RU2010133701A - METHOD FOR PRODUCING 1,3,5-THIADIAZINAN-4- (TI) ON - Google Patents

METHOD FOR PRODUCING 1,3,5-THIADIAZINAN-4- (TI) ON Download PDF

Info

Publication number
RU2010133701A
RU2010133701A RU2010133701/04A RU2010133701A RU2010133701A RU 2010133701 A RU2010133701 A RU 2010133701A RU 2010133701/04 A RU2010133701/04 A RU 2010133701/04A RU 2010133701 A RU2010133701 A RU 2010133701A RU 2010133701 A RU2010133701 A RU 2010133701A
Authority
RU
Russia
Prior art keywords
buona
carbamide
thio
thiadiazinan
butanol
Prior art date
Application number
RU2010133701/04A
Other languages
Russian (ru)
Other versions
RU2447067C1 (en
Inventor
Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
Внира Рахимовна Ахметова (RU)
Внира Рахимовна Ахметова
Регина Радиевна Хайруллина (RU)
Регина Радиевна Хайруллина
Асхат Габдрахманович Ибрагимов (RU)
Асхат Габдрахманович Ибрагимов
Райхана Валиулловна Кунакова (RU)
Райхана Валиулловна Кунакова
Original Assignee
Учреждение Российской академии наук ИНСТИТУТ НЕФТЕХИМИИ И КАТАЛИЗА РАН (RU)
Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Учреждение Российской академии наук ИНСТИТУТ НЕФТЕХИМИИ И КАТАЛИЗА РАН (RU), Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран filed Critical Учреждение Российской академии наук ИНСТИТУТ НЕФТЕХИМИИ И КАТАЛИЗА РАН (RU)
Priority to RU2010133701/04A priority Critical patent/RU2447067C1/en
Publication of RU2010133701A publication Critical patent/RU2010133701A/en
Application granted granted Critical
Publication of RU2447067C1 publication Critical patent/RU2447067C1/en

Links

Landscapes

  • Nitrogen- Or Sulfur-Containing Heterocyclic Ring Compounds With Rings Of Six Or More Members (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

Способ получения 1,3,5-тиадиазинан-4-(ти)онов общей формулы (1): ! ! отличающийся тем, что насыщенный сероводородом водный 37%-ный раствор формальдегида подвергают взаимодействию со свежеприготовленной смесью (тио)карбамид - н-BuONa (в бутаноле) при мольном соотношении исходных реагентов (тио)карбамид:CH2O:H2S:н-BuONa, равном 10:20:20:40 при температуре 70-90°C и атмосферном давлении в течение 5-7 ч. The method of obtaining 1,3,5-thiadiazinan-4- (ty) ones of the general formula (1):! ! characterized in that the aqueous 37% solution of formaldehyde saturated with hydrogen sulfide is reacted with a freshly prepared mixture of (thio) carbamide - n-BuONa (in butanol) at a molar ratio of the starting reagents (thio) carbamide: CH2O: H2S: n-BuONa equal to 10 : 20: 20: 40 at a temperature of 70-90 ° C and atmospheric pressure for 5-7 hours

Claims (1)

Способ получения 1,3,5-тиадиазинан-4-(ти)онов общей формулы (1):The method of obtaining 1,3,5-thiadiazinan-4- (ty) ones of the general formula (1):
Figure 00000001
Figure 00000001
 отличающийся тем, что насыщенный сероводородом водный 37%-ный раствор формальдегида подвергают взаимодействию со свежеприготовленной смесью (тио)карбамид - н-BuONa (в бутаноле) при мольном соотношении исходных реагентов (тио)карбамид:CH2O:H2S:н-BuONa, равном 10:20:20:40 при температуре 70-90°C и атмосферном давлении в течение 5-7 ч. characterized in that the aqueous 37% solution of formaldehyde saturated with hydrogen sulfide is reacted with a freshly prepared mixture of (thio) carbamide - n-BuONa (in butanol) at a molar ratio of the starting reagents (thio) carbamide: CH 2 O: H 2 S: n- BuONa, equal to 10: 20: 20: 40 at a temperature of 70-90 ° C and atmospheric pressure for 5-7 hours.
RU2010133701/04A 2010-08-11 2010-08-11 Method of producing 1,3,5-thiadiazinan-4-(thi)ones RU2447067C1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RU2010133701/04A RU2447067C1 (en) 2010-08-11 2010-08-11 Method of producing 1,3,5-thiadiazinan-4-(thi)ones

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RU2010133701/04A RU2447067C1 (en) 2010-08-11 2010-08-11 Method of producing 1,3,5-thiadiazinan-4-(thi)ones

Publications (2)

Publication Number Publication Date
RU2010133701A true RU2010133701A (en) 2012-02-20
RU2447067C1 RU2447067C1 (en) 2012-04-10

Family

ID=45854271

Family Applications (1)

