RU2236154C2 - Prophylactic product, biologically active food supplement, perfume-cosmetic product based on cedar nut shell and method for it preparing - Google Patents

Abstract

FIELD: food and perfume-cosmetic industry.

SUBSTANCE: invention relates, in particular, to manufacturing dietetic and prophylactic products. Prophylactic products and also biologically active food supplement and perfume-cosmetic product comprising cedar nut shell powder prepared by the definite method. Powder has particles size 10-1200 mcm wherein the lipid content is up to 9.7 wt.-%, the flavonoid content is up to 1.4 wt.-%, the tannins content is up to 9.7 wt.-%, the proteins content is up to 6.9 wt.-%, the polysaccharides content is up to 57.0-58.0%, the potassium content is about 3300 mg/kg, the phosphorus content is about 680 mg/kg, the magnesium content is about 650 mg/kg, the iron content is about 140 mg/kg, the calcium content is about 80 mg/kg, the zinc content is about 35 mg/kg, the copper content is about 2.6 mg/kg. Powder is prepared by grinding cedar nuts shell. Grinding is carried out by formation of two counter flows of dried raw with required rate moving raw in the flow from 100 to 450 m/s with possibility for collision of raw particles in limited zone at temperature that is not lower of the pasteurization point. Invention provides addition of cedar nuts shell obtained by the developed method in cedar nuts shell and this method is directed for formation of optimal composition of cedar nuts shell powder due to operation of intensity of interaction of components.

EFFECT: improved preparing method, valuable properties of supplement.

24 cl

Description

The invention relates to the food industry, in particular to the production of dietary and preventive products, as well as to the perfumery, cosmetic and pharmaceutical industries.

Currently, biologically active substances that are relevant for human and animal nutrition are isolated from various raw materials, including herbs, tree leaves, pine and spruce needles, etc. Coniferous trees are the source of many products valuable to humans: vitamins E, K, F, provitamin A, carotenoids, B vitamins, bioflavonoids, as well as essential amino acids and proteins, from the needles and shoots of pine and spruce extract the components used in preventive medicine. In folk medicine, water infusions from pine and spruce needles are widely used, containing water-soluble components, which are used as anti-zingotic, enhancing the body's immunity, vitaminizing agents for various inflammatory diseases, especially pulmonary. Also widely known are products based on cedar seeds - the kernel of pine nuts, therapeutic agents and multicomponent biologically active additives (BAA) containing pine nut oil, flour from pine kernel kernels, pine nut cake, etc. In preventive and traditional medicine, in the alcoholic beverage industry, pine nuts, the film and shell surrounding the core are used to prepare water-alcohol infusions and alcohol extracts that improve organoleptic characteristics and increase the therapeutic properties of the products. At the same time, alcohol-free products using pine nutshells are little known.

Known therapeutic and prophylactic product according to the patent of the Russian Federation No. 2098985 (publication date 12/20/97) containing honey, cedar oil, pine nutshell, cedar cake, Rhodiola rosea root powder, blade root powder, sea buckthorn oil.

Also known is a therapeutic and prophylactic product according to the patent of the Russian Federation No. 2115336 (publication date 07/20/98), containing honey, cedar oil, pine nutshell (9.7-10.7 wt.%), Cedar cake, propolis tincture, birch buds, fruits of viburnum and rose hips. The combination of components in a certain ratio provides a general strengthening effect on the body and increases its protective functions. The specified therapeutic and prophylactic product is the closest analogue of the developed therapeutic and prophylactic product.

A disadvantage of the known products, including the closest analogue, is that in products containing natural pine nutshells, all the possibilities of increasing the nutritional and medicinal value of this component are not fully used. So, in both known products, pine nutshell is used as a flavoring additive and as a source of cellulose and hemicellulose, other valuable components are not taken into account when forming a composition with desired therapeutic and prophylactic properties.

Products with increased nutritional and medicinal value of the components can be prepared on the basis of fine powders from plant, and / or mineral, and / or animal raw materials. The use of powder, the particle size of which is 1-500 microns, leads to an increase in the digestibility of the components, increases the biological activity of the product by increasing the surface area of the particles and intensifying the process of extracting useful substances.

