RU2008118971A - Устройство для проведения химических реакций - Google Patents

Устройство для проведения химических реакций Download PDF

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RU2008118971A
RU2008118971A RU2008118971/12A RU2008118971A RU2008118971A RU 2008118971 A RU2008118971 A RU 2008118971A RU 2008118971/12 A RU2008118971/12 A RU 2008118971/12A RU 2008118971 A RU2008118971 A RU 2008118971A RU 2008118971 A RU2008118971 A RU 2008118971A
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installation according
reaction unit
housing
installation
reactor
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RU2008118971/12A
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RU2389541C2 (ru
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Ахим ФИШЕР (DE)
Ахим ФИШЕР
Харальд ХАЙНЦЕЛЬ (DE)
Харальд ХАЙНЦЕЛЬ
Кристоф ВЕКБЕККЕР (DE)
Кристоф ВЕКБЕККЕР
Клаус ХУТМАХЕР (DE)
Клаус ХУТМАХЕР
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Эвоник Дегусса ГмБх (DE)
Эвоник Дегусса Гмбх
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/248—Reactors comprising multiple separated flow channels
    • B01J19/249—Plate-type reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0278—Feeding reactive fluids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0449—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
    • B01J8/0453—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being superimposed one above the other
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0476—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more otherwise shaped beds
    • B01J8/048—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more otherwise shaped beds the beds being superimposed one above the other
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0476—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more otherwise shaped beds
    • B01J8/0484—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more otherwise shaped beds the beds being placed next to each other
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0492—Feeding reactive fluids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/065—Feeding reactive fluids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067—Heating or cooling the reactor
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/02—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols
    • C07C319/08—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols by replacement of hydroxy groups or etherified or esterified hydroxy groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B01J2208/00221—Plates; Jackets; Cylinders comprising baffles for guiding the flow of the heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00018—Construction aspects
    • B01J2219/0002—Plants assembled from modules joined together
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2461—Heat exchange aspects
    • B01J2219/2462—Heat exchange aspects the reactants being in indirect heat exchange with a non reacting heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2491—Other constructional details
    • B01J2219/2492—Assembling means
    • B01J2219/2496—Means for assembling modules together, e.g. casings, holders, fluidic connectors

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

1. Установка для проведения экзотермических химических реакций, состоящая из корпуса и блока проведения реакций, который посредством расположения основного фланцевого соединения в верхней трети корпуса выполнен с возможностью его полной или частичной замены. ! 2. Установка по п.1, отличающаяся тем, что блок проведения реакций размещен в кожухе реактора в подвешенном или стоячем (вертикальном) положении. ! 3. Установка по п.1, отличающаяся тем, что блок проведения реакций состоит из многих модулей, число n которых может достигать 10. ! 4. Установка по п.3, отличающаяся тем, что модули расположены рядом друг с другом или друг над другом. ! 5. Установка по п.1, отличающаяся тем, что блок проведения реакций устанавливается в корпус снизу или сверху. ! 6. Установка по п.1, отличающаяся тем, что камера реактора, выполненная в виде камеры нагнетания, заключает в себе охладительную камеру. ! 7. Установка по одному из пп.1-6, отличающаяся тем, что блок проведения реакций выполнен в форме установки из труб, пластин или одной или же нескольких решеток. ! 8. Установка по одному из пп.1-6, отличающаяся тем, что блок проведения реакций закреплен на крышке реактора в подвешенном положении. ! 9. Установка по п.7, отличающаяся тем, что блок проведения реакций закреплен на крышке реактора в подвешенном положении. ! 10. Установка по одному из пп.1-6, отличающаяся тем, что блок проведения реакций соединен с корпусом посредством воспринимающих нагрузку штуцерных вводов. ! 11. Установка по п.7, отличающаяся тем, что блок проведения реакций соединен с корпусом посредством воспринимающих нагрузку штуцерных вводов.