Application Number Title Priority Date Filing Date
RU2010133701/04A RU2447067C1 (en) 2010-08-11 2010-08-11 Method of producing 1,3,5-thiadiazinan-4-(thi)ones

Country Status (1)

Country Link
RU (1) RU2447067C1 (en)

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IL104081A (en) * 1991-12-21 1996-05-14 Basf Ag Preparation of substantially dust-free tetrahydro-3, 5-dimethyl-1, 3, 5-thiadiazine-2-thione granules
KR100329700B1 (en) * 1994-12-30 2002-10-25 주식회사 엘지씨아이 Process for preparing tetrahydro-1,3,5-thiadiazin-4-one

Also Published As

Publication number Publication date
RU2447067C1 (en) 2012-04-10

Similar Documents

Publication Publication Date Title
RU2010131168A (en) SULFENAMIDE, VOLCANIZATION ACCELERATOR OF RUBBER CONTAINING SULFENAMID AND METHOD FOR PRODUCING VULCANIZATION ACCELERATOR
RU2010132919A (en) METHOD FOR SELECTIVE OBTAINING α, ω-BIS- (1,3,5-DITIAZINAN-5-IL) -3-OXOPENTANE And α, ω-BIS- (1,3,5-DITIAZINAN-5-IL) -3,6 -DIOXOACTANE
RU2008122310A (en) TWO-COMPONENT HYDROGEN HYDROGEN ABSORBENT AND METHOD FOR ITS PRODUCTION
RU2005114653A (en) METHOD FOR PRODUCING 5- [ORTO- (STEAM -) - HYDROXYPHENYL] -1,3,5-Dithiazines
AR064658A1 (en) PROCESS TO PREPARE DULOXETINE AND ITS RELATED COMPOUNDS, AS WELL AS ALSO USEFUL INTERMEDIARIES IN THE SAME
RU2010108950A (en) METHOD FOR PRODUCING 3,7-DIARIL-1,3,5,7-DITIADIAZAOCTANES
CO6341607A2 (en) SEVOFLURAN SYNTHESIS METHOD
RU2009100738A (en) METHOD FOR PRODUCING 2-PROPYL-3-ETHYLQUINOLINE
RU2005114640A (en) METHOD FOR PRODUCING N-METHYLENE-4H-1,3,5-Dithiazinyl-5 (6H) AMINE
RU2010133701A (en) METHOD FOR PRODUCING 1,3,5-THIADIAZINAN-4- (TI) ON
RU2006128805A (en) METHOD FOR PRODUCING 3-TIA-1,5-DIAZABICYCLO [4,3,1] DECAN AND 5- [4- (1,3,5-DITIAZINAN-5-IL) BUTYL] 1,3,5-DITIAZINAN
RU2012100111A (en) METHOD FOR PRODUCING 2- AND 2,3-SUBSTITUTED QUINOLINS
RU2010122542A (en) METHOD FOR PRODUCING MONO- (DI-, TETRA-) METHYL-1,2-BIS- (1,3,5-DITIAZINAN-5-IL) ETHANES
RU2009102797A (en) METHOD FOR SELECTIVE OBTAINING 2-, 3-, AND 4- (1,3,5-DITIAZINAN-5-IL) THIOPHENOLS
RU2010108958A (en) METHOD FOR PRODUCING 3,5-DIARIL-1,3,5-THIADIAZINANES
RU2010108948A (en) METHOD FOR PRODUCING 1,7-BIS [4 (5) -METHYL-1,3-THIAZOL-2-IL] -3,5-DITIA-1,7-DIAZAGEPTANES
RU2008132580A (en) METHOD FOR SELECTIVE PRODUCTION OF 6,7-DIHYDRO-1,3,5,7-BENZOTRITIAZONINE
RU2012144046A (en) METHOD FOR PRODUCING α, ω- {BIS [(PENTAN-2,4-DION-3-IL) METHYL SULFANIL]} - ALKANOV
RU2007104626A (en) METHOD FOR PRODUCING 5-ACETYLSALICYLOYL-1,3,5-DITIAZINAN
RU2007133954A (en) METHOD FOR PRODUCING 1- (5-BENZOYL-1,3-DITIAN-5-IL) -1-ETHANONE
RU2012147376A (en) METHOD FOR PRODUCING 3,3-DI (METHOXICARBONIL) -1,5-DITIACYCLOalkanes
RU2008152916A (en) METHOD FOR PRODUCING 4- (DIMETHYLAMINO) -2-BUTINYLalkanoates
RU2012141443A (en) METHOD FOR PRODUCING 5-METHOXICARBONIL-1,3-DITIAN, FUNGICIDAL ACTIVITY
RU2012145638A (en) METHOD FOR PRODUCING 3-Pyridinyl-1,5,3-Dithiazocinanes
RU2013152027A (en) METHOD FOR PRODUCING N, N, N-THREE [(Phenyl (Benzyl) Sulfanyl) Methyl] AMINES

Legal Events

Date Code Title Description
MM4A The patent is invalid due to non-payment of fees

Effective date: 20120812