According to the patent of the Russian Federation No. 2063151 (publication date 10.07.96), a biologically active food supplement based on a powder with a particle size of 0.6-25.0 μm from ginseng root is known.

Known biologically active food supplement based on a powder with a particle size of 50-600 microns from plant materials, containing vitamins, mineral salts and plant fibers (RF patent No. 2110194, publication date 05/10/98). As a plant raw material, it also uses, in a number of traditionally used vegetables, berries and fruits, the roots and rhizomes of herbs and shrubs, the bark of trees and shrubs.

According to the patent of the Russian Federation No. 2167665 (publication date 05/27/01), a biologically active food supplement based on a powder with a particle size of 15-20 microns from black birch fungus fungus is used to normalize metabolism, remove toxins, heavy metals and radionuclides from the body, prevention consequences of radiation exposure, as well as gastrointestinal and cancer diseases.

A disadvantage of known biologically active food additives based on fine powders is that they use expensive and / or rare plant materials, such as ginseng, or rhizomes of herbs, or bark of shrubs, or raw materials that can be consumed by humans in kind, such as vegetables and fruit.

The closest analogue to the developed biologically active food supplement is a biologically active food supplement known by the patent of the Russian Federation No. 2124847 (publication date 01/20/99) - cryopowder from plant and / or mineral raw materials used to improve the properties of the food module. The ability of finely dispersed powders to structure the product, to act as disintegrants, absorbers of excess moisture, as well as dyes, sweeteners, antioxidants, etc. is used. This food supplement can be made practically on the basis of food production wastes, such as shells of seeds of various plants. A nutritional supplement may include cryopowders of cereals, seaweed, shellfish, vegetable greens, eggshells, walnutshells, apricot and almond kernels, pumpkin seeds shells.

However, in the closest analogue, the shell of plant seeds is considered as mineral raw materials, while many useful properties of the shell are lost. In addition, finely dispersed cryopowders in the manufacture are exposed to elevated temperatures only during drying, and subsequent grinding is carried out with simultaneous cooling, and the content of some substances that can be obtained from the shell of seeds of plants by grinding with simultaneous exposure to elevated temperatures is reduced in the closest analogue.

The processed products of plant materials in the form of fine powders are often used as a component in the products of the perfumery and cosmetics industry. Thus, the perfumery and cosmetic product according to patent No. 2163814 is known (publication date 10.04.2000). Cryopowders, in particular cryopowders of vegetable, and / or berry, and / or fruit raw materials, and / or legumes, and / or vegetable greens, and / or cereals, and / or cereals, are used in the perfumery and cosmetic product in the form of cosmetic, hygienic, and pharmacological agents. or their embryos, and / or algae, and / or vegetable medicinal raw materials, and / or mushrooms, and / or shell powders, and / or shells of crustaceans, and / or reptiles, and / or shells of mollusks, while cryopowders have particle sizes 10-800 microns. Powders from natural raw materials, in particular shells, are sources of various natural compounds in perfumes and cosmetics, such as simple sugars, oligosaccharides, flavonoids, organic acids and / or their salts, phenolic substances, amino acids, micro and macro elements and other

Perfume and cosmetic product is also known according to the application No. 96120959 (date of publication 10.01.99). The product is a cosmetic cleansing mask for facial skin care. This perfumery and cosmetic product is the closest analogue of the claimed invention, since in this product, as a finely dispersed vegetable sorbent, crushed pine nuts shell with an average particle size of not more than 20 microns is used.

However, crushed pine nutshell is introduced into the closest analogue only as a mechanically cleansing agent for the skin, and the therapeutic and prophylactic qualities of the powder are not used.

In methods for the manufacture of dehydrated food products, including in the form of powders, such methods as raising and subsequent lowering the temperature and lowering the pressure are traditionally used. Reducing the temperature is often carried out simultaneously with the grinding of raw materials, since upon freezing, the particles of the raw materials become more fragile, and the powder is finer.

A known method of producing a food additive from ginseng root according to the patent of the Russian Federation No. 2063151 (publication date 07/10/96), in which the food additive is obtained by drying the ginseng root to a moisture content of not more than 13%. In this case, the dried ginseng root is crushed in three stages: in the first stage, ginseng root is crushed to a particle size of 3.0-10.0 mm, in the second stage, the crushed mass is treated with liquid nitrogen until the temperature in the whole mass reaches (-170) - (- 180 ) ° C and crushed to a particle size of 25-200 microns, in the third stage, the resulting mass is cooled to a temperature of (-190) - (-193) ° C and crushed to a particle size of 0.6-25.0 microns.

