3,3-tetrafluoropropene process azeotropes with HF
JP5817373B2 (ja) * 2010-11-10 2015-11-18 セントラル硝子株式会社 トランス−１，３，３，３−テトラフルオロプロペンの製造方法
CN104024189B (zh) * 2011-12-28 2016-01-13 旭硝子株式会社 2,3,3,3-四氟丙烯的纯化方法，纯化装置及制造方法
JP6011008B2 (ja) * 2012-04-27 2016-10-19 旭硝子株式会社 共沸または共沸様組成物、および２，３，３，３−テトラフルオロプロペンまたはヘキサフルオロプロペンの製造方法
FR3000093B1 (fr) * 2012-12-26 2015-07-17 Arkema France Composition azeotropique ou quasi-azeotropique de chloromethane
FR3003569B1 (fr) * 2013-03-20 2015-12-25 Arkema France Composition comprenant hf et 1,3,3,3-tetrafluoropropene
FR3003565B1 (fr) 2013-03-20 2018-06-29 Arkema France Composition comprenant hf et 2,3,3,3-tetrafluoropropene
FR3003567B1 (fr) * 2013-03-20 2015-03-06 Arkema France Composition comprenant hf et 3,3,3-trifluoropropene
CN103288589A (zh) * 2013-06-04 2013-09-11 同济大学 一种生产三氟乙烯联产氟化氢的方法
CN103673503A (zh) * 2013-12-27 2014-03-26 上海磊诺工业气体有限公司 一种七氟丙烷的回收系统
JP6102984B2 (ja) * 2015-05-29 2017-03-29 ダイキン工業株式会社 含フッ素化合物の製造方法
WO2017104829A1 (ja) * 2015-12-16 2017-06-22 旭硝子株式会社 ハイドロフルオロオレフィンの製造方法
FR3046165B1 (fr) * 2015-12-23 2019-12-13 Arkema France Procede de production et de purification du 2,3,3,3-tetrafluoro-1-propene
FR3046159B1 (fr) * 2015-12-23 2019-12-13 Arkema France Procede de preparation du 2,3,3,3-tetrafluoropropene et recyclage du 1,1,1,2,2-pentafluoropropane exempt d'impuretes.
FR3046162B1 (fr) * 2015-12-23 2019-12-13 Arkema France Procede de production et de purification du 2,3,3,3-tetrafluoro-1-propene.
FR3046163B1 (fr) * 2015-12-23 2019-12-13 Arkema France Procede de production et de purification du 2,3,3,3-tetrafluoro-1-propene.
FR3046164B1 (fr) * 2015-12-23 2021-01-08 Arkema France Procede de production et de purification du 2,3,3,3-tetrafluoropropene.
US10399004B2 (en) * 2016-09-08 2019-09-03 Eastman Chemical Company Thermally integrated distillation systems and processes using the same
FR3065726B1 (fr) * 2017-04-28 2019-04-19 Arkema France Procede de production et de purification du 2,3,3,3-tetrafluoropropene.
US10351494B1 (en) * 2018-01-08 2019-07-16 Honeywell International Inc. Systems and methods for reducing the formation of impurities during 244bb dehydrochlorination to 1234yf
MX2021005775A (es) 2018-11-15 2021-07-02 Arkema Inc Metodo para purificar una corriente en bruto que contiene hidroclorofluorolefina.
WO2020158668A1 (ja) * 2019-01-28 2020-08-06 ダイキン工業株式会社 １，２－ジフルオロエチレン又は１，１，２－トリフルオロエチレンと、フッ化水素とを含む共沸様組成物
MX2022005324A (es) * 2019-11-06 2022-05-26 Honeywell Int Inc Composiciones azeotropicas o de tipo azeotropo de 3,3,3-trifluoropropino (tfpy) y fluoruro de hidrogeno (hf).
CN113624570B (zh) * 2021-08-06 2023-04-28 清华大学 汽液相平衡装置及氟代烃中的hf的分析方法
US20240018074A1 (en) * 2022-07-14 2024-01-18 Honeywell International Inc. METHOD FOR REDUCING CHLOROFLUOROCARBON IMPURITIES IN THE MANUFACTURE OF TRANS-1,3,3,3-TETRAFLUOROPROPENE (HFO-1234ze(E))
US20240376360A1 (en) * 2023-05-09 2024-11-14 Honeywell International Inc. Azeotrope and azeotrope-like compositions of 1,1,2-trichloro-1,2,2-trifluoroethane (cfc-113) and 1,1,2-trifluoroethane (hfc-143) and applications thereof
US20240376031A1 (en) * 2023-05-10 2024-11-14 Honeywell International Inc. Azeotrope and azeotrope-like compositions of 1,1,2-trifluoroethane (hfc-143) and 1-chloro-1,1,2-trifluoroethane (hcfc-133b) and applications thereof

