RU2006126091A - METHOD FOR PRODUCING UNCLEANED PRODUCT - Google Patents

METHOD FOR PRODUCING UNCLEANED PRODUCT Download PDF

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RU2006126091A
RU2006126091A RU2006126091/04A RU2006126091A RU2006126091A RU 2006126091 A RU2006126091 A RU 2006126091A RU 2006126091/04 A RU2006126091/04 A RU 2006126091/04A RU 2006126091 A RU2006126091 A RU 2006126091A RU 2006126091 A RU2006126091 A RU 2006126091A
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crude product
crude
inorganic salt
total
content
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RU2006126091/04A
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Russian (ru)
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Томас Фэйрчайлд БРАУНСКОМБ (US)
Томас Фэйрчайлд Браунскомб
Скотт Ли ВЕЛЛИНГТОН (US)
Скотт Ли Веллингтон
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Шелл Интернэшнл Рисерч Маатсхаппий Б.В. (NL)
Шелл Интернэшнл Рисерч Маатсхаппий Б.В.
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Publication of RU2006126091A publication Critical patent/RU2006126091A/en

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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/78—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with alkali- or alkaline earth metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/02—Sulfur, selenium or tellurium; Compounds thereof
    • B01J27/04—Sulfides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/02—Sulfur, selenium or tellurium; Compounds thereof
    • B01J27/04—Sulfides
    • B01J27/043—Sulfides with iron group metals or platinum group metals
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/02—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
    • C10G45/04—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G49/00—Treatment of hydrocarbon oils, in the presence of hydrogen or hydrogen-generating compounds, not provided for in a single one of groups C10G45/02, C10G45/32, C10G45/44, C10G45/58 or C10G47/00
    • C10G49/02—Treatment of hydrocarbon oils, in the presence of hydrogen or hydrogen-generating compounds, not provided for in a single one of groups C10G45/02, C10G45/32, C10G45/44, C10G45/58 or C10G47/00 characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G65/00—Treatment of hydrocarbon oils by two or more hydrotreatment processes only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/04—Liquid carbonaceous fuels essentially based on blends of hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/107—Atmospheric residues having a boiling point of at least about 538 °C
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1074—Vacuum distillates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1096—Aromatics or polyaromatics
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/30—Physical properties of feedstocks or products
    • C10G2300/301—Boiling range
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/30—Physical properties of feedstocks or products
    • C10G2300/305—Octane number, e.g. motor octane number [MON], research octane number [RON]

Claims (18)

