PL2204372T3 - Sposób wytwarzania triamidów kwasu tiofosforowego przy użyciu niepolarnych amin - Google Patents
Sposób wytwarzania triamidów kwasu tiofosforowego przy użyciu niepolarnych aminInfo
- Publication number
- PL2204372T3 PL2204372T3 PL10156176T PL10156176T PL2204372T3 PL 2204372 T3 PL2204372 T3 PL 2204372T3 PL 10156176 T PL10156176 T PL 10156176T PL 10156176 T PL10156176 T PL 10156176T PL 2204372 T3 PL2204372 T3 PL 2204372T3
- Authority
- PL
- Poland
- Prior art keywords
- end product
- auxiliary base
- polar
- acid
- base
- Prior art date
Links
- RYYWUUFWQRZTIU-UHFFFAOYSA-N Thiophosphoric acid Chemical compound OP(O)(S)=O RYYWUUFWQRZTIU-UHFFFAOYSA-N 0.000 title abstract 3
- 150000001412 amines Chemical class 0.000 title 1
- 239000007795 chemical reaction product Substances 0.000 abstract 9
- 239000002253 acid Substances 0.000 abstract 6
- 239000002798 polar solvent Substances 0.000 abstract 4
- 150000003839 salts Chemical class 0.000 abstract 4
- DBAKFASWICGISY-DASCVMRKSA-N Dexchlorpheniramine maleate Chemical compound OC(=O)\C=C/C(O)=O.C1([C@H](CCN(C)C)C=2N=CC=CC=2)=CC=C(Cl)C=C1 DBAKFASWICGISY-DASCVMRKSA-N 0.000 abstract 2
- 150000007513 acids Chemical class 0.000 abstract 2
- 239000007791 liquid phase Substances 0.000 abstract 2
- 239000011541 reaction mixture Substances 0.000 abstract 2
- 238000000926 separation method Methods 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- 239000012736 aqueous medium Substances 0.000 abstract 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 abstract 1
- 125000000467 secondary amino group Chemical class [H]N([*:1])[*:2] 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/22—Amides of acids of phosphorus
- C07F9/224—Phosphorus triamides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B63/00—Purification; Separation; Stabilisation; Use of additives
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fertilizers (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102005053540A DE102005053540A1 (de) | 2005-11-08 | 2005-11-08 | Verfahren zur Abtrennung von Säuren aus chemischen Reaktionsgemischen mit Hilfe unpolarer Amine |
| EP10156176A EP2204372B1 (de) | 2005-11-08 | 2006-09-15 | Verfahren zur Herstellung von Thiophosophorsäuretriamiden mit Hilfe unpolarer Amine |
| EP06793548A EP1948670B1 (de) | 2005-11-08 | 2006-09-15 | Verfahren zur abtrennung von säuren aus chemischen reaktionsgemischen mit hilfe unpolarer tertiärer amine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL2204372T3 true PL2204372T3 (pl) | 2012-05-31 |
Family
ID=37596190
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL06793548T PL1948670T3 (pl) | 2005-11-08 | 2006-09-15 | Sposób wydzielania kwasów z chemicznych mieszanin reakcyjnych za pomocą niepolarnych amin trzeciorzędowych |
| PL10156176T PL2204372T3 (pl) | 2005-11-08 | 2006-09-15 | Sposób wytwarzania triamidów kwasu tiofosforowego przy użyciu niepolarnych amin |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL06793548T PL1948670T3 (pl) | 2005-11-08 | 2006-09-15 | Sposób wydzielania kwasów z chemicznych mieszanin reakcyjnych za pomocą niepolarnych amin trzeciorzędowych |
