PL3308B1 - A method of processing lug containing salmic acid in iron apparatuses. - Google Patents

A method of processing lug containing salmic acid in iron apparatuses. Download PDF

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Publication number
PL3308B1
PL3308B1 PL3308A PL330823A PL3308B1 PL 3308 B1 PL3308 B1 PL 3308B1 PL 3308 A PL3308 A PL 3308A PL 330823 A PL330823 A PL 330823A PL 3308 B1 PL3308 B1 PL 3308B1
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PL
Poland
Prior art keywords
iron
salmic
apparatuses
acid
processing
Prior art date
Application number
PL3308A
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Polish (pl)
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Publication date
Application filed filed Critical
Publication of PL3308B1 publication Critical patent/PL3308B1/en

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Wyrób salhnjaiku z chlorku sodowego i atmomijaiku z równoczeistneni uzyskiWaimleim kMcynowalnej sody jest znanym procesem o wielkiem znaJozeniiu gospodkrczem. Przy tej fabrykalcji otrzymuje sie naprzód lug, który zawiera okolo 15% salmjaku i 8% soli kuchennej obok nieznacznych ilosci zwiiazków silajrki, dwuweglanów sodu i a- monu. Jezeli parowanie i dalsza przerób¬ ka] tych lugów odbywa sie w zelaznych a- pairatach, to pociagaj to za soba te nastep¬ stwa), ze luigi w czasie ogjrzeiwatoiila srozpu- sizczaja tyle zelaza, wchodzajcego w sklad alparatów, ze nieiylfco same alparaty ulegar ja stopniowo zniszczeniu, lecz takze otrzy¬ mane produkty koncowe, sól kuchenna i saLmjak, sa zanieczyszczone tak, ze staja sile bezuzyteczne.Wskutek tego zelazne aiparaity okazaly sie nlieistosowne, wtiec zaczeto uzywac do pairowialnilaj lugów zawieraljajcych salmjak aparatów kamiennych, emal jowialnych i t. p., które sa jednak nieekonomiczne dla wielkiej produkcji przemyslu aMotawo-na- wozowego.Wedlug sposobu Cuimberlanda znana jest ochrona kotlów patowych i skrapla- czów przed nagryzaniem przez wlaczanie chronionych powierzchni) zelaiznych w ko¬ lo pradu jako biegunów ujemnych. Jako biegunów dodalmibh uzywa sie równiez e- lektrod zeilalznych posiajdlajacych duza trwa¬ losc. Przewodnikiem pradu jest woda zaL warta w danym kotle. Sposób ten próbo- walnio zastosowac takze do takich dieczy chemicznych, które nagjryzlaija metaliczne1 zelazo ii wskutek tego nie moga byc goto- wiaine w zelaznych aparatach. W kazdym nalzriie dtodalttail prad musi tu byc wprowa¬ dzony zlapoimoca tak zwataej uiierozpusizczail- nej elektrody, bo uzycie zelaznej alnjody, tak jak w sposobie Cumberlaindal, nile jest tu wlskaizamie z ptoWodu jej chemicznej rozpu- szczalnloiscil i zajniieczyszteanfai cieczy. W piletrwsizym wymileniionym wypadku przera- biianiia roztiworów, które skladaja sie glów- niJe z siailinjaktii i soli kuchennej, nilerozpu- szdzatlina aiuod^J nfe da sie uzyc z tego zno- ^ # ,, ^ wiu powiódu, ze musiblby nai rufej powfctawae ^ cfrior, Idióirylby^wkDir^^ z siailmjakiem chlo¬ rek "ajzotto.Zgfalsiziaijacy odkryli nfeispodzilalnfe, ze moznial osiagnac cel uzywajac rozpu- szfczailmej anody zelaznej, zaipomoca której doprowadza! sile db lugu slaby prad staly uchodzacy potem przez zelalzne sciany a- paratów, jakkolwiek zelazo — jako metal anody — przechodni wtiedy w roztwór j al¬ ko chlorek zelaza w ilosci odpowiadaj apej w najkorzystniejszym raizie równowaizniko- wil przesylanego pradu. Z wyparowanych w ten sposób lugów krystalfeuje sajlmjak zabierajacy 98^-99% NH4 Cl, który moz¬ na zatem uznac za technicznie czysty. Lugi pokrystalilzacyjale miesza sie z nowemal ilo¬ sciami lugów koncowych z fabryki sody a^ morgowej, poczesn wracaja one ztoowtu do wypamika, wiec wyparowuje sie je niej ar ko do suchego. Wbrew wszelkiemu ocze¬ kiwaniu rozrtwór nie zateiieczy^zcza sie ze¬ lazem atmodowem. Nalwet w czasie nieprzer- waWej pracy przez cale tygodnie krystali¬ zuje z&wsfce saiknjak o 98—99% NHJJl i na¬ gryzanie scian zelaznego naczynia stykaja¬ cego sie z lugamii nie ujawnia sie nawet przy uiyciki zwyklego zelaiza kujnego.Po dluzszym czasie zbieraja sile copraiw- daj zwiazki silarfoowe, pochodzace z proce¬ su sddowego i) obecnie glównie w postaci polirtijoniianów, które jedtoak nie Wplywaja riiiekoirzystlnile na niniejszy sposób, lecz o ile wfcbogaica sie zbyt silnie, to nallezy pelw- na czesc lugów mafcilerizystych wylaczyc z opisanego cyklu kolloiwiegjo.Niewielka ilosc zelazn w| postaci chlor¬ ku znajduje sile w czaisie pracy nMejiSizym sposobem w stalym obiegu wraz z lugami.Jego stracenie jako wodorotlenku zelaza. nie odbywa .sie nawet w razie nieuniknione¬ go wtargniecia powiletrzal db urzadzen kry- stailiizafcyjnych.Prad elektryczny uchodzacy z po¬ wierzchni) zelateniej aparatu, statoowilacej katode i posiadajacy natezenie 0.1 A na dfcrni2, wystarcza- najzupelniej dbosiagniecia ochrony sciialn