Claims (11)

1. Установка для проведения экзотермических химических реакций, состоящая из корпуса и блока проведения реакций, который посредством расположения основного фланцевого соединения в верхней трети корпуса выполнен с возможностью его полной или частичной замены.
2. Установка по п.1, отличающаяся тем, что блок проведения реакций размещен в кожухе реактора в подвешенном или стоячем (вертикальном) положении.
3. Установка по п.1, отличающаяся тем, что блок проведения реакций состоит из многих модулей, число n которых может достигать 10.
4. Установка по п.3, отличающаяся тем, что модули расположены рядом друг с другом или друг над другом.
5. Установка по п.1, отличающаяся тем, что блок проведения реакций устанавливается в корпус снизу или сверху.
6. Установка по п.1, отличающаяся тем, что камера реактора, выполненная в виде камеры нагнетания, заключает в себе охладительную камеру.
7. Установка по одному из пп.1-6, отличающаяся тем, что блок проведения реакций выполнен в форме установки из труб, пластин или одной или же нескольких решеток.
8. Установка по одному из пп.1-6, отличающаяся тем, что блок проведения реакций закреплен на крышке реактора в подвешенном положении.
9. Установка по п.7, отличающаяся тем, что блок проведения реакций закреплен на крышке реактора в подвешенном положении.
10. Установка по одному из пп.1-6, отличающаяся тем, что блок проведения реакций соединен с корпусом посредством воспринимающих нагрузку штуцерных вводов.
11. Установка по п.7, отличающаяся тем, что блок проведения реакций соединен с корпусом посредством воспринимающих нагрузку штуцерных вводов.
RU2008118971/12A 2005-10-15 2006-09-18 Устройство для проведения химических реакций RU2389541C2 (ru)

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DE102005049457.9 2005-10-15
DE102005049457A DE102005049457A1 (de) 2005-10-15 2005-10-15 Vorrichtung zur Durchführung chemischer Reaktionen

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RU2008118971A true RU2008118971A (ru) 2009-11-20
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US (1) US8057749B2 (ru)
EP (1) EP1933973A1 (ru)
JP (1) JP2009511257A (ru)
CN (1) CN101287544B (ru)
BR (1) BRPI0617418A2 (ru)
CA (1) CA2626004A1 (ru)
DE (1) DE102005049457A1 (ru)
RU (1) RU2389541C2 (ru)
WO (1) WO2007045531A1 (ru)

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US3914111A (en) * 1974-04-18 1975-10-21 Universal Oil Prod Co Alkylation reaction chamber
JPS5959242A (ja) * 1982-09-28 1984-04-05 Toyo Eng Corp 反応方法およびそのための反応器
DE3663652D1 (en) * 1985-03-05 1989-07-06 Ici Plc Steam reforming hydrocarbons
DE3532413A1 (de) * 1985-09-11 1987-03-12 Uhde Gmbh Vorrichtung zur erzeugung von synthesegas
EP0287765B1 (en) * 1987-02-26 1993-05-12 Ammonia Casale S.A. System to improve the efficiency of reactors for exothermic synthesis and more particularly for the reaction of ammonia
JPS63218244A (ja) * 1987-03-05 1988-09-12 Mitsubishi Heavy Ind Ltd メタノ−ル合成用多管式反応器
EP0386692A3 (en) * 1989-03-09 1991-01-09 Ammonia Casale S.A. System for modifying in situ reactors for the synthesis of ammonia
US5266281A (en) * 1989-09-16 1993-11-30 Xytel Technologies Partnership Catalytic reactor
US5362454A (en) * 1993-06-28 1994-11-08 The M. W. Kellogg Company High temperature heat exchanger
CN2273619Y (zh) * 1996-09-06 1998-02-04 东南大学 带有内衬并易于装卸的高压釜
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JP2001038195A (ja) * 1999-06-28 2001-02-13 Basf Ag 熱交換板を備えた反応器
EP1153653A1 (en) * 2000-05-11 2001-11-14 Methanol Casale S.A. Reactor for exothermic or endothermic heterogeneous reactions
EP1221339A1 (en) * 2001-01-05 2002-07-10 Methanol Casale S.A. Catalytic reactor with heat exchanger for exothermic and endothermic heterogeneous chemical reactions

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CA2626004A1 (en) 2007-04-26
JP2009511257A (ja) 2009-03-19
US20080253926A1 (en) 2008-10-16
WO2007045531A1 (de) 2007-04-26
CN101287544B (zh) 2012-10-10
DE102005049457A1 (de) 2007-05-16
BRPI0617418A2 (pt) 2012-04-17
CN101287544A (zh) 2008-10-15
US8057749B2 (en) 2011-11-15
EP1933973A1 (de) 2008-06-25
RU2389541C2 (ru) 2010-05-20

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Effective date: 20150919