1. Способ получения неочищенного продукта, образующегося в процессе нефтедобычи, вводят в контакт неочищенное сырье с источником водорода в присутствии неорганического солевого катализатора с получением суммарного продукта, который включает в себя неочищенный продукт, который представляет собой жидкую смесь при 25°С и 0,101 МПа, причем неочищенное сырье имеет содержание остатка, по меньшей мере, 0,2 г остатка на 1 г неочищенного сырья; неорганический солевой катализатор содержит, по меньшей мере, две неорганические соли металла, неорганический солевой катализатор содержит на 1 г неорганического солевого катализатора от 0 до 0,1 г композиций, которые образуют стекла при температурах, по меньшей мере 350°С, и для неорганического солевого катализатора наблюдается точка перегиба при выделении газа в диапазоне температур, который определяется по методу Временного анализа продуктов (ВАП), где точка перегиба при выделении газа находится в диапазоне температур между а) температурой дифференциальной сканирующей калориметрии (ДСК), по меньшей мере, одной из двух неорганических солей металла, и b) температурой ДСК неорганического солевого катализатора; и1. The method of obtaining the crude product resulting from the oil production process is brought into contact with the crude feed with a hydrogen source in the presence of an inorganic salt catalyst to obtain a total product that includes the crude product, which is a liquid mixture at 25 ° C and 0.101 MPa, moreover, the crude feed has a residue content of at least 0.2 g of residue per 1 g of crude feed; an inorganic salt catalyst contains at least two inorganic metal salts, an inorganic salt catalyst contains from 0 to 0.1 g of compositions per 1 g of inorganic salt catalyst that form glass at temperatures of at least 350 ° C., and for inorganic salt of the catalyst, an inflection point is observed during gas evolution in the temperature range, which is determined by the method of Temporary Product Analysis (VAP), where the inflection point during gas evolution is in the temperature range between a) swarm differential scanning calorimetry (DSC), at least one of the two inorganic metal salts, and b) a DSC temperature of the inorganic salt catalyst; and регулируют условия контактирования, такие как температура, давление, поток сырья, поток суммарного продукта, время пребывания, поток источника водорода или их сочетания, таким образом, что неочищенный продукт имеет содержание остатка, выраженное в граммах остатка на 1 г неочищенного продукта, по большей мере, 30% от содержания остатка в неочищенном сырье, где содержание остатка определяется по методу ASTM D5307.regulate contact conditions, such as temperature, pressure, feed stream, total product stream, residence time, hydrogen source stream or a combination thereof, so that the crude product has a residue content, expressed in grams of residue per 1 g of crude product, at most , 30% of the residue content in the crude feed, where the residue content is determined according to ASTM D5307. 2. Способ по п.1, в котором, по меньшей мере, одна из двух неорганических солей металла имеет ДСК температуру выше 500°С.2. The method according to claim 1, in which at least one of the two inorganic metal salts has a DSC temperature above 500 ° C. 3. Способ по п.1 или 2, в котором ДСК температура неорганического солевого катализатора лежит в диапазоне между 250 и 450°С или 300-400°С.3. The method according to claim 1 or 2, in which the DSC temperature of the inorganic salt catalyst lies in the range between 250 and 450 ° C or 300-400 ° C. 4. Способ по любому из пп.1 и 2, в котором выделившийся газ содержит пары воды и/или диоксид углерода.4. The method according to any one of claims 1 and 2, in which the evolved gas contains water vapor and / or carbon dioxide. 5. Способ по любому из пп.1 и 2, в котором неорганический солевой катализатор включает, по меньшей мере, один карбонат щелочного металла, по меньшей мере, один карбонат щелочно-земельного металла, по меньшей мере, один гидроксид щелочного металла, по меньшей мере, один гидроксид щелочно-земельного металла, по меньшей мере, один гидрид щелочного металла, по меньшей мере, один гидрид щелочно-земельного металла, по меньшей мере, один сульфид одного или нескольких щелочных металлов, по меньшей мере, один сульфид одного или нескольких щелочно-земельных металлов, по меньшей мере, один амид одного или нескольких щелочных металлов, по меньшей мере, один амид одного или нескольких щелочно-земельных металлов или их смеси.5. The method according to any one of claims 1 and 2, in which the inorganic salt catalyst comprises at least one alkali metal carbonate, at least one alkaline earth metal carbonate, at least one alkali metal hydroxide, at least at least one alkaline earth metal hydroxide, at least one alkali metal hydride, at least one alkaline earth metal hydride, at least one sulfide of one or more alkali metals, at least one sulfide of one or more alkaline earths metals, at least one amide of one or more alkali metals, at least one amide of one or more alkaline earth metals, or mixtures thereof. 6. Способ по п.5, в котором по меньшей мере один щелочной металл представляет собой натрий, калий, рубидий, цезий или их смеси; и/или по меньшей мере один щелочно-земельный металл представляет собой кальций, магний или их смеси.6. The method according to claim 5, in which at least one alkali metal is sodium, potassium, rubidium, cesium, or mixtures thereof; and / or at least one alkaline earth metal is calcium, magnesium, or mixtures thereof. 