RU2006126085A - METHOD FOR PRODUCING UNCLEANED PRODUCT - Google Patents

METHOD FOR PRODUCING UNCLEANED PRODUCT Download PDF

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RU2006126085A
RU2006126085A RU2006126085/04A RU2006126085A RU2006126085A RU 2006126085 A RU2006126085 A RU 2006126085A RU 2006126085/04 A RU2006126085/04 A RU 2006126085/04A RU 2006126085 A RU2006126085 A RU 2006126085A RU 2006126085 A RU2006126085 A RU 2006126085A
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Prior art keywords
crude
crude product
total
content
product
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RU2006126085/04A
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Russian (ru)
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Томас Фэйрчайлд БРАУНСКОМБ (US)
Томас Фэйрчайлд Браунскомб
Скотт Ли ВЕЛЛИНГТОН (US)
Скотт Ли Веллингтон
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Шелл Интернэшнл Рисерч Маатсхаппий Б.В. (NL)
Шелл Интернэшнл Рисерч Маатсхаппий Б.В.
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Publication of RU2006126085A publication Critical patent/RU2006126085A/en

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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/78—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with alkali- or alkaline earth metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/02—Sulfur, selenium or tellurium; Compounds thereof
    • B01J27/04—Sulfides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/02—Sulfur, selenium or tellurium; Compounds thereof
    • B01J27/04—Sulfides
    • B01J27/043—Sulfides with iron group metals or platinum group metals
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/02—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
    • C10G45/04—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G49/00—Treatment of hydrocarbon oils, in the presence of hydrogen or hydrogen-generating compounds, not provided for in a single one of groups C10G45/02, C10G45/32, C10G45/44, C10G45/58 or C10G47/00
    • C10G49/02—Treatment of hydrocarbon oils, in the presence of hydrogen or hydrogen-generating compounds, not provided for in a single one of groups C10G45/02, C10G45/32, C10G45/44, C10G45/58 or C10G47/00 characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G65/00—Treatment of hydrocarbon oils by two or more hydrotreatment processes only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/04—Liquid carbonaceous fuels essentially based on blends of hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/107—Atmospheric residues having a boiling point of at least about 538 °C
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1074—Vacuum distillates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1096—Aromatics or polyaromatics
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/30—Physical properties of feedstocks or products
    • C10G2300/301—Boiling range
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/30—Physical properties of feedstocks or products
    • C10G2300/305—Octane number, e.g. motor octane number [MON], research octane number [RON]

Claims (17)