According to the patent of the Russian Federation No. 2110194 (publication date 05/10/98), a method is known for producing a food additive from vegetable (vegetable, and / or berry, and / or fruit, and / or melon) raw materials, which provides for drying the raw material to a moisture content of not more than 10% at a pressure below atmospheric and temperatures below 80 ° C, its preliminary grinding, cooling the resulting mass with a refrigerant to reach a temperature of (-80) - (- 165) ° C in the whole mass, followed by grinding to a particle size of 50-600 microns.

According to the patent of the Russian Federation No. 2167665 (publication date 05/27/01), there is a known method for producing a food supplement based on powder from plant materials, in particular from black birch fungus fungus. Freshly prepared raw materials (chaga birch mushroom) are pre-treated with an inert liquefied gas, and then dried by vacuum sublimation to a residual moisture of chaga of 1-8%. Pre-treatment of freshly prepared raw materials is carried out with an inert liquefied gas for 30-60 minutes. Grinding in an inert liquefied gas medium is carried out to a particle size of 15-20 microns.

A known method of producing a food additive based on powder from plant materials according to the patent of the Russian Federation No. 2176894 (publication date 12/20/01), including drying plant materials (herbs, and / or leaves of trees, and / or leaves of shrubs) using IR radiation at low pressure followed by drying at atmospheric pressure in two stages. The first stage is carried out at a temperature of no higher than 90 ° C for no more than 4 hours, and the second at a temperature of no higher than 60 ° C for no more than 2 hours, after which the dried raw material is cooled over its entire mass to a temperature of no higher than -80 ° C refrigerant and grind at a given temperature in the environment of the refrigerant.

The closest analogue of the developed method for producing a food supplement based on powder from plant materials is the above-described method according to RF patent No. 2176894, which includes several stages proceeding under different conditions and aimed at processing publicly available plant materials. This method, like all of these methods for producing a food supplement based on powder from plant materials, is aimed at preserving useful substances contained in the raw materials in the powder by reducing the intensity of the reaction of the components of the raw materials with the components of the environment and among themselves.

However, in the closest analogue, as in other known methods, substances are not sufficiently processed, the digestibility and amount of which in food additives from plant materials increases with increasing intensity of the reaction of the components of the raw materials with each other. Thus, the content of certain substances in food additives that can be obtained from plant materials by grinding with simultaneous exposure to elevated temperatures is reduced in them.

The task to which the proposed group of inventions is directed is to create products based on powder from plant materials that would be affordable and cheap, namely a therapeutic and prophylactic product and a biologically active food additive, a perfumery and cosmetic product with high therapeutic and preventive value for due to the introduction of pine nutshell powder into the products, obtained by the developed method, aimed at the formation of the optimal composition of pine nutshell powder s by controlling the intensity of the reaction between a raw material components.

The essence of the developed therapeutic and prophylactic product is that it also, as the closest analogue, contains a pine nut shell.

New in the developed therapeutic product is that it contains pine nutshells in the form of a powder with particle sizes of 10-1200 microns, where the lipid content is up to 9.7 wt.%, Flavonoids up to 1.4 wt.%, Tannides up to 5.5 wt.%, proteins up to 6.9 wt.%, polysaccharides 57.0-58.0 wt.%, potassium approximately 3300 mg / kg, phosphorus approximately 680 mg / kg, magnesium approximately 650 mg / kg, iron - approximately 140 mg / kg, calcium - approximately 80 mg / kg, zinc - approximately 35 mg / kg, copper - approximately 2.6 mg / kg.

In a specific implementation, the content of pine powder shell powder in the developed therapeutic product is 99.5%.

In a particular case, the therapeutic product additionally contains plant and / or animal raw materials.

In another particular case, the therapeutic product as a vegetable raw material contains vegetables and / or grains and / or fruits.

