PL42952B3 - - Google Patents
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- Publication number
- PL42952B3 PL42952B3 PL42952A PL4295258A PL42952B3 PL 42952 B3 PL42952 B3 PL 42952B3 PL 42952 A PL42952 A PL 42952A PL 4295258 A PL4295258 A PL 4295258A PL 42952 B3 PL42952 B3 PL 42952B3
- Authority
- PL
- Poland
- Prior art keywords
- germanium
- gallium
- dust
- thorium
- uranium
- Prior art date
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- 229910052732 germanium Inorganic materials 0.000 claims description 9
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 claims description 9
- GYHNNYVSQQEPJS-UHFFFAOYSA-N Gallium Chemical compound [Ga] GYHNNYVSQQEPJS-UHFFFAOYSA-N 0.000 claims description 8
- 229910052733 gallium Inorganic materials 0.000 claims description 8
- 239000000428 dust Substances 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 4
- ZSLUVFAKFWKJRC-IGMARMGPSA-N 232Th Chemical compound [232Th] ZSLUVFAKFWKJRC-IGMARMGPSA-N 0.000 claims description 2
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 2
- 229910052776 Thorium Inorganic materials 0.000 claims description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 2
- 229910052770 Uranium Inorganic materials 0.000 claims description 2
- 229910017052 cobalt Inorganic materials 0.000 claims description 2
- 239000010941 cobalt Substances 0.000 claims description 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 2
- 229910052750 molybdenum Inorganic materials 0.000 claims description 2
- 239000011733 molybdenum Substances 0.000 claims description 2
- 229910052718 tin Inorganic materials 0.000 claims description 2
- 229910052719 titanium Inorganic materials 0.000 claims description 2
- 239000010936 titanium Substances 0.000 claims description 2
- JFALSRSLKYAFGM-UHFFFAOYSA-N uranium(0) Chemical compound [U] JFALSRSLKYAFGM-UHFFFAOYSA-N 0.000 claims description 2
- 229910052720 vanadium Inorganic materials 0.000 claims description 2
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims 1
- 239000003245 coal Substances 0.000 claims 1
- 229910052759 nickel Inorganic materials 0.000 claims 1
- 239000003208 petroleum Substances 0.000 claims 1
- 239000011135 tin Substances 0.000 claims 1
- 229910052725 zinc Inorganic materials 0.000 claims 1
- 239000011701 zinc Substances 0.000 claims 1
- 238000000859 sublimation Methods 0.000 description 2
- 230000008022 sublimation Effects 0.000 description 2
- 241000586605 Parlatoria proteus Species 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 239000010883 coal ash Substances 0.000 description 1
- 239000010779 crude oil Substances 0.000 description 1
- -1 gorman Chemical compound 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
Description
Opublikowano dnia 10 lulogo 1960 r» VAT£V ,. w-i^ 4 POLSKIEJ RZECZYPOSPOLITEJ LUDOWEJ OPIS PATENTOWY EllBLI«9TBK.SB- Nr 42952 Zaklady Cynkowe „Trzebinia"*) Trzebinia, Polska KI. 40 a, 44/54 i/n Sposób wzbogacania popiolu wagla lub ropy naftowej w pierwiastki rzadki*, |ak gal, gorman, tytan, wanad, molibden, uran, tor oraz cyno, kobalt I ntklol Patent dodatkowy do patentu Nr 42074 Patent trwa od dnia 8 grudnia 1958 r.Pyl wzbogacony w german i gal wedlug pa¬ tentu glównego Nr 42074 zawiera german i gal w postaci wolnych tlenków o niskim stopniu utlenienia jako Geo oraz GasO.Sposób wedlug wynalazku daje mozliwosc dalszego wzbogacenia germanu i galu droga su* blimacji w atmosferze obojetnej lub lekko re¬ dukcyjnej przy podwyzszeniu temperatury po¬ wyzej 700° C.Próby w skali laboratoryjnej przeprowadzono w retorcie zamknietej umieszczonej w piecu.Gaz ochronny jak CO*, CO* zawierajace CO, Ar, He itd. przechodzi przez retorte gdzie umiesz¬ czony zostal pyl germanu i galonosny otrzyma¬ ny ze zbogacenia wedlug patentu glównego.Uchodzacy z retorty gaz przechodzi przez sze¬ reg odbieralników oraz pompe ssaco-tloczaca.Próby przeprowadzone w temperaturze powyzej 700° C wykazaly, ze mozliwe jest wtórne osubli- twórca motanie germanu i galu w postaci GeO i GatO z uzyskiem okolo 9Q*/o.To wtórne wzbogacenie przez sublimacje mo¬ ze dac nawet 40-to krotne wzbogacenie germa¬ nu i galu w pyle wtórnym uchodzacym z retort w stosunku do stezen w pyle pierwotnym. PLPublished on July 10, 1960 »VAT £ V,. wi ^ 4 POLISH PEOPLE'S REPUBLIC PATENT DESCRIPTION OF EllBLI «9TBK.SB- No. 42952 Zaklady Zynkowe" Trzebinia "*) Trzebinia, Poland KI. 40 a, 44/54 i / n Method of enriching coal ash or crude oil with rare elements *, | ak gallium, gorman, titanium, vanadium, molybdenum, uranium, thorium and tin, cobalt and ntclol Patent additional to patent No. 42074 Patent valid since December 8, 1958 Dust enriched in germanium and gallium according to the main patent No. 42074 contains germanium and gallium in the form of free oxides of low oxidation state as Geo and GasO. The method according to the invention gives the possibility of further enrichment of germanium and gallium by means of sublimation in an inert or slightly reducing atmosphere with an increase in temperature above 700 ° C. Scale tests The laboratory was carried out in a closed retort placed in a furnace. Protective gas such as CO *, CO * containing CO, Ar, He etc. passes through the retort where the germanium dust and gallon dust obtained from the enrichment according to the main patent were placed. retorts, the gas passes through a series of receivers and a suction pump. Tests carried out at temperatures above 700 ° C have shown that it is possible to re-sublimate germanium and gallium in the form of GeO and GatO with a yield of about 9Q * / o. enrichment by sublimation can give even a 40-fold enrichment of germanium and gallium in the secondary dust escaping from the retorts in relation to the concentrations in the primary dust. PL
Claims (1)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL42952B3 true PL42952B3 (en) | 1960-02-15 |
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