PL7306B1 - A method of quantitative oxygen evolution from aqueous salt solutions for disinfection, bleaching and washing. - Google Patents

A method of quantitative oxygen evolution from aqueous salt solutions for disinfection, bleaching and washing. Download PDF

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Publication number
PL7306B1
PL7306B1 PL7306A PL730626A PL7306B1 PL 7306 B1 PL7306 B1 PL 7306B1 PL 7306 A PL7306 A PL 7306A PL 730626 A PL730626 A PL 730626A PL 7306 B1 PL7306 B1 PL 7306B1
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PL
Poland
Prior art keywords
oxygen
bleaching
washing
salt solutions
aqueous salt
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Application number
PL7306A
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Polish (pl)
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Publication date
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Publication of PL7306B1 publication Critical patent/PL7306B1/en

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Pranie proszkami, zawierajacemi wyso¬ ko - utlenione sole, z których wydziela sie tlen, jest bardzo rozpowszechnione, ponie¬ waz tlen in statu nascendi bieli i dezynfe¬ kuje bielizne.Stosowanie proszków mydlanych, za¬ wierajacych wysoko - utlenione sole, ma jednak duze wady.Proszki te po wiekszej czesci traca przy dluzszem lezeniu duza czesc zawartego w nich tlenu (w przeciagu 3 — 4-ch miesiecy do 50%).Dla zwolnienia, przynajmniej znacznej czesci tlenu dla procesu bielenia, nalezy je gotowac przez dluzszy czas, co znów jest szkodliwe dla wszelkiego rodzaju bielizny, a w kazdym razie sposób ten nie moze "byc stosowany do tkanin, które nie powinny byc traktowane na goraco.Trwale, t. j. specjalnie uodpornione proszki, nawet przy dluzszem gotowaniu nie wydzielaja calkowitej ilosci tlenu i w 50% zostaja wylane w stanie nierozlozo- nym.Przy gotowaniu wydzielenie tlenu jest ograniczone krótkim czasem, poniewaz przy dluzszem gotowaniu bielizna niszczy sie; z drugiej strony znaczna ilosc tlenu zostaje porwana para wodna i wogóle nie dziala.Nasuwala sie przeto potrzeba zbadania, czy przez stosowanie katalizatorów (po¬ równaj Bernthsen'a Kurzes Lehrbuch der organischen Chemie, wydanie 16 str. 39 i 40), nie jest mozliwe ilosciowe uwalnianie tlenu przy dowolnej temperaturze.Ponizej zostaje przytoczonych kilka doswiadczen: 1. Przy pokojowej temperaturze belkatalizatora. 0,1% -owy roztwór nadboranu (fabrykat Coswig'a) tracil w przeciagu 18 godz 10% tlenu. 1%-owy roztwór proszku mydlanego z 30%-owa zawartoscia tluszczu i 10-owa zawartoscia nadboranu tracil przy pozo¬ stawieniu w przeciagu 18 godz 8 ^— 10% tlenu. 2. Przy pokojowej temperaturze z ka¬ talizatorem. Roztwór wodny, zawierajacy 0,1% nadboranu i jako katalizator 0,008% siarczanu mangano - potasowego, albo 0,003% mleczanu manganowego traci w 2 godz 100% tlenu.Roztwór, zawierajacy 0,1% nadboranu i 0,25% bezwodnej sody i jako katalizator 0,008% siarczanu mangano - potasowego albo 0,003% mleczanu manganowego, tra¬ cil w 3 godz 100% tlenu.Roztwór, zawierajacy 1% prosizku my¬ dlanego w powyzszym skladzie i jako ka¬ talizator 0,008% siarczanu mangano - po¬ tasowego, albo 0,003% laktamu mangano¬ wego^ tracil po 18 godz 100% tlenu.Ten sam roztwór proszku mydlanego tracil przy dodaniu 20 cm3 tyrosynozy (20 cm8 wytloczyn z 500 g dbierek karto¬ flanych, dezynfekowane 2% chloroformu) w 18 godz 100%. 3. Po gotowaniu przez XU godz bez katalizatora, 0,1 %-owy roztwór nadboranu tracil 60%, 1%-owy roztwór proszku tracil 30 — 50%. 4. Po gotowaniu przez V* godz z kata¬ lizatorem. Roztwór, zawierajacy 0,1% nad¬ boranu i 0,0002% siarczanu mangano - po¬ tasowego, albo 0,00008% mleczanu manga¬ nowego, tracil 100%, Roztwór, zawierajacy 1% proszku my¬ dlanego w powyzszym skladzie, zawiera¬ jacy jako katalizator 0,0002% siarczanu mangano - potasowego, albo 0,00008% lak- tanu manganowego, tracil 100%.Powyzsze przyklady dowodza, ze uzy¬ cie katalizatorów przy bieleniu i praniu srodkami, zawieraj acemi tlen, umozliwia ilosciowa wydajnosc tlenu przy dowolnej temperaturze, bez gotowania, co nalezy uwazac za wielki postep w stosunku do do¬ tychczasowych metod prania