In specific implementations of a therapeutic and prophylactic product, the amount of pine nut shell powder in the production of bakery products is up to 10 wt.%, In the production of soft drinks - up to 15 wt.%, In the manufacture of confectionery products - up to 10 wt.%, In the production of meat products - up to 7 wt.%, dairy products up to 3 wt.%.

In other special cases of a therapeutic and prophylactic product, the amount of pine nut shell powder in the preparation of feed for dairy cows is up to 60 grams per head per day, for calves - up to 15 grams per head per day, for poultry - up to 3 grams per head per day.

The essence of the developed biologically active food supplement is that it also, as the closest analogue, contains plant seed shell powder.

New in the developed dietary supplement is that it contains pine nutshell powder as a shell powder. In a specific implementation, the content in the powder of the pine nutshell shell is up to 9.7 wt.%, Flavonoids - up to 1.4 wt.%, Tannins - up to 5.5 wt.%, Proteins - up to 6.9 wt.%, Polysaccharides - 57.0-58.0 wt.%, Potassium - approximately 3300 mg / kg, phosphorus - approximately 680 mg / kg, magnesium - approximately 650 mg / kg, iron - approximately 140 mg / kg, calcium - approximately 80 mg / kg; zinc, approximately 35 mg / kg; copper, approximately 2.6 mg / kg.

In a particular case, the biologically active food supplement additionally contains vitamins and / or sterols and / or fats and / or saponins.

In a specific implementation in a biologically active food supplement, vegetable and / or animal raw materials are used as sources of vitamins and / or fats and / or sterols and / or saponins.

In another specific implementation, in a biologically active food additive, medicinal plants, and / or cereal and / or vegetable raw materials or their extracts are used as plant materials.

In another particular case, the biologically active food supplement further comprises binders.

In another particular case, the biologically active food supplement is made in tablet or dosage form.

The essence of the developed perfumery and cosmetic product is that it, as well as the closest analogue, contains pine pine shell powder.

New in the developed perfumery and cosmetic product is that in it the powder from the pine nutshell is obtained by the developed method and contains lipids - up to 9.7 wt.%, Flavonoids - up to 1.4 wt.%, Tannides - up to 5.5 wt. wt.%, proteins - up to 6.9 wt.%, polysaccharides - 57.0-58.0 wt.%, potassium - approximately 3300 mg / kg, phosphorus - approximately 680 mg / kg, magnesium - approximately 650 mg / kg, iron — about 140 mg / kg; calcium — about 80 mg / kg; zinc — about 35 mg / kg; copper — about 2.6 mg / kg.

In a specific implementation, in the manufacture of perfumes and cosmetics, the perfumes and cosmetics product further comprises technological components.

In the particular case of the perfumery-cosmetic product, the powder of pine nutshell shells makes up to 10% of the mass of technological components.

The essence of the developed method for producing powder from plant materials is that it, like the closest analogue, includes drying of plant materials with subsequent grinding.

New in the developed method is that the raw materials are crushed by forming two counter flows of dried raw materials with a given speed of movement of the raw materials in the stream from 100 to 450 m / s with the possibility of collision of particles of raw materials in a limited area at a temperature not lower than the pasteurization temperature.

In the particular case of the method, part of the raw material is used to form counter flows at least twice.

In a specific implementation of the method according to a predetermined rule, the volume of part of the feed and the speed of the oncoming flows are determined for the second formation of the oncoming flows and, accordingly, each subsequent one.

In the claimed therapeutic and prophylactic product, the use of cedar shells in the form of a powder with a particle size of 10-1200 μm, with a specified content of lipids, flavonoids, tannides, proteins, polysaccharides, potassium, phosphorus, magnesium, iron, calcium, zinc and copper allows you to expand the range food products with improved consumer characteristics. Thus, the high content of the polysaccharide fraction allows us to recommend the developed product as a source of dietary fiber to normalize digestion. The presence of tannins and polysaccharides contributes to the improvement of the functioning of the gastrointestinal tract. The presence of lipids improves lipid metabolism. Studies have shown in the developed product a high content of protein, flavonoids, essential minerals. A product containing almost exclusively pine nut shell powder has a high nutritional and therapeutic value, since it can be used without additional ingredients if a wide spectrum of biological activity is revealed. Introduction to the developed therapeutic product of additional plant and / or animal raw materials is aimed at improving the properties of a number of food products. A therapeutic and prophylactic product in the form of compositions of pine nut powder and plant materials such as vegetables, and / or cereals, and / or fruits, is the basis of the diet food - baby food, therapeutic nutrition.