Country Status (18)
| Country | Link |
|---|---|
| US (2) | US9359269B2 (pl) |
| EP (2) | EP1948670B1 (pl) |
| CN (1) | CN101305015A (pl) |
| AT (2) | ATE489393T1 (pl) |
| AU (1) | AU2006311130B2 (pl) |
| BR (1) | BRPI0618331B1 (pl) |
| CA (1) | CA2628503C (pl) |
| DE (2) | DE102005053540A1 (pl) |
| DK (2) | DK1948670T3 (pl) |
| ES (2) | ES2355941T3 (pl) |
| MX (2) | MX295383B (pl) |
| NO (1) | NO20081962L (pl) |
| NZ (1) | NZ567995A (pl) |
| PL (2) | PL1948670T3 (pl) |
| PT (2) | PT2204372E (pl) |
| RU (1) | RU2417229C9 (pl) |
| UA (1) | UA90188C2 (pl) |
| WO (1) | WO2007054392A1 (pl) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102007062614C5 (de) * | 2007-12-22 | 2019-03-14 | Eurochem Agro Gmbh | Mischung zur Behandlung von harnstoffhaltigen Düngemitteln, Verwendungen der Mischung und harnstoffhaltiges Düngemittel enthaltend die Mischung |
| EP2107064A1 (de) * | 2008-04-02 | 2009-10-07 | Basf Se | Verfahren zur Herstellung von Triamiden aus Ammoniak und Amido-Dichloriden |
| CZ302400B6 (cs) | 2008-10-20 | 2011-05-04 | Agra Group, A.S. | Zpusob prípravy N-(hydrokarbyl)triamidu kyseliny fosforecné nebo thiofosforecné |
| CN102746333B (zh) * | 2012-06-12 | 2015-04-01 | 上虞盛晖化工股份有限公司 | 一种n-正丁基硫代磷酰三胺的合成方法 |
| HUE028532T2 (en) | 2012-07-18 | 2016-12-28 | Saltigo Gmbh | Process for the preparation of asymmetric (thio) phosphoric triamides |
| CN104640826A (zh) | 2012-08-15 | 2015-05-20 | 科氏农艺服务有限责任公司 | 含有脲酶抑制剂和二醇烷基醚的改善的液体组合物及其制造和使用方法 |
| CA2881711A1 (en) | 2012-08-15 | 2014-02-20 | Koch Agronomic Services, Llc | Liquid compositions containing urease inhibitors and aryl alkyl alcohols |
| US8888886B1 (en) | 2013-08-06 | 2014-11-18 | Garnett B Whitehurst | NBPT solutions for preparing urease inhibited urea fertilizers prepared from N-substituted morpholines |
| EP3212592A1 (en) | 2014-10-31 | 2017-09-06 | Koch Agronomic Services, LLC | Nitrification inhibitor compositions and methods of making thereof |
| EP3763692B1 (en) | 2014-12-23 | 2024-10-02 | Basf Se | Compositions with improved urease-inhibiting effect comprising (thio) phosphoric acid triamide and further compounds such as amines and colorants |
| HUE061477T2 (hu) | 2015-10-01 | 2023-07-28 | Basf Se | Eljárás (tio)foszforsav-származékot tartalmazó elegy kinyerésére |
| BR112018009985B8 (pt) | 2015-12-01 | 2021-04-06 | Basf Se | processo para o isolamento de um derivado de ácido |
| CN112402998B (zh) * | 2020-12-11 | 2022-06-14 | 安徽标王农牧股份有限公司 | 一种适用于氨基酸的分级提取装置 |
| AU2022238316B2 (en) | 2021-03-15 | 2025-05-08 | Gary David Mcknight | Reaction methods for producing nitrogenous phosphoryl compounds that are in situ fluid compositions |
| US12098109B2 (en) | 2021-03-15 | 2024-09-24 | Soilgenic Technologies, Llc | Reaction methods for producing nitrogenous phosphoryl compounds that are in situ fluid compositions |
