PL399597A1 - Process for the preparation of monocalcium phosphate feed - Google Patents

Process for the preparation of monocalcium phosphate feed

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Publication number
PL399597A1
PL399597A1 PL399597A PL39959712A PL399597A1 PL 399597 A1 PL399597 A1 PL 399597A1 PL 399597 A PL399597 A PL 399597A PL 39959712 A PL39959712 A PL 39959712A PL 399597 A1 PL399597 A1 PL 399597A1
Authority
PL
Poland
Prior art keywords
monocalcium phosphate
reaction
phosphoric acid
ashes
preparation
Prior art date
Application number
PL399597A
Other languages
Polish (pl)
Other versions
PL222555B1 (en
Inventor
Zygmunt Kowalski
Zbigniew Wzorek
Kinga Krupa-Żuczek
Original Assignee
Politechnika Krakowska Im. Tadeusza Kosciuszki
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Politechnika Krakowska Im. Tadeusza Kosciuszki filed Critical Politechnika Krakowska Im. Tadeusza Kosciuszki
Priority to PL399597A priority Critical patent/PL222555B1/en
Publication of PL399597A1 publication Critical patent/PL399597A1/en
Publication of PL222555B1 publication Critical patent/PL222555B1/en

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  • Materials For Medical Uses (AREA)
  • Compositions Of Oxide Ceramics (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

Sposób wytwarzania fosforanu paszowego jednowapniowego polega na tym, że popioły z odpadów mięsno-kostnych, kalcynowanych w atmosferze utleniającej w temperaturze 600-1100°C, miesza się z wysuszonym fosforanem jednowapniowym będącym produktem reakcji popiołu z kwasem fosforowym, przy stosunku wagowym popiołu do fosforanu jednowapniowego od 1:1 do 1:5. Do tej mieszaniny dozuje się, ciągle mieszając, kwas fosforowy o stężeniu korzystnie 65-75%, w ilości stechiometrycznej wynikającej z reakcji hydroksyapatytu i kwasu fosforowego oraz prowadzi w tych warunkach reakcję przez 30 do 60 min.. Następnie zawierającą fosforan jednowapniowy poreakcyjną mieszaninę suszy się w temperaturze 105-120°C w ciągu 1-3 h i jej część odprowadza się jako gotowy produkt, a część zawraca do procesu mieszania z popiołami.The method of producing monocalcium phosphate feed consists in the fact that ashes from meat and bone waste, calcined in an oxidizing atmosphere at a temperature of 600-1100°C, are mixed with dried monocalcium phosphate being a product of the reaction of ash with phosphoric acid, with the weight ratio of ash to monocalcium phosphate from 1:1 to 1:5. Phosphoric acid with a concentration of preferably 65-75%, in the stoichiometric amount resulting from the reaction of hydroxyapatite and phosphoric acid, is added to this mixture, while stirring, and the reaction is carried out under these conditions for 30 to 60 minutes. Then, the post-reaction mixture containing monocalcium phosphate is dried at the temperature of 105-120°C for 1-3 h and part of it is discharged as a finished product, and part is recycled to the process of mixing with ashes.

PL399597A 2012-06-21 2012-06-21 Process for the preparation of monocalcium phosphate feed PL222555B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL399597A PL222555B1 (en) 2012-06-21 2012-06-21 Process for the preparation of monocalcium phosphate feed

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL399597A PL222555B1 (en) 2012-06-21 2012-06-21 Process for the preparation of monocalcium phosphate feed

Publications (2)

Publication Number Publication Date
PL399597A1 true PL399597A1 (en) 2013-12-23
PL222555B1 PL222555B1 (en) 2016-08-31

Family

ID=49767864

Family Applications (1)

Application Number Title Priority Date Filing Date
PL399597A PL222555B1 (en) 2012-06-21 2012-06-21 Process for the preparation of monocalcium phosphate feed

Country Status (1)

Country Link
PL (1) PL222555B1 (en)

Also Published As

Publication number Publication date
PL222555B1 (en) 2016-08-31

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