The composition of the developed product allows its use in food compositions in the production of bakery products (up to 10 wt.%), Where the structuring function of polysaccharides is used. In the production of soft drinks, the developed product is used as a source of flavonoids: R-vitamin and tannides - tonic and vaso-strengthening substances. Flavonoids in pine nutshell powder are also a valuable food coloring. In the production of meat products, the function of flavonoids as stabilizers of fats is highlighted, for dairy products, among other things, pine nut shell powder is of great importance as a source of polysaccharides that ensure product homogeneity.

The composition of the developed product, especially the presence of a complex of lipids, allows you to use it as a therapeutic and prophylactic product in the preparation of feed for animals and poultry.

In the claimed biologically active food supplement, introducing into the shells of seeds of plants in the form of a powder of shells of pine nuts with the indicated content of lipids, flavonoids, tannides, proteins, polysaccharides, potassium, phosphorus, magnesium, iron, calcium, zinc and copper allows to increase the value of therapeutic and prophylactic preparations due to a wide range of biological activity. The introduction of vitamins and / or sterols, and / or fats, and / or saponins, in addition to the powder of the pine nutshell powder, into the developed nutritional supplement allows the formation of more narrowly directed compositions. The introduction of plant materials, such as medicinal plants, and / or cereal and / or vegetable raw materials or their extracts, binders allows you to expand the variety of forms of food additives. The implementation of biologically active food additives in tablet or dosage form increases usability.

The high content of the polysaccharide fraction allows us to recommend the developed biologically active food supplement as a source of dietary fiber to normalize digestion. The tannins contained in it contribute to improving the functioning of the gastrointestinal tract, and also have pronounced anti-inflammatory, analgesic, and hemostatic properties. A balanced lipid fraction also improves the functioning of the gastrointestinal tract. In the claimed biologically active food supplement, the content of protein and bioflavonoids is increased. Bioflavonoids exhibit antioxidant activity and are direct antihypoxants, while they have a wide range of useful pharmacological properties, including membrane-stabilizing, immunomodulating, anti-inflammatory, capillary-healing wound healing effects. They are characterized by a combination of high biological activity and low toxicity (15-17 units). In the claimed biologically active food supplement, the content of certain essential mineral substances is also increased. Regular use of the developed dietary supplement in recommended doses will make it possible to fill up to 1/4 of the average daily requirement for copper and 1/3 of the daily requirement for iron, which confirms the advisability of using the developed dietary supplement for anemia. Due to the developed biologically active nutritional supplement, it is possible to fill in 1/2 the daily requirement for manganese, necessary, for example, to ensure the process of splitting arginine to urea - the final product of nitrogen metabolism, as well as for the flow of vital for the regulation of vital body functions (cell proliferation, muscle contraction, metabolic cascades, immune reactions, etc.) of phosphorylation reactions. The developed food supplement contains silicon, zinc, and nickel in significant quantities.

In the developed perfumery and cosmetic product, pine nutshell powder due to the lipids, flavonoids, tannides, proteins, polysaccharides, potassium, phosphorus, magnesium, iron, calcium, zinc and copper contained in it provides a wound healing, strengthening, fortifying, tonic effect on the skin with the implementation of perfumes and cosmetics in the form of creams, scrubs, masks, cleansing lotions, hair colors, as well as on the mucous membranes when performing the perfumes and cosmetics in the form of toothpaste or lips oh lipstick. The introduction of various technological components provides an expansion of the variety of forms and types of perfumes and cosmetics.