1. Способ получения неочищенного продукта, в котором вводят в контакт неочищенное сырье с источником водорода в присутствии неорганического солевого катализатора, чтобы получить суммарный продукт, который включает неочищенный продукт, при этом неочищенный продукт представляет собой жидкую смесь при 25°С и 0,101 МПа, неочищенное сырье имеет содержание остатка, по меньшей мере, 0,2 г остатка на 1 г неочищенного сырья; неорганический солевой катализатор содержит одну или несколько солей щелочных металлов, одну или несколько солей щелочно-земельных металлов или их смеси, в котором одна из солей щелочного металла представляет собой карбонат щелочного металла, где щелочной металл имеет атомный номер, по меньшей мере, 11; и1. The method of obtaining the crude product, which is brought into contact with the crude feed with a hydrogen source in the presence of an inorganic salt catalyst to obtain a total product that includes the crude product, while the crude product is a liquid mixture at 25 ° C and 0.101 MPa, the crude the feed has a residue content of at least 0.2 g of residue per 1 g of crude feed; inorganic salt catalyst contains one or more alkali metal salts, one or more alkaline earth metal salts or mixtures thereof, in which one of the alkali metal salts is an alkali metal carbonate, where the alkali metal has an atomic number of at least 11; and регулируют условия контактирования: температуру, давление, скорость потока неочищенного сырья, потока суммарного продукта, время пребывания, скорость потока источника водорода или их сочетаний, чтобы получить суммарный продукт, который имеет содержание остатка, по большей мере, 30% от содержания остатка в неочищенном сырье, где содержание остатка определяется по методу ASTM D5307.the contact conditions are regulated: temperature, pressure, flow rate of the crude feed, total product flow, residence time, flow rate of a hydrogen source or combinations thereof to obtain a total product that has a residue content of at least 30% of the residue content of the crude feed where the residue content is determined according to ASTM D5307. 2. Способ по п.1, в котором, по меньшей мере, одна из солей щелочно-земельных металлов включает в себя карбонат и/или гидроксидные соли.2. The method according to claim 1, in which at least one of the salts of alkaline earth metals includes carbonate and / or hydroxide salts. 3. Способ по любому из пп.1 и 2, в котором щелочно-земельный металл, по меньшей мере, в одной из солей щелочно-земельных металлов представляет собой кальций и/или магний.3. The method according to any one of claims 1 and 2, in which the alkaline earth metal in at least one of the salts of alkaline earth metals is calcium and / or magnesium. 4. Способ по любому из пп.1 и 2, в котором щелочной металл, по меньшей мере, в одной из солей щелочных металлов представляет собой натрий, калий, рубидий, цезий или их смеси.4. The method according to any one of claims 1 and 2, in which the alkali metal in at least one of the salts of alkali metals is sodium, potassium, rubidium, cesium or a mixture thereof. 5. Способ по любому из пп.1 и 2, в котором источник водорода включает в себя водород, легкие углеводороды, воду или их смеси.5. The method according to any one of claims 1 and 2, in which the hydrogen source includes hydrogen, light hydrocarbons, water, or mixtures thereof. 6. Способ по любому из пп.1 и 2, в котором, по меньшей мере, часть суммарного продукта образуется в виде паров, причем, по меньшей мере, часть паров конденсируют при 25°С и 0,101 МПа с образованием неочищенного продукта.6. The method according to any one of claims 1 and 2, in which at least part of the total product is formed in the form of vapors, and at least part of the vapor is condensed at 25 ° C and 0.101 MPa with the formation of the crude product. 7. Способ по любому из пп.1 и 2, в котором контактирование неочищенного сырья с источником водорода в присутствии неорганического солевого катализатора происходит в зоне контактирования, водяной пар подают в зону контактирования до контактирования или во время контактирования.7. The method according to any one of claims 1 and 2, in which the contacting of the crude feed with a hydrogen source in the presence of an inorganic salt catalyst occurs in the contacting zone, water vapor is supplied to the contacting zone before contacting or during contacting. 8. Способ по любому из пп.1 и 2, в котором неочищенное сырье имеет от 0,2 до 0,99 г или от 0,3 до 0,8 г остатка на 1 г неочищенного сырья.8. The method according to any one of claims 1 and 2, in which the crude feed has from 0.2 to 0.99 g or from 0.3 to 0.8 g of residue per 1 g of crude feed. 9. Способ по любому из пп.1 и 2, в котором условия контактирования также регулируют таким образом, что в ходе контактирования на 1 г неочищенного сырья образуется, по большей мере, 0,2 г, по большей мере, 0,15 г, по большей мере, 0,1 г или, по большей мере, 0,05 г углеводородов, которые не конденсируются при 25°С и 0,101 МПа, что определяется с помощью материального баланса.9. The method according to any one of claims 1 and 2, in which the contact conditions are also controlled in such a way that during contact per 1 g of crude feed, at least 0.2 g, at least 0.15 g are formed, at most 0.1 g or at least 0.05 g of hydrocarbons that do not condense at 25 ° C and 0.101 MPa, which is determined using the material balance. 