RU2014149844A - Улучшенный способ выделения бутанола - Google Patents
Улучшенный способ выделения бутанола Download PDFInfo
- Publication number
- RU2014149844A RU2014149844A RU2014149844A RU2014149844A RU2014149844A RU 2014149844 A RU2014149844 A RU 2014149844A RU 2014149844 A RU2014149844 A RU 2014149844A RU 2014149844 A RU2014149844 A RU 2014149844A RU 2014149844 A RU2014149844 A RU 2014149844A
- Authority
- RU
- Russia
- Prior art keywords
- stream
- distillation column
- butanol
- fraction
- organic compounds
- Prior art date
Links
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 title claims abstract 68
- 238000000034 method Methods 0.000 title claims abstract 28
- 238000004821 distillation Methods 0.000 claims abstract 53
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract 51
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract 25
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims abstract 20
- 150000002894 organic compounds Chemical class 0.000 claims abstract 13
- 239000012071 phase Substances 0.000 claims abstract 12
- 239000012855 volatile organic compound Substances 0.000 claims abstract 12
- 239000008346 aqueous phase Substances 0.000 claims abstract 9
- 239000012074 organic phase Substances 0.000 claims abstract 9
- 239000000203 mixture Substances 0.000 claims abstract 8
- GNFTZDOKVXKIBK-UHFFFAOYSA-N 3-(2-methoxyethoxy)benzohydrazide Chemical compound COCCOC1=CC=CC(C(=O)NN)=C1 GNFTZDOKVXKIBK-UHFFFAOYSA-N 0.000 claims 6
- 238000011084 recovery Methods 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
- C07C29/82—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation by azeotropic distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/10—Vacuum distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B63/00—Purification; Separation; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C31/02—Monohydroxylic acyclic alcohols
- C07C31/12—Monohydroxylic acyclic alcohols containing four carbon atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB1210256.2 | 2012-06-11 | ||
| GBGB1210256.2A GB201210256D0 (en) | 2012-06-11 | 2012-06-11 | Improved butanol recovery process |
| PCT/US2013/043987 WO2013188162A1 (en) | 2012-06-11 | 2013-06-04 | Improved butanol recovery process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| RU2014149844A true RU2014149844A (ru) | 2016-07-27 |
Family
ID=46605716
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2014149844A RU2014149844A (ru) | 2012-06-11 | 2013-06-04 | Улучшенный способ выделения бутанола |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US20150152032A1 (forum.php) |
| EP (1) | EP2858967A1 (forum.php) |
| KR (1) | KR20150035579A (forum.php) |
| CN (2) | CN203923057U (forum.php) |
| BR (1) | BR112014030950A2 (forum.php) |
| GB (1) | GB201210256D0 (forum.php) |
| IN (1) | IN2015MN00013A (forum.php) |
| RU (1) | RU2014149844A (forum.php) |
| WO (1) | WO2013188162A1 (forum.php) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB201210256D0 (en) * | 2012-06-11 | 2012-07-25 | Invista Tech Sarl | Improved butanol recovery process |
| GB201507234D0 (en) * | 2015-04-28 | 2015-06-10 | Johnson Matthey Davy Technologies Ltd | Process |
| KR101959467B1 (ko) * | 2015-07-02 | 2019-07-02 | 주식회사 엘지화학 | 증류 장치 |
| CN106008158A (zh) * | 2016-05-24 | 2016-10-12 | 新疆天业（集团）有限公司 | 从低浓度有机废水中回收丁醇的装置及工艺 |
| CN109260748A (zh) * | 2018-11-26 | 2019-01-25 | 宁夏北控睿源再生资源有限公司 | 一种废甲醇生产回收装置及方法 |
| FR3120874B1 (fr) * | 2021-03-22 | 2023-03-10 | Ifp Energies Now | Procédé d’extraction d’alcools à partir d’un mélange initial comprenant des alcools en phase aqueuse |
| CN113289363A (zh) * | 2021-05-11 | 2021-08-24 | 天津天润化工科技有限公司 | 一种粗甲醇精制提纯系统 |
| US11612829B1 (en) * | 2022-06-18 | 2023-03-28 | David Norbert Kockler | Process for the separation of multicomponent mixtures using a prefractionation/main column arrangement |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IT1256062B (it) * | 1992-11-20 | 1995-11-23 | Snam Progetti | Procedimento per l'ottenimento di correnti di metanolo, etanolo, n-propanolo,isobutanolo,utilizzabili soprattutto nella preparazione diprodotti alto ottanici, da miscele contenenti detti alcoli con acqua ed altri composti bassobollenti e altobollenti |
| US8968523B2 (en) * | 2009-07-15 | 2015-03-03 | Butamax Advanced Biofuels Llc | Recovery of butanol isomers from a mixture of butanol isomers, water, and an organic extractant |
| GB201210256D0 (en) * | 2012-06-11 | 2012-07-25 | Invista Tech Sarl | Improved butanol recovery process |
| US9018426B1 (en) * | 2013-12-19 | 2015-04-28 | Celanese International Corporation | Processes for producing multi-carbon alcohols |
-
2012
- 2012-06-11 GB GBGB1210256.2A patent/GB201210256D0/en not_active Ceased
-
2013
- 2013-06-04 US US14/406,898 patent/US20150152032A1/en not_active Abandoned
- 2013-06-04 IN IN13MUN2015 patent/IN2015MN00013A/en unknown
- 2013-06-04 KR KR20147034397A patent/KR20150035579A/ko not_active Withdrawn
- 2013-06-04 RU RU2014149844A patent/RU2014149844A/ru unknown
- 2013-06-04 WO PCT/US2013/043987 patent/WO2013188162A1/en active Application Filing
- 2013-06-04 BR BR112014030950A patent/BR112014030950A2/pt not_active IP Right Cessation
- 2013-06-04 EP EP13803911.0A patent/EP2858967A1/en not_active Withdrawn
- 2013-06-13 CN CN201320337171.4U patent/CN203923057U/zh not_active Expired - Lifetime
- 2013-06-13 CN CN201310232441.XA patent/CN103483147B/zh active Active
Also Published As
| Publication number | Publication date |
|---|---|
| BR112014030950A2 (pt) | 2017-06-27 |
| IN2015MN00013A (forum.php) | 2015-10-16 |
| WO2013188162A1 (en) | 2013-12-19 |
| CN203923057U (zh) | 2014-11-05 |
| CN103483147A (zh) | 2014-01-01 |
| US20150152032A1 (en) | 2015-06-04 |
| EP2858967A1 (en) | 2015-04-15 |
| CN103483147B (zh) | 2016-05-04 |
| GB201210256D0 (en) | 2012-07-25 |
| KR20150035579A (ko) | 2015-04-06 |
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