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2117651C1 (ru) * 1992-12-10 1998-08-20 Аусимонт С.п.А. Способ выделения hf из жидких смесей, содержащий 1,1,1-трифтор-2,2-дихлорэтан и/или 1,1,1,2-тетрафтор-2-хлорэтан
US6521803B1 (en) * 1998-12-18 2003-02-18 Solvay (Societe Anonyme) Method for separating a mixture comprising at least an hydrofluoroalkane and hydrogen fluoride, methods for preparing a hydrofluoroalkane and azeotropic compositions
US20060106263A1 (en) * 2004-10-29 2006-05-18 Miller Ralph N Processes for production and purification of hydrofluoroolefins
CA2626080A1 (en) * 2005-11-01 2007-05-10 E. I. Du Pont De Nemours And Company Azeotrope compositions comprising e-1,3,3,3-tetrafluoropropene and hydrogen fluoride and uses thereof
WO2007053688A2 (en) * 2005-11-01 2007-05-10 E. I. Du Pont De Nemours And Company Azeotrope compositions comprising 1,1,1,2,3-pentafluoropropene and hydrogen fluoride and uses thereof
WO2007053177A1 (en) * 2005-11-01 2007-05-10 E. I. Du Pont De Nemours And Company Azeotrope compositions comprising 1,1,3,3,3-pentafluoropropene and hydrogen fluoride and uses thereof
WO2008012559A1 (en) * 2006-07-27 2008-01-31 Ineos Fluor Holdings Limited Process for separating a fluoropropene from a mixture
US20080045758A1 (en) * 2001-07-20 2008-02-21 Great Lakes Chemical Corporation Halocarbon production processes, halocarbon separation processes, and halocarbon separation systems

Family Cites Families (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2831902A (en) 1957-01-18 1958-04-22 Dow Chemical Co Separation of 2-fluoropropene
US2931840A (en) 1958-11-25 1960-04-05 Du Pont Process for preparing 2, 3, 3, 3-tetrafluoropropene
US2996555A (en) 1959-06-25 1961-08-15 Dow Chemical Co Preparation of 2, 3, 3, 3-tetrafluoropropene
GB1054745A (https=) * 1963-02-13
JPS53116314A (en) * 1977-03-19 1978-10-11 Mitsui Petrochem Ind Ltd Separation of acetic acid and water
SU1706690A1 (ru) 1988-04-19 1992-01-23 Всесоюзный Научно-Исследовательский Институт Технического Углерода Пористый углеродный материал
US4975156A (en) * 1989-05-04 1990-12-04 Atochem North America, Inc. Process for the separation of hydrogen fluoride, 1,1-dichloro-1-fluoroethane and 1-chloro-1,1-difluoroethane from liquid mixtures thereof
WO1993025510A1 (fr) 1992-06-05 1993-12-23 Daikin Industries, Ltd. Procedes d'obtention de 1,1,1,2,3-pentafluoro-propene et de 1,1,1,2,3-pentafluoro-propane
US5396000A (en) 1993-05-24 1995-03-07 E. I. Du Pont De Nemours And Company Process for the manufacture of 1,1,1,2,3,-pentafluoropropane
DE69812901T2 (de) 1997-01-31 2003-11-06 E.I. Du Pont De Nemours And Co., Wilmington Katalytische herstellung von pentafluorpropenen
RU2181114C2 (ru) 1997-03-24 2002-04-10 И.Ай.Дю Пон Де Немурс Энд Кампани Способ получения аддуктов фторсодержащих углеводородов и олефинов
US6031141A (en) 1997-08-25 2000-02-29 E. I. Du Pont De Nemours And Company Fluoroolefin manufacturing process
JP4275313B2 (ja) * 1997-10-17 2009-06-10 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー フッ化水素から１，１，１，３，３−ペンタフルオロプロパンを分離する方法
US5918481A (en) 1997-11-20 1999-07-06 Alliedsignal Inc. Process for separating hydrogen fluoride from fluorocarbons
WO1999026907A1 (en) 1997-11-25 1999-06-03 Imperial Chemical Industries Plc Preparation of fluorine-containing organic compounds
US6013846A (en) 1998-03-05 2000-01-11 Elf Atochem North America, Inc. Azeotrope of HF and 1233zd
DE02705908T1 (de) * 2001-01-25 2004-07-15 Honeywell International Inc. Verfahren zur herstellung von fluorkohlenwasserstoffen
US20030028057A1 (en) 2001-07-20 2003-02-06 Stephen Owens Methods and materials for the preparation and purification of halogenated hydrocarbons
CA2564991C (en) 2004-04-29 2013-03-19 Honeywell International Inc. Processes for synthesis of 1,3,3,3-tetrafluoropropene and 2,3,3,3-tetrafluoropropene
US20060094911A1 (en) * 2004-10-29 2006-05-04 Rao Velliyur N M Noncatalytic manufacture of 1,1,3,3,3-pentafluoropropene from 1,1,1,3,3,3-hexafluoropropane
US7385094B2 (en) 2005-11-01 2008-06-10 E.I. Du Pont De Nemours And Company Azeotrope compositions comprising tridecafluoro-3-heptene and hydrogen fluoride and uses thereof
US7476771B2 (en) 2005-11-01 2009-01-13 E.I. Du Pont De Nemours + Company Azeotrope compositions comprising 2,3,3,3-tetrafluoropropene and hydrogen fluoride and uses thereof
US7709438B2 (en) 2005-11-01 2010-05-04 E. I. Du Pont De Nemours And Company Azeotrope compositions comprising nonafluoropentene and hydrogen fluoride and uses thereof
US7803975B2 (en) * 2006-07-13 2010-09-28 E.I. Du Pont De Nemours And Company Process for separating a fluoroolefin from HF by liquid-liquid extraction
ES2450945T3 (es) 2006-08-24 2014-03-25 E. I. Du Pont De Nemours And Company Procedimientos para la separación de fluoroolefinas a partir de fluoruro de hidrógeno por destilación azeotrópica
WO2009105517A2 (en) 2008-02-21 2009-08-27 E. I. Du Pont De Nemours And Company Azeotrope compositions comprising 3,3,3-trifluoropropene and hydrogen fluoride and processes for separation thereof
KR102136117B1 (ko) 2008-02-21 2020-07-22 더 케무어스 컴퍼니 에프씨, 엘엘씨 공비 증류에 의한 플루오르화수소로부터의 1,3,3,3-테트라플루오로프로펜의 분리 방법