i bielenia. PL PLWashing with powders containing highly oxidized salts from which oxygen is released is very widespread because oxygen in the state of nascent whiteness and disinfects the linen. The use of soap powders containing highly oxidized salts, however, has a lot of effect. These powders lose a large part of the oxygen contained in them over a longer period of time (up to 50% within 3 - 4 months). In order to release at least a significant part of the oxygen for the bleaching process, boil them for a longer time, which Again, it is harmful to all kinds of linen, and in any case this method cannot be applied to fabrics that should not be treated hot. Permanently, i.e. specially resistant powders, even when boiled for a long time do not give off the total amount of oxygen and 50% are poured out When cooking, the release of oxygen is limited by a short time, because the linen is destroyed with longer cooking; on the other hand, a significant amount of oxygen the water vapor is entrained and it does not work at all, so there was a need to investigate whether by the use of catalysts (see Bernthsen Kurzes Lehrbuch der organischen Chemie, 16th edition, pp. 39 and 40), quantitative oxygen release at any temperature is not possible Several experiments are cited below: 1. At room temperature of the catalyst. 0.1% perborate solution (manufactured by Coswig) lost 10% oxygen within 18 hours. A 1% fat solution of soap powder with 30% fat and 10% perborate lost 8-10% oxygen when left standing for 18 hours. 2. At room temperature with catalyst. An aqueous solution containing 0.1% perborate and as a catalyst 0.008% manganese - potassium sulphate or 0.003% manganese lactate loses 100% oxygen in 2 hours Solution containing 0.1% perborate and 0.25% anhydrous soda and as a catalyst 0.008% potassium manganese sulfate or 0.003% manganese lactate, consumed in 3 hours with 100% oxygen. A solution containing 1% soap powder in the above composition and as a catalyst 0.008% potassium manganese sulfate, or 0.003 The% manganese lactam lost 100% oxygen after 18 hours. The same soap powder solution lost 100% with the addition of 20 cm3 of tyrosinose (20 cm3 of pulp from 500 g of carton paper, disinfected with 2% chloroform) in 18 hours. 3. After boiling for XU hours without catalyst, 0.1% tracil perborate solution 60%, 1% tracil powder solution 30 - 50%. 4. After boiling for V * hours with the catalyst. A solution containing 0.1% perborate and 0.0002% manganese potassium sulphate or 0.00008% manganese lactate lost 100%. A solution containing 1% soap powder in the above composition contains As a catalyst, 0.0002% manganese-potassium sulphate, or 0.00008% manganese lactate, lost 100%. The above examples show that the use of catalysts in bleaching and washing with agents containing oxygen, allows quantitative oxygen yield at any temperature, without boiling, which is considered a great advance in relation to the conventional methods of washing and bleaching. PL PL

Claims (1)

1. Zastrzezenie patentowe. Sposób ilosciowego wydzielania tlenu z wodnych roztworów soli o duzej zawartosci tlenu, albo ich mieszanin z innemi solami, znamienny tern, ze dodaje sie katalizatory w takiej ilosci, iz tlen z odpowiednia do reakcji szybkoscia do celów bielenia przy pozadanej temperaturze wydziela sie ilo¬ sciowo. Dr. 'Jerzy L es z i k. Zastepca: M. Brokman, rzecznik patentowy. Druk L. Boguslawskiego, Wars7awi. PL PL1. Patent claim. A method for the quantitative evolution of oxygen from aqueous salt solutions with high oxygen content, or mixtures thereof with other salts, characterized by adding the amount of catalysts that the oxygen is quantitatively released at a reaction rate suitable for the bleaching at the desired temperature. Dr. Jerzy L es with and near Zastepca: M. Brokman, patent attorney. Printed by L. Boguslawski, Wars7awi. PL PL
PL7306A 1926-07-16 A method of quantitative oxygen evolution from aqueous salt solutions for disinfection, bleaching and washing. PL7306B1 (en)

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PL7306B1 true PL7306B1 (en) 1927-05-31

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