| CN113860943B (zh) * | 2021-09-24 | 2022-11-25 | 中船(邯郸)派瑞特种气体股份有限公司 | 一种对三氟甲磺酸制备中釜残的综合处理方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE791311A (fr) | 1971-11-16 | 1973-05-14 | Wacker Chemie Gmbh | Procede pour isoler le chlorure du bis-(dimethylamide) de l'acide phosphorique ou le tris-(dimethylamide) de l'acide phosphorique de leurs solutions impures |
| DD100475A1 (pl) * | 1972-01-31 | 1973-09-20 | ||
| US4530714A (en) * | 1983-03-16 | 1985-07-23 | Allied Corporation | N-aliphatic and N,N-aliphatic phosphoric triamide urease inhibitors and urease inhibited urea based fertilizer compositions |
| CH678054A5 (de) | 1989-07-17 | 1991-07-31 | Enco Eng Ag | Verfahren zur herstellung von tertiaeren amin-schwefel-trioxid-komplexen. |
| US5770771A (en) * | 1997-01-21 | 1998-06-23 | Albemarle Corporation | Preparation of N-hydrocarbylthiophosphoric triamides |
| AR038161A1 (es) | 2002-01-24 | 2004-12-29 | Basf Ag | Procedimiento para separar acidos de mezclas de reaccion quimicas con la ayuda de liquidos ionicos |
| DE10360397A1 (de) | 2003-12-19 | 2005-07-14 | Basf Ag | Verfahren zur Abtrennung von Säuren aus chemischen Reaktionsgemischen mit Hilfe von 1-Alkylimidazolen |
-
2005
- 2005-11-08 DE DE102005053540A patent/DE102005053540A1/de not_active Withdrawn
-
2006
- 2006-09-15 NZ NZ567995A patent/NZ567995A/en not_active IP Right Cessation
- 2006-09-15 PL PL06793548T patent/PL1948670T3/pl unknown
- 2006-09-15 PT PT10156176T patent/PT2204372E/pt unknown
- 2006-09-15 RU RU2008122537/04A patent/RU2417229C9/ru active
- 2006-09-15 US US12/092,392 patent/US9359269B2/en active Active
- 2006-09-15 BR BRPI0618331A patent/BRPI0618331B1/pt not_active IP Right Cessation
- 2006-09-15 ES ES06793548T patent/ES2355941T3/es active Active
- 2006-09-15 DE DE502006008403T patent/DE502006008403D1/de active Active
- 2006-09-15 AT AT06793548T patent/ATE489393T1/de active
- 2006-09-15 CN CNA2006800417865A patent/CN101305015A/zh active Pending
- 2006-09-15 CA CA2628503A patent/CA2628503C/en active Active
- 2006-09-15 DK DK06793548.6T patent/DK1948670T3/da active
- 2006-09-15 AU AU2006311130A patent/AU2006311130B2/en not_active Ceased
- 2006-09-15 EP EP06793548A patent/EP1948670B1/de active Active
- 2006-09-15 PL PL10156176T patent/PL2204372T3/pl unknown
- 2006-09-15 PT PT06793548T patent/PT1948670E/pt unknown
- 2006-09-15 AT AT10156176T patent/ATE540045T1/de active
- 2006-09-15 UA UAA200807757A patent/UA90188C2/ru unknown
- 2006-09-15 DK DK10156176.9T patent/DK2204372T3/da active
- 2006-09-15 WO PCT/EP2006/066397 patent/WO2007054392A1/de not_active Ceased
- 2006-09-15 ES ES10156176T patent/ES2378344T3/es active Active
- 2006-09-15 EP EP10156176A patent/EP2204372B1/de active Active
-
2008
- 2008-04-25 NO NO20081962A patent/NO20081962L/no not_active Application Discontinuation
- 2008-05-02 MX MX2011000779A patent/MX295383B/es unknown
- 2008-05-02 MX MX2008005701A patent/MX285596B/es active IP Right Grant
-
2016
- 2016-05-06 US US15/148,430 patent/US9493491B2/en active Active
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