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2117651C1 (ru) * 1992-12-10 1998-08-20 Аусимонт С.п.А. Способ выделения hf из жидких смесей, содержащий 1,1,1-трифтор-2,2-дихлорэтан и/или 1,1,1,2-тетрафтор-2-хлорэтан
US6521803B1 (en) * 1998-12-18 2003-02-18 Solvay (Societe Anonyme) Method for separating a mixture comprising at least an hydrofluoroalkane and hydrogen fluoride, methods for preparing a hydrofluoroalkane and azeotropic compositions
RU2261856C2 (ru) * 1998-12-18 2005-10-10 Солвей (Сосьете Аноним) Способ разделения смеси, содержащей по меньшей мере один гидрофторалкан и фтористый водород, способ получения гидрофторалкана и азеотропная композиция
US20080045758A1 (en) * 2001-07-20 2008-02-21 Great Lakes Chemical Corporation Halocarbon production processes, halocarbon separation processes, and halocarbon separation systems
US20060106263A1 (en) * 2004-10-29 2006-05-18 Miller Ralph N Processes for production and purification of hydrofluoroolefins
CA2626080A1 (en) * 2005-11-01 2007-05-10 E. I. Du Pont De Nemours And Company Azeotrope compositions comprising e-1,3,3,3-tetrafluoropropene and hydrogen fluoride and uses thereof
WO2007053688A2 (en) * 2005-11-01 2007-05-10 E. I. Du Pont De Nemours And Company Azeotrope compositions comprising 1,1,1,2,3-pentafluoropropene and hydrogen fluoride and uses thereof
WO2007053177A1 (en) * 2005-11-01 2007-05-10 E. I. Du Pont De Nemours And Company Azeotrope compositions comprising 1,1,3,3,3-pentafluoropropene and hydrogen fluoride and uses thereof
WO2007053689A2 (en) * 2005-11-01 2007-05-10 E. I. Du Pont De Nemours And Company Azeotrope compositions comprising e-1,3,3,3-tetrafluoropropene and hydrogen fluoride and uses thereof
WO2007053689A3 (en) * 2005-11-01 2007-07-12 Du Pont Azeotrope compositions comprising e-1,3,3,3-tetrafluoropropene and hydrogen fluoride and uses thereof
WO2008012559A1 (en) * 2006-07-27 2008-01-31 Ineos Fluor Holdings Limited Process for separating a fluoropropene from a mixture

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KR20160120803A (ko) 2016-10-18
JP5809331B2 (ja) 2015-11-10
WO2009105521A1 (en) 2009-08-27
KR101937117B1 (ko) 2019-01-09
JP2014193931A (ja) 2014-10-09
CN101952229B (zh) 2014-06-04
KR101851887B1 (ko) 2018-04-24
US8658846B2 (en) 2014-02-25
KR20100138932A (ko) 2010-12-31
KR102136117B1 (ko) 2020-07-22
MX2010009081A (es) 2010-09-07
EP2247560A1 (en) 2010-11-10
CA2712616A1 (en) 2009-08-27
CN101952229A (zh) 2011-01-19
KR20180042459A (ko) 2018-04-25
JP2011513228A (ja) 2011-04-28
BRPI0906015A2 (pt) 2015-06-30
EP2247560B1 (en) 2014-06-04
RU2010138730A (ru) 2012-03-27
ES2483995T3 (es) 2014-08-08
KR20190002750A (ko) 2019-01-08
US20120261252A1 (en) 2012-10-18
KR20200039844A (ko) 2020-04-16

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