In the developed method for producing powder from plant materials, crushing of pine nuts shells is carried out in a limited area in counter flows of shell particles. The range of possible flow velocities is selected for reasons of the most efficient grinding of at least 100 m / s; at flow velocities of more than 450 m / s, the raw material particles can ignite, since the process temperature rises in proportion to the collision speed of the raw material particles. At the same time, by setting the flow velocity from the interval from 100 to 450 m / s, the specified collision intensity is provided, which means destruction of the shell particles and their transformation into powder. Setting the process temperature not lower than the pasteurization temperature ensures the disinfection of the powder, this allows to separate the drying and grinding operations in time. The task of the speed of raw materials in the stream is aimed at providing the ability to vary the composition of the powder of the shell of pine nuts within the established limits. So, at a high flow rate in the resulting product (and a high collision intensity), the polysaccharide content will be increased, at low - the powder will become a source of mainly tannides. This occurs not only due to an increase in the degree of grinding and, accordingly, the recoverability of the components, but also due to the intensification of the reactions of the components of the pine nutshell shells among themselves. All this allows you to formulate the composition of the resulting powder in accordance with the goals of its further use, in addition, the method provides the ability to align the performance of the powder of the shell of pine nuts in accordance with the changing composition of the raw material. The use of a certain part of the raw material for the formation of oncoming flows two or more times allows achieving the desired indicators even more precisely. In this case, the same particle of the raw material will be exposed several times to elevated temperatures during the collision time, which will lead to a predetermined change in the product parameters. At the same time, it is advisable for each type of product to be produced, according to the data on the composition of the raw materials, to pre-set the number of parts of the raw materials included in the stream, the volumes of the parts of the raw materials and the speed of the oncoming flows, which enhances the indicated effect.

Thus, in the presented group of inventions, united by one inventive concept, the expansion of the spectrum of biological activity of products is achieved by introducing pine powder shell powder with improved properties into them, obtained by the developed method, aimed at intensifying the reactions of raw material components and providing increased stability of product parameters, insensitivity product to fluctuations in the composition of raw materials, the ability to obtain pine powder shell powder with desired properties and, consistent with the intended use, by implementing the actions of the method.

New unknown properties of pine nut shell powder were revealed during testing at the St. Petersburg State Chemical Pharmaceutical Academy, the Central Scientific Research Forest Chemical Institute, and the Scientific Research Institute of Chemistry of Nizhny Novgorod State University Lobachevsky, Scientific Research Veterinary Institute of the Non-Black Earth Zone of the Russian Federation, Russian Academy of Agricultural Sciences.

Specialists of the Central Scientific Research Forest Chemical Institute, Scientific Research Institute of Chemistry, Nizhny Novgorod State University Lobachevsky conducted a study of the chemical composition of the powder of the shell of pine nuts, experimental batches of which are made for research purposes using the developed method. An important result of the research was the presence of tannid pine nuts in the powder, generally speaking, atypical of coniferous seeds.

The work of the St. Petersburg State Chemical Pharmaceutical Academy was related to the study of indicators of biologically active food additives (BAA) based on pine nutshell powder. It is shown that the developed biologically active food supplement has a number of unique properties that expand the indications for use and has no analogues in the spectrum of pharmacological activity among dietary supplements registered in Russia.

At the Scientific Research Veterinary Institute of the Non-Black Earth Zone of the Russian Academy of Medical Sciences, studies were conducted on feeding powder of pine nutshell to calves of prophylactic age, dairy cows and poultry. Feeding standards have been established: the amount of pine nut shell powder in the preparation of feed for dairy cows is up to 60 grams per head per day, for calves - up to 15 grams per head per day, for poultry - up to 3 grams per head per day. In animals, normalization of carbohydrate and lipid metabolism was noted. The therapeutic and prophylactic food product when fed to animals has a positive effect on the indicators of natural resistance and the immune status of the blood, while providing a preventive effect in case of gastrointestinal diseases. An effect was noted in the form of a reduction in the time course of gastrointestinal diseases of calves by 1-3 days, as well as a positive effect on metabolic processes and an increase in milk productivity in dairy cows.

A therapeutic and prophylactic product, a biologically active food additive, and a perfumery and cosmetic product can be used, for example, as follows.