10. Способ по любому из пп.1 и 2, в котором неочищенный продукт имеет от 0,00001 до 0,03 г или от 0,0001 до 0,01 г кокса на 1 г неочищенного продукта.10. The method according to any one of claims 1 and 2, in which the crude product has from 0.00001 to 0.03 g or from 0.0001 to 0.01 g of coke per 1 g of crude product. 11. Способ по любому из пп.1 и 2, в котором неочищенное сырье также имеет суммарное кислотное число (СКЧ), суммарное содержание Ni/V/Fe, суммарное содержание гетероатомов, выраженные в граммах Ni/V/Fe или в граммах гетероатомов на 1 г сырья, и условия контактирования регулируются таким образом, что неочищенный продукт имеет СКЧ, суммарное содержание Ni/V/Fe и/или суммарное содержание гетероатомов, по большей мере, 90%, от величин СКЧ, суммарного содержания Ni/V/Fe и/или суммарного содержания гетероатомов в неочищенном сырье.11. The method according to any one of claims 1 and 2, in which the crude feed also has a total acid number (SKH), a total content of Ni / V / Fe, a total content of heteroatoms, expressed in grams of Ni / V / Fe or in grams of heteroatoms per 1 g of raw material, and the contacting conditions are regulated so that the crude product has an RMS, the total Ni / V / Fe content and / or the total heteroatom content is at least 90% of the RMS, the total Ni / V / Fe content and / or the total content of heteroatoms in the crude feed. 12. Способ по любому из пп.1 и 2, в котором неочищенный продукт также имеет на 1 грамм неочищенного продукта от 0,00001 до 0,2 г нафты, от 0,0001 до 0,9 г дистиллята, от 0,0001 до 0,99 г вакуумного газойля или их смесей.12. The method according to any one of claims 1 and 2, in which the crude product also has 1 gram of crude product from 0.00001 to 0.2 g of naphtha, from 0.0001 to 0.9 g of distillate, from 0.0001 to 0.99 g of vacuum gas oil or mixtures thereof. 13. Способ по любому из пп.1 и 2, в котором неочищенный продукт имеет от 0,000001 до 0,1 г, от 0,00001 до 0,05 г, от 0,001 до 0,03 г или от 0,005 до 0,04 г остатка на 1 г неочищенного продукта.13. The method according to any one of claims 1 and 2, in which the crude product has from 0.000001 to 0.1 g, from 0.00001 to 0.05 g, from 0.001 to 0.03 g, or from 0.005 to 0, 04 g of residue per 1 g of crude product. 14. Способ по любому из пп.1 и 2, в котором смешивают неочищенный продукт с сырьем, являющимся таким же или отличающимся от неочищенного сырья, чтобы получить смесь.14. The method according to any one of claims 1 and 2, in which the crude product is mixed with a raw material that is the same or different from the crude raw material to obtain a mixture. 15. Способ по любому из пп.1 и 2, который обеспечивает получение транспортного топлива, котельного топлива, смазочных средств или химикалий.15. The method according to any one of claims 1 and 2, which provides for the production of transport fuel, boiler fuel, lubricants or chemicals. 16. Способ по п.15, в котором переработка представляет собой дистилляцию неочищенного продукта или смеси, чтобы получить одну или несколько дистиллятных фракций.16. The method according to clause 15, in which the processing is the distillation of the crude product or mixture to obtain one or more distillate fractions. 17. Способ по п.16, в котором переработка включает гидроочистку.17. The method according to clause 16, in which the processing includes hydrotreating.
RU2006126085/04A 2003-12-19 2004-12-16 METHOD FOR PRODUCING UNCLEANED PRODUCT RU2006126085A (en)

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US53150603P 2003-12-19 2003-12-19
US60/531,506 2003-12-19
US61879904P 2004-10-14 2004-10-14
US60/618,799 2004-10-14

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RU2006126088/04A RU2006126088A (en) 2003-12-19 2004-12-16 METHOD FOR PRODUCING UNCLEANED PRODUCT
RU2006126085/04A RU2006126085A (en) 2003-12-19 2004-12-16 METHOD FOR PRODUCING UNCLEANED PRODUCT
RU2006126086/15A RU2379331C2 (en) 2003-12-19 2004-12-16 Non-refined product and gas with hydrogen content production methods
RU2006126084/04A RU2372381C2 (en) 2003-12-19 2004-12-16 Methods of producing crude product
RU2006126089/04A RU2006126089A (en) 2003-12-19 2004-12-16 METHODS FOR PRODUCING UNCLEANED PRODUCT AND UNCLEANED PRODUCT

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RU2006126084/04A RU2372381C2 (en) 2003-12-19 2004-12-16 Methods of producing crude product
RU2006126089/04A RU2006126089A (en) 2003-12-19 2004-12-16 METHODS FOR PRODUCING UNCLEANED PRODUCT AND UNCLEANED PRODUCT

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