7. Способ по любому из пп.1 и 2, в котором источник водорода включает в себя водород, легкие углеводороды, воду или их смесей.7. The method according to any one of claims 1 and 2, in which the hydrogen source includes hydrogen, light hydrocarbons, water, or mixtures thereof. 8. Способ по любому из пп.1 и 2, в котором контактирование неочищенного сырья с источником водорода в присутствии неорганического солевого катализатора происходит в зоне контактирования, при этом дополнительно подают водяной пар в зону контактирования, до или во время контактирования.8. The method according to any one of claims 1 and 2, in which the contacting of the crude feed with a hydrogen source in the presence of an inorganic salt catalyst occurs in the contacting zone, while additionally supplying steam to the contacting zone, before or during contacting. 9. Способ по п.8, в котором, по меньшей мере, часть суммарного продукта образуется в виде паров, причем конденсируют, по меньшей мере, часть паров при 25°С и 0,101 МПа, с образованием неочищенного продукта.9. The method of claim 8, in which at least part of the total product is formed in the form of vapors, and at least part of the vapor is condensed at 25 ° C and 0.101 MPa, with the formation of the crude product. 10. Способ по любому из пп.1 и 2, в котором условия контактирования регулируются таким образом, что в ходе контактирования на 1 г неочищенного сырья образуется, по большей мере, 0,2 г, по большей мере, 0,15 г, по большей мере, 0,1 г или, по большей мере, 0,05 грамма углеводородов, которые не конденсируются при 25°С и 0,101 МПа, что определяется с помощью материального баланса.10. The method according to any one of claims 1 and 2, in which the contact conditions are controlled in such a way that during contact per 1 g of crude feed, at least 0.2 g, at least 0.15 g, are formed, more than 0.1 g, or at least 0.05 grams of hydrocarbons that do not condense at 25 ° C and 0.101 MPa, which is determined using the material balance. 11. Способ по любому из пп.1 и 2, в котором неочищенное сырье имеет от 0,2 до 0,99 г или от 0,3 до 0,8 г остатка на 1 г неочищенного сырья.11. The method according to any one of claims 1 and 2, in which the crude feed has from 0.2 to 0.99 g or from 0.3 to 0.8 g of residue per 1 g of crude feed. 12. Способ по п.11, в котором неочищенный продукт имеет от 0,00001 до 0,03 г или от 0,0001 до 0,01 г кокса на 1 г неочищенного продукта.12. The method according to claim 11, in which the crude product has from 0.00001 to 0.03 g or from 0.0001 to 0.01 g of coke per 1 g of the crude product. 13. Способ по любому из пп.1 и 2, в котором неочищенное сырье имеет СКЧ, суммарное содержание Ni/V/Fe, суммарное содержание гетероатомов, выраженные в граммах Ni/V/Fe или граммах гетероатомов на 1 г сырья, и условия контактирования регулируются таким образом, что неочищенный продукт имеет СКЧ, суммарное содержание Ni/V/Fe и/или суммарное содержание гетероатомов, по большей мере, равное 90%, от величин СКЧ, суммарного содержания Ni/V/Fe и/или суммарного содержания гетероатомов в неочищенном сырье.13. The method according to any one of claims 1 and 2, in which the crude feed has an SKH, the total content of Ni / V / Fe, the total content of heteroatoms, expressed in grams of Ni / V / Fe or grams of heteroatoms per 1 g of raw material, and contact conditions are regulated in such a way that the crude product has a TAN, the total Ni / V / Fe content and / or the total heteroatom content is at least 90% of the TAN, the total Ni / V / Fe content and / or the total heteroatom content in unrefined raw materials. 14. Способ по любому из пп.1 и 2, в котором неочищенный продукт имеет на 1 г неочищенного продукта от 0,00001 до 0,2 г нафты, от 0,0001 до 0,9 г дистиллята, от 0,0001 до 0,99 г вакуумного газойля или их смесей.14. The method according to any one of claims 1 and 2, in which the crude product has 1 g of crude product from 0.00001 to 0.2 g of naphtha, from 0.0001 to 0.9 g of distillate, from 0.0001 to 0 99 g of vacuum gas oil or mixtures thereof. 15. Способ по любому из пп.1 и 2, который дополнительно включает смешение неочищенного продукта с сырьем, являющимся таким же или отличающимся от неочищенного сырья, с получением смеси.15. The method according to any one of claims 1 and 2, which further includes mixing the crude product with a raw material that is the same or different from the crude raw material, to obtain a mixture. 16. Способ по любому из пп.1 и 2, который дополнительно включает переработку неочищенного продукта или смеси с целью получения транспортного топлива, котельного топлива, смазочных средств или химикалий.16. The method according to any one of claims 1 and 2, which further includes processing the crude product or mixture in order to obtain transport fuel, boiler fuel, lubricants or chemicals. 17. Способ по п.16, в котором переработка включает в себя дистилляцию неочищенного продукта или смеси, чтобы получить одну или несколько дистиллятных фракций.17. The method according to clause 16, in which the processing includes distillation of the crude product or mixture to obtain one or more distillate fractions. 18. Способ по п.16, в котором переработка включает гидроочистку.18. The method according to clause 16, in which the processing includes hydrotreating.
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CA2549405C (en) 2013-07-23
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