The therapeutic and prophylactic product in the form of bakery products according to claim 5 of the claims is made according to traditional technology for bread, the powder of the pine nut shell in the recommended amounts is mixed with flour when kneading the dough. Also, confectionery based on flour - gingerbread cookies, cookies are also made. In the confectionery according to claim 6, the therapeutic and prophylactic product is used in the form of a filling for waffles, gingerbread, cookies, sweets, in the form of jam, jam, etc. The treatment-and-prophylactic product according to claim 7 of the invention in the form of meat products also does not require changes in known technologies, cedar nutshell powder is added to sausage, dumplings, cutlets, and pasta minced meat as spices are usually added. In the manufacture of a therapeutic and prophylactic product based on unrefined meat, pine nutshell powder is applied to the surface of the product before baking, smoking, curing, as well as spices and flavorings. In the manufacture of a therapeutic and prophylactic product according to claim 9 of the claims in the form of a non-alcoholic beverage, pine powder shell powder, in addition to the therapeutic and prophylactic functions, also functions as a coloring and flavoring additive. In drinks, it is advisable to use both powder and its extract. At the same time, the use of a therapeutic and prophylactic product, for example, according to claim 9, in the form of a food product as such is possible with a content of 99.5% pine nut shell powder in it. It can be added to any dish to the taste of the person applying, but can be eaten directly, for example, mixed in a small amount of water, can be brewed as fragrant tea, etc. When using a therapeutic and prophylactic product in the form of animal feed, for example, according to claim 11, one dose (up to 15 grams) of pine nut shell powder is diluted in 100-150 ml of warm boiled water and the calf is evaporated once a day, starting with birthday, 20-30 minutes before the second feed with colostrum for 10 days.

The dietary supplement according to claims 13, 14 of the claims can be used as a general strengthening agent for metabolic disorders, as well as a natural source of dietary fiber to normalize the functions of the gastrointestinal tract. It is recommended to take 2 powders (one powder - approximately one teaspoon) 3 times a day before a dietary supplement in the form of a powder of pine nutshell shells. Before use, pine nutshell powder is dissolved in half a glass of boiled water. Duration of admission is 2-3 weeks. The biologically active food supplement according to claim 19 is carried out in a dosage form, for example, for convenience, the powder product can be packaged in tea leaves.

Perfume and cosmetic product according to claim 20 of the claims can be made in the form of shampoo, cream, mask, toothpaste, lipstick, etc. For the manufacture of, for example, toothpaste with a pleasant aroma, taste and color, and at the same time with enhanced therapeutic and prophylactic properties, pine nut shell powder is introduced into the composition of silicon dioxide, sorbitol, sodium carboxymethyl cellulose, sodium monofluorophosphate, sodium fluoride, titanium dioxide , methylparaben sodium salt. In the perfumery and cosmetic product, CO ₂ pine nut powder extract can also be used.

Developed therapeutic and prophylactic product, biologically active food additive and perfumery and cosmetic product are made by the developed method using a device that includes a container, for example, in the form of a drum or box, restricting the zone of collision of the flows of raw material particles. Streams are formed using a compressor or due to the rotation of the end elements of the container in the form of a drum. It is most advisable to rotate the end elements of the detachable container in the form of a drum with the help of electric motors so that the rotation of the elements is multidirectional. In this case, a predetermined speed of oncoming circular flows of raw materials is achieved, and a degree of closure of the collision zone of the particles of raw materials sufficient to ensure a corresponding rise in the process temperature. In case of insufficient rise in the process temperature, for example, at low flow rates or in the presence of substantial gaps between the container parts, additional heating can be provided. Shell particles in streams collide at a high relative speed and are effectively destroyed to the state of a fine powder, while the surface area and, accordingly, the area of heating and reaction of shell particles increase. If it is necessary to achieve the specified parameters of the composition of the powder, it is possible to return a part of the crushed shell after the first grinding stage to the collision zone. The control of the residence time of the shell powder particles in the collision zone under shock and thermal action leads to an increase in the content of the target components in the final product.

Claims (24)