naczynia przed lugami za- wfiieraljacemil salmjak ii majacemi! wlasnosc rozpuszczania zelaza, PLThe production of salhnjaik from sodium chloride and atmomijaik with the simultaneous recovery of Waimleim kMinovable soda is a well-known process of great importance. With this fabrication, the first slug is obtained, which contains about 15% salmic acid and 8% table salt, along with small amounts of silica compounds, sodium bicarbonate and ammonium. If the steaming and further processing of these lugs takes place in iron a-pairs, then these consequences attract them), that the lures, during the heating process, break down so much iron, which is part of the alparatus, that the alparatus themselves succumb it is gradually deteriorated, but also the resulting end products, table salt and salmon, are contaminated to such a point that they become useless forces. Consequently, the iron aiparaites turned out to be irrelevant, so they began to use pairs of balms containing salmies, stone apparatuses, and steam which, however, are uneconomical for the large production of the motor-fertilizer industry. According to the Cuimberland method, it is known to protect stalemate boilers and condensers from being bitten by turning the protected surfaces of irons in the current circle as negative poles. Strength electrodes with long durability are also used as dodalmibh poles. The conductor of the current is the water in the boiler. This method has also been tried to be applied to such chemical diets that nebulize metallic iron and consequently cannot be prepared in iron appliances. In every dtodalttail, the current must be introduced here to the catch of the so-called non-resistive electrode, because the use of an iron alniode, as in the Cumberlaindal method, is not here to be drawn from the water of its chemical dissolving and dissolving liquid. In the most exhilarating case of the processing of solutions, which consist mainly of siailinjaktia and table salt, nileroz-slatlina aiuod ^ J It can be used from this arduous reason that it would have to be , Idióirylby ^ wkDir ^^ with siailmjak chloess "ajzotto. Zgfalsiziaijacy discovered a nfeispodalnfe, that it was possible to achieve the goal by using a dissolving iron anode, helping to bring the strength of the debt to a weak sweat, such as a steady flow of electricity, - as the metal of the anode - then transferable to the solution, it is iron chloride in the amount corresponding to the most advantageous equivalents of the transmitted current. The liquor which evaporates in this way crystallizes to take 98-99% of NH4 Cl, which can therefore be to be considered technically clean. I eat it dry. Contrary to all expectations, the solution will not become stained with atmodium iron. Even during uninterrupted work for weeks, the saiknjak crystallizes with 98-99% NHJJl and the biting of the walls of the iron vessel in contact with the lugs does not reveal itself even with the use of ordinary iron iron copra. - they give silarfoic compounds, derived from the judicial process, and) now mainly in the form of polyrionionates, which, however, do not have an adverse effect on this method, but if it is too strong in this way, it will form part of the mafilic bonds of the above-described cycle A small amount of iron in | Chloride form finds strength in constant circulation with the liquors in constant circulation with the lyes. Its loss as iron hydroxide. does not take place, even in the event of an unavoidable intrusion, has plugged the crystalline and flaccid devices. Electric current escaping from the surface of the apparatus, a static cathode and having an intensity of 0.1 A at dfcrni2, it is sufficient to protect the vessel wall against ligaments wfiieraljacemil salmjak ii majacemi! iron dissolving property, PL

Claims (1)

1. Zastrzezenie patentowe. Sposób przerabiania lugów, zawieraja¬ cych salmjak,, w zelaznych ajpajrafetich, zna¬ mienny tern, ze ziapomoca zelajzJnej anody doprowadza sie dlo lugów slaby prad sialy, który uchodzi przez zelalzne sciany apa¬ ratów. Henkel & Cie. Walter Weber. Zastepca: M. Kryzan, rzecznik patentowy. Druk L. Boguslawskiego, Warszawa PL1. Patent claim. The method of processing the lures, which contain salmia in iron ajpayrafeti, is characterized by a significant area, that by means of a cast iron anode, a weak current is supplied to the lengths of the lures, which flows through the iron walls of the installments. Henkel & Cie. Walter Weber. Deputy: M. Kryzan, patent attorney. Print by L. Boguslawski, Warsaw PL
PL3308A 1923-02-19 A method of processing lug containing salmic acid in iron apparatuses. PL3308B1 (en)

Publications (1)

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PL3308B1 true PL3308B1 (en) 1925-12-31

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