1. A preventive product containing a pine nut shell, characterized in that the pine nut shell is used in the form of a powder obtained by the method according to item 22, with particle sizes of 10-1200 μm, where the lipid content is up to 9.7 wt.%, Flavonoids up to 1.4 wt.%, Tannides up to 5.5 wt.%, Proteins up to 6.9 wt.%, Polysaccharides 57.0-58.0%, potassium approximately 3300 mg / kg, phosphorus approximately 680 mg / kg, magnesium approximately 650 mg / kg, iron approximately 140 mg / kg, calcium approximately 80 mg / kg, zinc approximately 35 mg / kg, copper approximately 2.6 mg / kg. 2. Preventive product according to claim 1, characterized in that the content of the powder of the pine shell shell is 99.5%. 3. The preventive product according to claim 1, characterized in that it further comprises plant and / or animal raw materials. 4. Preventive product according to claim 3, characterized in that the vegetable raw material contains vegetables and / or cereals and / or fruits. 5. Preventive product according to claim 3 or 4, characterized in that in the production of bakery products the amount of powder of the pine nut shell is up to 10 wt.%. 6. A prophylactic product according to claim 3 or 4, characterized in that in the manufacture of confectionery products, the amount of cedar nut shell powder is up to 10 wt.%. 7. Preventive product according to claim 3 or 4, characterized in that in the production of meat products, the amount of powder of the shell of pine nuts is up to 7 wt.%. 8. A prophylactic product according to claim 3 or 4, characterized in that in the production of dairy products, the amount of cedar nut shell powder is up to 3 wt.%. 9. Preventive product according to claim 3 or 4, characterized in that in the production of non-alcoholic drinks the amount of pine powder shell powder is up to 15 wt.%. 10. The prophylactic product according to claim 1, characterized in that in the production of feed for dairy cows the amount of powder of the pine nut shell is up to 60 g per head per day. 11. The preventive product according to claim 1, characterized in that in the production of feed for calves, the amount of powder of the shell of pine nuts is up to 15 g per head per day. 12. The prophylactic product according to claim 1, characterized in that in the production of feed for poultry, the amount of pine nut shell powder is up to 3 g per head per day. 13. A biologically active food supplement containing plant seed shell powder, characterized in that the shell powder contains pine nut shell powder obtained by the method according to claim 22 and containing lipids up to 9.7 wt.%, Flavonoids up to 1.4 wt. %, tannides up to 5.5 wt.%, proteins up to 6.9 wt.%, polysaccharides 57.0-58.0%, potassium approximately 3300 mg / kg, phosphorus approximately 680 mg / kg, magnesium approximately 650 mg / kg, iron approximately 140 mg / kg, calcium approximately 80 mg / kg, zinc approximately 35 mg / kg, copper approximately 2.6 mg / kg. 14. The dietary supplement of claim 13, further comprising vitamins and / or sterols and / or fats and / or saponins. 15. A biologically active food supplement according to claim 14, characterized in that it contains vegetable and / or animal raw materials as sources of vitamins and / or fats and / or sterols and / or saponins. 16. The biologically active food supplement according to claim 13, characterized in that it further comprises medicinal plants, and / or grain and / or vegetable raw materials or their extracts. 17. A biologically active food supplement according to claim 13, or 14, or 15, or 16, characterized in that it further comprises binders. 18. Biologically active food supplement according to item 13, or 14, or 15, or 16, or 17, characterized in that it is made in tablet or dosage form. 19. Perfume and cosmetic product containing a powder of pine nutshell, characterized in that it contains a powder of pine nutshell, obtained by the method according to item 22, contains lipids up to 9.7 wt.%, Flavonoids up to 1.4 wt. %, tannides up to 5.5 wt.%, proteins up to 6.9 wt.%, polysaccharides 57.0-58.0%, potassium approximately 3300 mg / kg, phosphorus approximately 680 mg / kg, magnesium approximately 650 mg / kg iron about 140 mg / kg, calcium about 80 mg / kg, zinc about 35 mg / kg, copper about 2.6 mg / kg. 20. Perfume and cosmetic product according to claim 19, characterized in that in the manufacture of perfume and cosmetic products additionally contains technological components. 21. Perfume and cosmetic product according to claim 20, characterized in that the powder from the shell of pine nuts makes up to 10% by weight of the technological components. 22. A method of producing powder from plant materials, including drying of plant materials followed by grinding, characterized in that pine nutshells are used as plant materials, grinding is carried out by forming two counter flows of dried raw materials with a given speed of movement of the raw materials in the stream from 100 to 450 m / s with the possibility of collision of particles of raw materials in a limited area at a temperature not lower than the pasteurization temperature. 23. The method according to item 22, wherein the part of the raw material is used to form counter flows at least twice. 24. The method according to item 23, wherein the volume of the portion of the raw materials used for each re-formation of the oncoming flows, and the speed of the oncoming flows for each formation is determined before the start of the corresponding re-formation for each type of product produced in accordance with the composition of the raw materials.